Comparison of four kinds of extraction techniques and kinetics of microwave-assisted extraction of vanillin from Vanilla planifolia Andrews

2014 ◽  
Vol 149 ◽  
pp. 54-61 ◽  
Author(s):  
Zhizhe Dong ◽  
Fenglin Gu ◽  
Fei Xu ◽  
Qinghuang Wang
2008 ◽  
Vol 91 (5) ◽  
pp. 1124-1129 ◽  
Author(s):  
Takamitsu Otake ◽  
Yoshie Aoyagi ◽  
Masahiko Numata ◽  
Takashi Yarita

Abstract The efficiency of microwave-assisted extraction (MAE) was evaluated for the analysis of polychlorinated biphenyls (PCBs) and organochlorine pesticides (OCPs) in fish. An isotope dilution method was used for quantification via analysis of the samples by gas chromatography and mass spectrometry. MAE solvent, temperature, and time were optimized, and observed concentrations were compared. The MAE results were also compared to those of other extraction techniques (Soxhlet extraction, pressurized liquid extraction, saponification, and homogenization). Concentrations of PCBs and OCPs obtained by MAE at 120C for 10 min were comparable to those by the other techniques. The results suggest that MAE can be used for the analysis of PCBs and OCPs in fish.


Author(s):  
Megawati ◽  
D S Fardhyanti ◽  
D Widjanarko ◽  
Hanifah ◽  
G M Bungsu ◽  
...  

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