Formation mechanisms of precipitates in an Al–Cu–Li–Zr alloy and their effects on strength and electrical resistance of the alloy

There have Been a number of studies of low-angle, θ < 4°, [10] tilt boundaries in the diamond lattice. Dislocations with Burgers vectors a/2<110>, a/2<112>, a<111> and a<001> have been reported in melt-grown bicrystals of germanium, and dislocations with Burgers vectors a<001> and a/2<112> have been reported in hot-pressed bicrystals of silicon. Most of the dislocations were found to be dissociated, the dissociation widths being dependent on the tilt angle. Possible dissociation schemes and formation mechanisms for the a<001> and a<111> dislocations from the interaction of lattice dislocations have recently been given.The present study reports on the dislocation structure of a 10° [10] tilt boundary in chemically vapor deposited silicon. The dislocations in the boundary were spaced about 1-3nm apart, making them difficult to resolve by conventional diffraction contrast techniques. The dislocation structure was therefore studied by the lattice-fringe imaging technique.

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Formation Mechanisms for Multiply Twinned Particles During Nucleation in the Au/MICA System

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100114049 ◽

1975 ◽

Vol 33 ◽

pp. 84-85

Author(s):

Eal H. Lee ◽

Helmut Poppa

Keyword(s):

Deposition Time ◽

High Vacuum ◽

Dark Field ◽

Ultra High Vacuum ◽

Formation Mechanisms ◽

Heat Treated ◽

Cluster Density ◽

Diffraction Patterns ◽

Crystal Particle ◽

Multiply Twinned Particles

The formation of thin films of gold on mica has been studied in ultra-high vacuum (5xl0-10 torr) . The mica substrates were heat-treated for 24 hours at 375°C, cleaved, and annealed for 15 minutes at the deposition temperature of 300°C prior to deposition. An impingement flux of 3x1013 atoms cm-2 sec-1 was used. These conditions were found to give high number densities of multiple twin particles and are based on a systematic series of nucleation experiments described elsewhere. Individual deposits of varying deposition time were made and examined by bright and dark field TEM after "cleavage preparation" of highly transparent specimens. In the early stages of growth, the films generally consist of small particles which are either single crystals or multiply twinned; a strong preference for multiply twinned particles was found whenever the particle number densities were high. Fig. 1 shows the stable cluster density ns and the variation with deposition time of multiple twin particle and single crystal particle densities, respectively. Corresponding micrographs and diffraction patterns are shown in Fig. 2.

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Microtwinning Evidence For The Apparent Five-Fold Symmetry in T2(Al6Li3Cu)

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100125178 ◽

1987 ◽

Vol 45 ◽

pp. 24-25

Author(s):

Kenneth S. Vecchio ◽

David B. Williams

Keyword(s):

Stable Equilibrium ◽

Equilibrium Phase ◽

Convergent Beam Electron Diffraction ◽

Icosahedral Structure ◽

Cubic Crystals ◽

Icosahedral Phases ◽

Heat Treated ◽

Zero Layer ◽

Convergent Beam ◽

Zr Alloy

Since the discovery in 1984 by Shechtman et al. of crystals which display apparent five-fold symmetry, extensive effort has been given to establishing a theoretical basis for the existence of icosahedral phases (eg.2.). Several other investigations have been centered on explaining these observations based on twinning of cubic crystals (eg.3.). Recently, the existence of a stable, equilibrium phase T2Al6 Li3Cu) possessing an icosahedral structure has been reported in the Al-Li-Cu system(4-6).In the present study an Al-2.6wt.%Li-l.5wt.%Cu-0.lwt.%Zr alloy was heat treated at 300°C for 100hrs. to produce large T2 precipitates. Convergent Beam Electron Diffraction (CBED) patterns were obtained from two-fold, three-fold, and apparent five-fold axes of T2 particles. Figure 1 shows the five-fold symmetric zero layer CBED pattern obtained from T2 particles.

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Deformation and fracture behavior of an Al-Li-Cu-Mg-Zr alloy 8090

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100178008 ◽

1990 ◽

Vol 48 (4) ◽

pp. 974-975

Author(s):

D.M. Jiang ◽

B.D. Hong

Keyword(s):

High Strength ◽

Deformation And Fracture ◽

Fracture Behaviors ◽

Aluminum Lithium ◽

Carbon Fiber Reinforced Composites ◽

Peak Aged ◽

Aluminum Lithium Alloys ◽

High Strength Aluminum Alloys ◽

Lithium Alloys ◽

Zr Alloy

Aluminum-lithium alloys have been recently got strong interests especially in the aircraft industry. Compared to conventional high strength aluminum alloys of the 2000 or 7000 series it is anticipated that these alloys offer a 10% increase in the stiffness and a 10% decrease in density, thus making them rather competitive to new up-coming non-metallic materials like carbon fiber reinforced composites.The object of the present paper is to evaluate the inluence of various microstructural features on the monotonic and cyclic deformation and fracture behaviors of Al-Li based alloy. The material used was 8090 alloy. After solution treated and waster quenched, the alloy was underaged (190°Clh), peak-aged (190°C24h) and overaged (150°C4h+230°C16h). The alloy in different aging condition was tensile and fatigue tested, the resultant fractures were observed in SEM. The deformation behavior was studied in TEM.

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