Simultaneous thermogravimetric analysis and in situ thermo-Raman spectroscopic investigation of thermal decomposition of zinc acetate dihydrate forming zinc oxide nanoparticles

2003 ◽  
Vol 381 (3-4) ◽  
pp. 262-270 ◽  
Author(s):  
Anil Vithal Ghule ◽  
Bertrand Lo ◽  
Shin-Hwa Tzing ◽  
Kalyani Ghule ◽  
Hua Chang ◽  
...  
Keyword(s):  
Thermal Decomposition ◽  
Zinc Oxide ◽  
Thermogravimetric Analysis ◽  
Spectroscopic Investigation ◽  
Zinc Oxide Nanoparticles ◽  
Zinc Acetate Dihydrate ◽  
Oxide Nanoparticles ◽  
Acetate Dihydrate ◽  
Raman Spectroscopic

scholarly journals Synthesis of N-doped ZnO nanoparticles with cabbage morphology as a catalyst for the efficient photocatalytic degradation of methylene blue under UV and visible light

RSC Advances ◽  
2019 ◽  
Vol 9 (13) ◽  
pp. 7509-7535 ◽  
Author(s):  
Eswaran Prabakaran ◽  
Kriveshini Pillay
Keyword(s):  
Methylene Blue ◽  
Zinc Oxide ◽  
Zno Nanoparticles ◽  
Zinc Oxide Nanoparticles ◽  
Zinc Acetate Dihydrate ◽  
Oxide Nanoparticles ◽  
Acetate Dihydrate ◽  
Hydrazine Monohydrate ◽  
Nitrogen Doped ◽  
Doped Zno

In this study, the synthesis of nitrogen-doped zinc oxide nanoparticles with a cabbage like morphology (N-ZnONCBs) by a hydrothermal method using zinc acetate dihydrate as a precursor and hydrazine monohydrate as a nitrogen source is reported.

scholarly journals Phytosynthetic Ag doped ZnO nanoparticles: Semiconducting green remediators

2018 ◽  
Vol 16 (1) ◽  
pp. 556-570 ◽  
Author(s):  
Khuram Shahzad Ahmad ◽  
Shaan Bibi Jaffri
Keyword(s):  
Zinc Oxide ◽  
Zno Nanoparticles ◽  
Zinc Oxide Nanoparticles ◽  
Organic Dyes ◽  
Zinc Acetate Dihydrate ◽  
Polluted Water ◽  
Oxide Nanoparticles ◽  
Pseudo First Order Reaction ◽  
One Pot ◽  
Doped Zno

AbstractHighly stable semiconducting silver doped zinc oxide nanoparticles have been synthesized via facile, biomimetic and sustainable route, through utilization of Zinc acetate dihydrate (C4H6O4Zn · 2H2O) as host, Silver nitrate (AgNO3) as dopant and phytochemicals of angiospermic medicinal plant Prunus cerasifera as the reducing agents. Synthesis of Ag doped ZnO nanoparticles was done in a one pot synthetic mode by varying the amount of dopant from 0.2 – 2.0%. Synthesized photocatalyst nanoparticles were analyzed via UV-vis, FTIR, XRD and SEM. Commendable alleviation in the direct band gap i.e. 2.81 eV was achieved as a result of doping. Silver doped zinc oxide nanoparticles size ranged between 72.11 – 100 nm with rough surface morphology and higher polydispersity degree. The XRD patterns revealed the hexagonal wurtzite geometry of crystals with an average crystallite size of 2.99 nm. Persistent organic dyes Methyl Orange, Safranin O and Rhodamine B were sustainably photodegraded in direct solar irradiance with remarkable degradation percentages up to 81.76, 74.11 and 85.52% in limited time with pseudo first order reaction kinetics (R2 =0.99, 0.99 and 0.97). Furthermore, efficient inhibition against nine microbes of biomedical and agriculturally significance was achieved. Synthesized nanoparticles are potential green remediators of polluted water and perilous pathogens.

Zinc oxide nanoparticles with surface modified by degradation of capping polymers in situ during microwave synthesis

2015 ◽  
Vol 26 (4) ◽  
pp. 1064-1071 ◽  
Author(s):  
Jakub Sedlák ◽  
Ivo Kuřitka ◽  
Michal Machovský ◽  
Pavol Šuly ◽  
Pavel Bažant ◽  
...  
Keyword(s):  
Zinc Oxide ◽  
Microwave Synthesis ◽  
Zinc Oxide Nanoparticles ◽  
Oxide Nanoparticles ◽  
Surface Modified

Electrochemical Method for Analysis of Cholesterol Based on In Situ Synthesized Graphene Decorated with Zinc Oxide Nanoparticles

2013 ◽  
Vol 3 (1) ◽  
pp. M5-M9 ◽  
Author(s):  
E. Watanabe ◽  
R. Spidle ◽  
S. Caudle ◽  
G. Manani ◽  
A. K. Wanekaya ◽  
...  
Keyword(s):  
Zinc Oxide ◽  
Zinc Oxide Nanoparticles ◽  
Electrochemical Method ◽  
Oxide Nanoparticles

In-situ study of mass and current density for electrophoretic deposition of zinc oxide nanoparticles

2016 ◽  
Vol 42 (6) ◽  
pp. 6906-6913 ◽  
Author(s):  
Meisam Hasanpoor ◽  
Mahmood Aliofkhazraei ◽  
Hamid Delavari H.
Keyword(s):  
Zinc Oxide ◽  
Electrophoretic Deposition ◽  
Current Density ◽  
Zinc Oxide Nanoparticles ◽  
Oxide Nanoparticles ◽  
In Situ Study

scholarly journals Zinc Oxide Nanoparticles for Removal of Arsenic from Water

2019 ◽  
Vol 8 (3S) ◽  
pp. 117-122
Keyword(s):  
Zinc Oxide ◽  
Zinc Oxide Nanoparticles ◽  
Linear Trend ◽  
Zinc Acetate Dihydrate ◽  
Sol Gel ◽  
Total Surface Area ◽  
Nanoparticle Size ◽  
Oxide Nanoparticles ◽  
Calcination Temperatures ◽  
Average Size

Removal of arsenate, As(V) from water was achieved using zinc oxide nanoparticles. The nanoparticles were synthesised from zinc acetate dihydrate and sodium hydroxide (NaOH) using the wet chemical sol-gel method. Different synthesis parameters were explored; including different ratios of Zn:NaOH and calcination temperatures. The synthesised samples were subsequently characterised and tested to investigate the adsorption capabilities of ZnO towards As(V). The colourimetric approach was utilised to analyse the samples’ performance. The particles had a relatively large average size as tested by the nanoparticle size analyser and the X-Ray Diffraction (XRD) characterisation of the samples confirmed the formation of ZnO. The peaks were narrow with high intensity, which indicates a larger crystal size and stable crystallinity. The samples showed a linear trend of increased adsorption capacity with the contact time. However, as indicated by the XRD and nanoparticle size analyser results, the particles had agglomerated and this has caused the total surface area to shrink. In summary, ZnO nanoparticles were successfully synthesised and were successful in adsorbing As(V) with different percentages for each sample. The adsorption trend was clear with respect to the changing parameters.

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