Measuring residual stress in Ti-6Al-4V with HR-EBSD, using reference patterns from annealed material

The oxidation of natural olivine has previously been performed on bulk samples and the reactions followed by preparation of TEM specimens from the annealed material. These results show that below ∼1000°C hematite and amorphous silica are formed, particularly around dislocations. At higher temperatures magnetite and some enstatite-like phase are formed. In both cases the olivine is left almost totally Fe depleted. By performing the oxidation on characterized thin TEM specimens it is possible to obtain more information on the nucleation and growth of the second phases formed. The conditions in a thin foil, however, are very different from those in the bulk especially with regard to surface effects. The nucleation of precipitates in particular may be expected to occur differently in these thin foils than in the bulk.TEM specimens of natural olivine (approximate composition Mg+Fe+Si2o4) which had been annealed at 1000°C for 1 hr were prepared by mechanical polishing and dimpling, followed by Ar ion milling to perforation. The specimens were characterized in the electron microscope and then heated in air in alumina boats to 900°C for between 30 and 180 minutes.

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The influence of heat treatment on the fiber/matrix interface in a SiC-reinforced glassceramic

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100105771 ◽

1988 ◽

Vol 46 ◽

pp. 742-743

Author(s):

E. Bischoff ◽

O. Sbaizero

Keyword(s):

Heat Treatment ◽

Aluminum Silicate ◽

Lithium Aluminum ◽

Interfacial Region ◽

Specimen Preparation ◽

Crack Wake ◽

Pull Out ◽

Annealed Material ◽

Ultrasonic Drilling ◽

Fiber Matrix Interface

Fiber or whisker reinforced ceramics show improved toughness and strength. Bridging by intact fibers in the crack wake and fiber pull-out after failure contribute to the additional toughness. These processes are strongly influenced by the sliding and debonding resistance of the interfacial region. The present study examines the interface in a laminated 0/90 composite consisting of SiC (Nicalon) fibers in a lithium-aluminum-silicate (LAS) glass-ceramic matrix. The material shows systematic changes in sliding resistance upon heat treatment.As-processed samples were annealed in air at 800 °C for 2, 4, 8, 16 and 100 h, and for comparison, in helium at 800 °C for 4 h. TEM specimen preparation of as processed and annealed material was performed with special care by cutting along directions having the fibers normal and parallel to the section plane, ultrasonic drilling, dimpling to 100 pm and final ionthinning. The specimen were lightly coated with Carbon and examined in an analytical TEM operated at 200 kV.

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TEM investigations of surface residual stress relaxation in A12O3 and Al2O3-SiC nanocomposite

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100170876 ◽

1994 ◽

Vol 52 ◽

pp. 628-629

Author(s):

J. Fang ◽

H. M. Chan ◽

M. P. Harmer

Keyword(s):

Residual Stress ◽

Single Phase ◽

Stress Relief ◽

Stress Recovery ◽

Surface Residual Stress ◽

Microscopic Mechanism ◽

Sic Particles ◽

Annealing Procedure ◽

The Difference ◽

Nano Size

It was Niihara et al. who first discovered that the fracture strength of Al2O3 can be increased by incorporating as little as 5 vol.% of nano-size SiC particles (>1000 MPa), and that the strength would be improved further by a simple annealing procedure (>1500 MPa). This discovery has stimulated intense interest on Al2O3/SiC nanocomposites. Recent indentation studies by Fang et al. have shown that residual stress relief was more difficult in the nanocomposite than in pure Al2O3. In the present work, TEM was employed to investigate the microscopic mechanism(s) for the difference in the residual stress recovery in these two materials.Bulk samples of hot-pressed single phase Al2O3, and Al2O3 containing 5 vol.% 0.15 μm SiC particles were simultaneously polished with 15 μm diamond compound. Each sample was cut into two pieces, one of which was subsequently annealed at 1300° for 2 hours in flowing argon. Disks of 3 mm in diameter were cut from bulk samples.

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Residual stress measurements and modeling of built-up Box-T sections

Thin-Walled Structures ◽

10.1016/j.tws.2020.107336 ◽

2021 ◽

Vol 160 ◽

pp. 107336

Author(s):

Ziqian Zhang ◽

Gang Shi ◽

Xuesen Chen ◽

Lijun Wang ◽

Le Zhou

Keyword(s):

Residual Stress ◽

Stress Measurements

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Comparative study of the effective parameters on residual stress relaxation in welded aluminum plates under cyclic loading

Mechanics & Industry ◽

10.1051/meca/2020061 ◽

2020 ◽

Vol 21 (5) ◽

pp. 505

Author(s):

Yousef Ghaderi Dehkordi ◽

Ali Pourkamali Anaraki ◽

Amir Reza Shahani

Keyword(s):

Residual Stress ◽

Cyclic Loading ◽

Stress Relaxation ◽

Stress Amplitude ◽

Cyclic Plasticity ◽

Mean Stress ◽

Effective Parameters ◽

Perfect Plasticity ◽

Residual Stress Relaxation ◽

Aluminum Plates

The prediction of residual stress relaxation is essential to assess the safety of welded components. This paper aims to study the influence of various effective parameters on residual stress relaxation under cyclic loading. In this regard, a 3D finite element modeling is performed to determine the residual stress in welded aluminum plates. The accuracy of this analysis is verified through experiment. To study the plasticity effect on stress relaxation, two plasticity models are implemented: perfect plasticity and combined isotropic-kinematic hardening. Hence, cyclic plasticity characterization of the material is specified by low cycle fatigue tests. It is found that the perfect plasticity leads to greater stress relaxation. In order to propose an accurate model to compute the residual stress relaxation, the Taguchi L18 array with four 3-level factors and one 6-level is employed. Using statistical analysis, the order of factors based on their effect on stress relaxation is determined as mean stress, stress amplitude, initial residual stress, and number of cycles. In addition, the stress relaxation increases with an increase in mean stress and stress amplitude.

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