Production of xylooligosaccharides by microwave-induced, organic acid-catalyzed hydrolysis of different xylan-type hemicelluloses: Optimization by response surface methodology

2017 ◽  
Vol 157 ◽  
pp. 214-225 ◽  
Author(s):  
Qixuan Lin ◽  
Huiling Li ◽  
Junli Ren ◽  
Aojie Deng ◽  
Weiying Li ◽  
...  
Keyword(s):  
Response Surface Methodology ◽  
Organic Acid ◽  
Response Surface ◽  
Acid Catalyzed ◽  
Hydrolysis Of

Enzyme-assisted Extraction for Optimized Recovery of Phenolic Bioactives from Peganum hermala Leaves Using Response Surface Methodology

2018 ◽  
Vol 17 (4) ◽  
pp. 349-354
Author(s):  
Qadir Rahman ◽  
Anwar Farooq ◽  
Amjad Gilani Mazhar ◽  
Nadeem Yaqoob Muhammad ◽  
Ahmad Mukhtar
Keyword(s):  
Response Surface Methodology ◽  
Response Surface ◽  
Enzyme Concentration ◽  
Coumaric Acid ◽  
Assisted Extraction ◽  
Pre Treatment ◽  
Optimized Conditions ◽  
Enzyme Complexes ◽  
Hydrolysis Of ◽  
Central Composite

This study investigates the effect of enzyme formulations (Zympex-014, Kemzyme dry-plus and Natuzyme) on recovery of phenolics from Peganum hermala (harmal) leaves, under optimized conditions using response surface methodology. As compared to the other enzyme complexes, the yield (34 g/100g) obtained through Zympex-014-assisted extraction was higher under optimized conditions such as time (75 min), temperature (70°C), pH (6.5) and enzyme concentration (5 g/100 g) using central composite design (CCD). Effectiveness of Zympex-014 towards hydrolysis of P. hermala leaves cell wall was examined by analyzing the control and enzyme-treated leave residues using scanning electron microscope (SEM). GC/MS characterization authenticated the presence of quercetin (1.44), gallic acid (0.23), caffeic acid (0.04), cinnamic acid (0.05), m-coumaric acid (0.23) and p-coumaric acid (0.37 μg/g) as the potent phenolics in Zympex-014 based extract. It can be concluded from the findings of the current work that pre-treatment of P. hermala leaves with Zympex-014 significantly enhanced the recovery of phenolics that supports its potential uses in the nutra-pharamaceutical industry.

Response Surface Methodology Optimization and Kinetic Study of Ultrafiltration-Enhanced, SCER-catalyzed Hydrolysis of Lard

2019 ◽  
Vol 17 (8) ◽  
Author(s):  
Enmin Lv ◽  
Shaoxuan Ding ◽  
Jie Lu ◽  
Zhuang Li ◽  
Lixiong Du ◽  
...  
Keyword(s):  
Response Surface Methodology ◽  
Reaction Time ◽  
Response Surface ◽  
Membrane Separation ◽  
Molar Ratio ◽  
Transmembrane Pressure ◽  
Cleaning Efficiency ◽  
Membrane Cleaning ◽  
Exponential Factor ◽  
Hydrolysis Of

Abstract The integration process of polyethersulphone (PES) ultrafiltration with catalytic hydrolysis of lard was optimized by response surface methodology (RSM). The influences of molar ratio of water to lard, reaction time and transmembrane pressure on the fatty acids (FAs) yield were investigated. Results showed that the maximum FAs yield of 99.52 % was obtained under the optimized conditions of molar ratio of water to lard of 6.0:1.0, reaction time of 10.0 h and transmembrane pressure of 100.0 kPa. Moreover, the membrane cleaning efficiency was studied after four cleanings. Furthermore, the kinetic model of membrane separation process was investigated and the activation energy and pre-exponential factor were determined.

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