Exposure assessment of French women and their newborn to brominated flame retardants: Determination of tri- to deca- polybromodiphenylethers (PBDE) in maternal adipose tissue, serum, breast milk and cord serum

2009 ◽  
Vol 157 (1) ◽  
pp. 164-173 ◽  
Author(s):  
Jean-Philippe Antignac ◽  
Ronan Cariou ◽  
Daniel Zalko ◽  
Alain Berrebi ◽  
Jean-Pierre Cravedi ◽  
...  
Author(s):  
Yu-Jie BEN ◽  
Long LI ◽  
Wen-Yue WANG ◽  
Xing-Hong LI ◽  
Yuan TIAN ◽  
...  

Chemosphere ◽  
2008 ◽  
Vol 73 (7) ◽  
pp. 1036-1041 ◽  
Author(s):  
Ronan Cariou ◽  
Jean-Philippe Antignac ◽  
Daniel Zalko ◽  
Alain Berrebi ◽  
Jean-Pierre Cravedi ◽  
...  

2008 ◽  
Vol 52 (2) ◽  
pp. 258-265 ◽  
Author(s):  
Jean-Philippe Antignac ◽  
Ronan Cariou ◽  
Daniel Maume ◽  
Philippe Marchand ◽  
Fabrice Monteau ◽  
...  

2014 ◽  
Vol 989-994 ◽  
pp. 506-510
Author(s):  
Ying Jie Chen ◽  
Pei Gang Dai ◽  
Liu Zhi Peng ◽  
Chao Du ◽  
Shang Jin Liang

A method of supercritical CO2 fluid extraction gas chromatography-mass spectrometry (GC-MS) was developed for the determination of 2 novel brominated flame retardants (BB-153 and TBECH)) in flexible polyurethane foam. The optimum conditions as follows: extraction temperature: 60°C, pressure:30Mpa, CO2 mass flow rate: 8g/min ,flow rate of methanol entrainer: 3mL/min and extraction time: 60min. The calibration curves were linear in the range of 0.1~50μg/mL with correlation coefficient of 0.9995~0.9999 and detection limits (S/N=20) of 0.05μg/mL. The average recoveries of the target compounds in sample were in the range of 97.3%~98.8%(BB-153)、99.2%~105.8% (TBECH) respectively. The results showed that this method was sensitive, reliable and environmental for the determination of 2 novel brominated flame retardants (BB-153 and TBECH)) in flexible polyurethane foam.


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