Large-scale synthesis of uniform Cu2O stellar crystals via microwave-assisted route

2004 ◽  
Vol 260 (3-4) ◽  
pp. 490-493 ◽  
Author(s):  
Zhengcui Wu ◽  
Mingwang Shao ◽  
Wu Zhang ◽  
Youbao Ni
Keyword(s):  
Large Scale ◽  
Microwave Assisted ◽  
Large Scale Synthesis

Industrializable synthesis of narrow-dispersed carbon dots achieved by microwave-assisted selective carbonization of surfactants and their applications as fluorescent nano-additives

2020 ◽  
Vol 8 (40) ◽  
pp. 21317-21326
Author(s):  
Laiping Fang ◽  
Minjian Wu ◽  
Chushu Huang ◽  
Zhaoyang Liu ◽  
Jinlun Liang ◽  
...  
Keyword(s):  
Carbon Dots ◽  
Large Scale ◽  
Economic Strategy ◽  
Microwave Assisted ◽  
Nano Additives ◽  
Large Scale Synthesis

The robust and economic strategy for the large-scale synthesis of narrow-dispersed hydrophobic C-dots and their successful application as fluorescent nano-additives indicate that C-dots are ready to go from lab to industry.

Large scale synthesis of ultrathin cupric oxide nanosheets via a rapid microwave-assisted and template-free route

2018 ◽  
Vol 214 ◽  
pp. 138-141
Author(s):  
Xingrong Han ◽  
Fan Liao ◽  
Yanfei Zhang ◽  
Chunju Xu ◽  
Huiyu Chen
Keyword(s):  
Large Scale ◽  
Cupric Oxide ◽  
Microwave Assisted ◽  
Template Free ◽  
Large Scale Synthesis

A rapid, high-yield and large-scale synthesis of uniform spherical silver nanoparticles by a microwave-assisted polyol process

RSC Advances ◽  
2015 ◽  
Vol 5 (112) ◽  
pp. 92144-92150 ◽  
Author(s):  
Jens Helmlinger ◽  
Martin Heise ◽  
Marc Heggen ◽  
Michael Ruck ◽  
Matthias Epple
Keyword(s):  
Silver Nanoparticles ◽  
Medical Devices ◽  
Large Scale ◽  
Consumer Products ◽  
Polyol Process ◽  
High Yield ◽  
Microwave Assisted ◽  
Large Scale Synthesis

Silver nanoparticles, often applied in medical devices and consumer products, can be conveniently prepared by microwave-based synthesis.

Microwave-assisted and large-scale synthesis of SnO2/carbon-nanotube hybrids with high lithium storage capacity

RSC Advances ◽  
2015 ◽  
Vol 5 (72) ◽  
pp. 58568-58573 ◽  
Author(s):  
Junting Zhang ◽  
Youqi Zhu ◽  
Chuanbao Cao ◽  
Faheem K. Butt
Keyword(s):  
Carbon Nanotube ◽  
Large Scale ◽  
High Efficiency ◽  
Storage Capacity ◽  
Atmospheric Condition ◽  
Cost Effective ◽  
Lithium Storage ◽  
Microwave Assisted ◽  
Large Scale Synthesis ◽  
Microwave Assisted Method

The microwave-assisted method is timesaving, cost-effective, high-efficiency and can be accessed under atmospheric condition.

A microwave-assisted template-free route for large-scale synthesis of photoluminescent single crystal CsPbI3 nanotubes

CrystEngComm ◽  
2020 ◽  
Vol 22 (4) ◽  
pp. 623-627
Author(s):  
Weiwei Xiong ◽  
Ziyi Zhang ◽  
Yutao Huang ◽  
Chenxin Xu ◽  
Jiajing Wu ◽  
...  
Keyword(s):  
Single Crystal ◽  
Large Scale ◽  
Synthetic Approach ◽  
High Quality ◽  
Single Crystalline ◽  
Microwave Assisted ◽  
Template Free ◽  
Large Scale Synthesis ◽  
Highly Uniform

High-quality single crystalline CsPbI3 nanotubes featuring highly uniform sizes and stable and bright photoluminescence were synthesized through a microwave-assisted synthetic approach.

scholarly journals Microwave-Assisted Expeditious Synthesis of 2-Alkyl-2-(N-arylsulfonylindol-3-yl)-3-N-acyl-5-aryl-1,3,4-oxadiazolines Catalyzed by HgCl2 under Solvent-Free Conditions as Potential Anti-HIV-1 Agents

