Development of Cd2+ sensor based on BZNA/Nafion/Glassy carbon electrode by electrochemical approach

2018 ◽  
Vol 352 ◽  
pp. 225-231 ◽  
Author(s):  
Reda M. El-Shishtawy ◽  
Huda A. Al-Ghamdi ◽  
M.M. Alam ◽  
Zahra M. Al-amshany ◽  
Abdullah M. Asiri ◽  
...  
2017 ◽  
Vol 184 (7) ◽  
pp. 2123-2129 ◽  
Author(s):  
Mohammed M. Rahman ◽  
Valero G. Alfonso ◽  
Francisco Fabregat-Santiago ◽  
Juan Bisquert ◽  
Abdullah M. Asiri ◽  
...  

2020 ◽  
Vol 44 (46) ◽  
pp. 20285-20293
Author(s):  
Mohammed M. Rahman ◽  
M. M. Alam ◽  
Abdullah M. Asiri ◽  
Jamal Uddin

Selective and sensitive 4-methoxyphenol chemical sensor was developed with a co-doped CeO2–ZrO2 nanocomposite modified glassy carbon electrode as a sensor probe by electrochemical approach for the safety of environmental and ecological fields in broad scales.


RSC Advances ◽  
2020 ◽  
Vol 10 (73) ◽  
pp. 44641-44653
Author(s):  
M. M. Alam ◽  
Abdullah M. Asiri ◽  
M. T. Uddin ◽  
Mohammed M. Rahman ◽  
M. A. Islam

In situ fabrication of a sensitive electrochemical toluene sensor probe using wet-chemically prepared ternary ZnO/MgO/Cr2O3 nanofiber (NF)-decorated glassy carbon electrode (GCE) with Nafion adhesive was the approach of this study.


2021 ◽  
Author(s):  
Md Mahmud Alam ◽  
M.T. Uddin ◽  
Mohammed M. Rahman ◽  
Abdullah M. Asiri ◽  
M.A. Islam

Abstract The 4-NPHyd (4-nitrophenylhydrazine) electrochemical sensor assembled using wet-chemically prepared ZnO/SnO2 nanoparticle (NPs) decorated a glassy carbon electrode (GCE) with conductive Nafion binder. The synthesized NPs characterized by XPS, ESEM, EDS, and XRD analysis. The calibration of the proposed sensor obtained from current versus concentration of 4-NPHyd found linear over a concentration (0.1nM~0.01mM) of 4-NPHyd, which denoted as the dynamic range (LDR) for detection of 4-NPHyd. The 4-NPHyd sensor sensitivity calculated using the LDR slope considering the active surface of GCE (0.0316 cm2), which is equal to be 7.6930 µAµM-1cm-2, an appreciable value. The detection limit (LOD) at signal/noise (S/N=3) estimated, and outstanding lower value at 94.63±4.73 pM perceived. The analytical parameters such as reproducibility, long-term performing ability and response time are found as appreciable. Finally, the projected sensor shows exceptional performances in the detection of 4-NPHyd in environmental samples.


RSC Advances ◽  
2018 ◽  
Vol 8 (35) ◽  
pp. 19754-19764 ◽  
Author(s):  
Mohammed M. Rahman ◽  
Tahir Ali Sheikh ◽  
Reda M. El-Shishtawy ◽  
Muhammad Nadeem Arshad ◽  
Fatimah A. M. Al-Zahrani ◽  
...  

A new Schiff base named 1,1′-(-(naphthalene-2,3-diylbis(azanylylidene))bis(methanylylidene))bis(naphthalen-2-ol) (NDNA) was synthesized by condensation reaction and then characterized by spectroscopic techniques for structure elucidation.


2019 ◽  
Vol 43 (22) ◽  
pp. 8651-8659 ◽  
Author(s):  
M. M. Alam ◽  
Abdullah M. Asiri ◽  
M. T. Uddin ◽  
M. A. Islam ◽  
Md. Rabiul Awual ◽  
...  

Highly sensitive and selective uric acid sensor was fabricated using facile wet-chemically prepared ternary doped ZnO/Ag2O/Co3O4 nanoparticles onto glassy carbon electrode by electrochemical approach, which introduced a prospective and reliable route to the future development of enzyme-free sensor by doped nanomaterials in broad scales.


Sensors ◽  
2020 ◽  
Vol 20 (24) ◽  
pp. 7060
Author(s):  
Mohammed M. Rahman ◽  
Md. M. Alam ◽  
Abdullah M. Asiri ◽  
Firoz. A. D. M. Opo

The facile wet-chemical technique was used to prepare the low-dimensional nano-formulated porous mixed metal oxide nanomaterials (CuO.Mn2O3.NiO; CMNO NMs) in an alkaline medium at low temperature. Detailed structural, morphological, crystalline, and functional characterization of CMNO NMs were performed by X-ray photoelectron spectroscopy (XPS), powder X-ray diffraction (XRD), ultraviolet-visible spectroscopy (UV-vis), Fourier-transform infrared spectroscopy (FTIR), field emission scanning electron microscopy (FESEM), and energy-dispersive X-ray spectroscopy (EDS) analyses. An efficient and selective creatine (CA) sensor probe was fabricated by using CMNO NMs decorated onto glassy carbon electrode (GCE) as CMNO NMs/GCE by using Nafion adhesive (5% suspension in ethanol). The relation of current versus the concentration of CA was plotted to draw a calibration curve of the CMNO NMs/GCE sensor probe, which was found to have a very linear value (r2 = 0.9995) over a large dynamic range (LDR: 0.1 nM~0.1 mM) for selective CA detection. The slope of LDR by considering the active surface area of GCE (0.0316 cm2) was applied to estimate the sensor sensitivity (14.6308 µAµM−1 cm−2). Moreover, the detection limit (21.63 ± 0.05 pM) of CMNO MNs modified GCE was calculated from the signal/noise (S/N) ratio at 3. As a CA sensor probe, it exhibited long-term stability, good reproducibility, and fast response time in the detection of CA by electrochemical approach. Therefore, this research technique is introduced as a promising platform to develop an efficient sensor probe for cancer metabolic biomarker by using nano-formulated mixed metal oxides for biochemical as well as biomedical research for the safety of health care fields.


2018 ◽  
Vol 42 (2) ◽  
pp. 1169-1180 ◽  
Author(s):  
Mohammad Musarraf Hussain ◽  
Abdullah M. Asiri ◽  
Muhammad Nadeem Arshad ◽  
Mohammed M. Rahman

A thin-layer of (E)-N′-methoxybenzylidenebenzenesulfonohydrazide (MBBSH) was fabricated by the deposition of MBBSH onto a smooth glassy carbon electrode with nafion binder for the sensitive and selective Ga3+ sensor probe.


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