Synthesis and size control of monodisperse copper nanoparticles by polyol method

2007 ◽  
Vol 311 (2) ◽  
pp. 417-424 ◽  
Author(s):  
Bong Kyun Park ◽  
Sunho Jeong ◽  
Dongjo Kim ◽  
Jooho Moon ◽  
Soonkwon Lim ◽  
...  
Keyword(s):  
Copper Nanoparticles ◽  
Size Control ◽  
Polyol Method

Understanding the Size Control Mechanism for Pt/C Catalysts Made Using the Polyol Method

2013 ◽  
pp. 165-172
Author(s):  
P.C. Favilla ◽  
J.J. Acosta ◽  
C.E. Schvezov ◽  
D.J. Sercovich ◽  
J.R. Collet-Lacoste
Keyword(s):  
Control Mechanism ◽  
Size Control ◽  
Polyol Method

scholarly journals Synthesis of Copper Nanoparticles Using Glass Microfluidic Device

Proceedings ◽  
2018 ◽  
Vol 2 (13) ◽  
pp. 1110
Author(s):  
Yiyang Liang ◽  
Yoko Shinozaki ◽  
Hiromasa Yagyu
Keyword(s):  
Particle Size ◽  
Ascorbic Acid ◽  
Microfluidic Device ◽  
Copper Nanoparticles ◽  
Flow Rate ◽  
Control Method ◽  
Size Control ◽  
Metallic Materials ◽  
First Time ◽  
Citrate Reduction

In a synthesis of gold nanoparticles on a microfluidic device by citrate reduction, a particle size control by changing a flow rate was reported. To apply this simple control method to the synthesis of other metallic materials, we propose the synthesis of copper nanoparticles (CuNPs) in ethylene glycol by the microfluidic device using ascorbic acid as both antioxidant and reducing agent. The experimental results found for the first time that the effect of the flow rate of agents on particle size of the synthesized CuNPs in the device.

Synthesis and size control of copper nanoparticles and their catalytic application

2015 ◽  
Vol 25 (12) ◽  
pp. 3995-4000 ◽  
Author(s):  
Shikha JAIN ◽  
Ankita JAIN ◽  
Pranav KACHHAWAH ◽  
Vijay DEVRA
Keyword(s):  
Copper Nanoparticles ◽  
Size Control ◽  
Catalytic Application

scholarly journals Efficient size control of copper nanoparticles generated in irradiated aqueous solutions of star-shaped polyelectrolyte containers

2015 ◽  
Vol 17 (17) ◽  
pp. 11490-11498 ◽  
Author(s):  
Alexey A. Zezin ◽  
Vladimir I. Feldman ◽  
Sergei S. Abramchuk ◽  
Gurgen V. Danelyan ◽  
Victor V. Dyo ◽  
...  
Keyword(s):  
Acrylic Acid ◽  
Aqueous Solutions ◽  
Copper Nanoparticles ◽  
Size Control ◽  
Radiation Induced ◽  
Poly Acrylic Acid

Star-shaped poly(acrylic acid) macromolecules act as nanoreactors for the preparation of narrow-dispersed copper nanoparticles by radiation-induced reduction of copper(ii) ions.

Synthesis of Silver-Copper Nanoparticles via Polyol Method: Effect of Reaction Time and Temperature

2015 ◽  
Vol 1113 ◽  
pp. 605-610 ◽  
Author(s):  
Nurul Hikmah ◽  
Nor Faeqah ◽  
Abdul Hadi
Keyword(s):  
Reaction Time ◽  
Copper Nanoparticles ◽  
Tween 80 ◽  
Polyol Method ◽  
Face Centered Cubic ◽  
X Ray Diffraction ◽  
Sorbitan Monooleate ◽  
Silver Copper ◽  
Green Approach ◽  
Face Centered

This paper discusses the effect of reaction time and temperature of silver-copper nanoparticles prepared by a polyol method. In this study, silver-copper nanoparticles were synthesized through the green approach of polyol method using ethylene glycol (EG) as green solvent and reductant, and polyoxyethylene-(80)-sorbitan monooleate (Tween 80) as a nontoxic stabilizer. The phase and morphology of silver-copper nanoparticles were characterized by X-ray diffraction (XRD) and Field emission scanning electron microscope (FESEM). The results XRD confirmed silver and copper nanoparticles to be phase-pure crystalline silver and copper with face-centered cubic (fcc) structure on the basis of XRD analyses. FESEM analysis confirmed the existence of Ag and Cu nanoparticles.

Synthesis of copper nanoparticles and role of pH on particle size control

2016 ◽  
Vol 3 (6) ◽  
pp. 1985-1991 ◽  
Author(s):  
K.M. Rajesh ◽  
B. Ajitha ◽  
Y. Ashok Kumar Reddy ◽  
Y. Suneetha ◽  
P. Sreedhara Reddy
Keyword(s):  
Particle Size ◽  
Copper Nanoparticles ◽  
Size Control ◽  
Particle Size Control

Palladium–zinc catalysts on mesoporous titania prepared by colloid synthesis. I. Size control synthesis of PdZn nanoclusters by a polyol method

2012 ◽  
Vol 14 (9) ◽  
Author(s):  
Lyudmila B. Okhlopkova ◽  
Michail A. Kerzhentsev ◽  
Fedor V. Tuzikov ◽  
Yurii V. Larichev ◽  
Igor P. Prosvirin ◽  
...  
Keyword(s):  
Size Control ◽  
Polyol Method ◽  
Control Synthesis ◽  
Mesoporous Titania ◽  
Colloid Synthesis

scholarly journals Polyol-mediated synthesis of size-controlled copper nanoparticles under microwave irradiation

2019 ◽  
Vol 17 (12.1) ◽  
pp. 21
Author(s):  
Anh Trần Thị Kiều ◽  
Trung Đặng Bảo
Keyword(s):  
Microwave Irradiation ◽  
Copper Nanoparticles ◽  
Inductively Coupled Plasma ◽  
Size Control ◽  
X Ray Diffraction ◽  
Inductively Coupled ◽  
Transmission Electron ◽  
Icp Ms ◽  
Plasma Mass Spectrometry ◽  
Size Controlled

In this research, well-dispersed zero-valent copper nanoparticles (CuNPs) were successfully synthesized from a well-defined complex of [Cu(OH)(TMEDA)]2Cl2 in neat glycerol via a polyol method, under microwave irradiation (MW) assistance. The as-prepared CuNPs were thoroughly characterized by means of various techniques such as inductively coupled plasma mass spectrometry (ICP-MS), Ultraviolet-visible spectroscopy (UV-vis), X-ray diffraction (XRD) and transmission electron microscopy (TEM) analyses, evidencing the formation of the spherical nanoparticles with the range of 3.24.2 nm in mean diameter. In addition, the size control of obtained CuNPs was examined via reaction time, thereby showing that the formation of CuNPs conformed to the model of “mono-dispersion”.

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