Molecules ◽  
2018 ◽  
Vol 23 (11) ◽  
pp. 2936 ◽  
Author(s):  
Zhiping Che ◽  
Yuee Tian ◽  
Shengming Liu ◽  
Jia Jiang ◽  
Mei Hu ◽  
...  
Keyword(s):  
Large Scale ◽  
Reaction Times ◽  
Solvent Free ◽  
Catalyst Loading ◽  
Microwave Assisted ◽  
Solvent Free Conditions ◽  
Large Scale Synthesis ◽  
Low Catalyst Loading ◽  
Anti Hiv ◽  
Hiv 1

A series of 2-alkyl-2-(N-arylsulfonylindol-3-yl)-3-N-acyl-5-aryl-1,3,4-oxadiazolines were expeditious prepared under microwave-assisted, catalyzed by HgCl2 and solvent-free conditions. This method has the advantage of low catalyst loading and recovering catalyst, ease reaction and repaid reaction times, easy separation products and excellent yields, and more conducive to the large-scale synthesis products. Furthermore, compounds 3s, 3y, 3a′, 3b′, 3f′, 3i′, 3q′, and 3r′ exhibited more potent anti-HIV-1 activity with EC50 values of 3.35, 6.12, 3.63, 9.54, 1.79, 0.51, 3.00, and 4.01 μg/mL, and TI values of 32.66, >32.68, 31.22, 13.94, 24.27, 39.59, 26.01, and 24.51, respectively. Especially compound 3i′ displayed the highest anti-HIV-1 activity with TI values of 39.59.

Exogenous Directing Group Free, Ligand-Enabled gamma-C(sp3)–H Arylation of Free Primary Aliphatic Amines and α-Amino Esters

2019 ◽  
Author(s):  
Yongzheng Ding ◽  
Shuai Fan ◽  
Xiaoxi Chen ◽  
yuzhen gao ◽  
Gang Li
Keyword(s):  
Amino Acids ◽  
Large Scale ◽  
Free Ligand ◽  
Aliphatic Amines ◽  
Rapid Synthesis ◽  
Amino Esters ◽  
Directing Group ◽  
Large Scale Synthesis ◽  
Primary Aliphatic Amines

A Pdᴵᴵ-catalyzed, ligand-enabled gamma-C(sp3)–H arylation of free primary aliphatic amines and amino esters without using an exogenous directing group is reported. This reaction is compatible with unhindered free aliphatic amines, and it is also be applicable to the rapid synthesis of biologically and synthetically valuable unnatural α-amino acids. Large scale synthesis is also feasible using this method.<br>

A Simplified Protocol for the ortho-Deuteration of Acidic Aromatic Compounds in D2O

2019 ◽  
Author(s):  
Alyssa Garreau ◽  
Hanyang Zhou ◽  
Michael Young
Keyword(s):  
Carboxylic Acid ◽  
Aromatic Compounds ◽  
Large Scale ◽  
Simplified Approach ◽  
Directing Group ◽  
Large Scale Synthesis

<div>Methods to catalytically introduce deuterium in synthetically useful yields ortho to a carboxylic acid directing group on arenes typically requires D2 or CD3CO2D, which makes using these approaches cost prohibitive for large scale synthesis (equipment and reagent costs respectively). Herein we present a simplified approach using catalytic RhIII and D2O as deuterium source, and show its application to H/D exchange on various acidic substrates.</div>

A Simplified Protocol for the ortho-Deuteration of Acidic Aromatic Compounds in D2O

2019 ◽  
Author(s):  
Alyssa Garreau ◽  
Hanyang Zhou ◽  
Michael Young
Keyword(s):  
Carboxylic Acid ◽  
Aromatic Compounds ◽  
Large Scale ◽  
Simplified Approach ◽  
Directing Group ◽  
Large Scale Synthesis

<div>Methods to catalytically introduce deuterium in synthetically useful yields ortho to a carboxylic acid directing group on arenes typically requires D2 or CD3CO2D, which makes using these approaches cost prohibitive for large scale synthesis (equipment and reagent costs respectively). Herein we present a simplified approach using catalytic RhIII and D2O as deuterium source, and show its application to H/D exchange on various acidic substrates.</div>

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