Microstructure characterization of a directionally solidified Mg-12wt.%Zn alloy: Equiaxed dendrites, eutectic mixture and type/ morphology of intermetallics

2018 ◽  
Vol 204 ◽  
pp. 105-131 ◽  
Author(s):  
Nathália C. Verissimo ◽  
Crystopher Brito ◽  
Conrado R. Afonso ◽  
José E. Spinelli ◽  
Noé Cheung ◽  
...  
Author(s):  
John A. Sutliff

Near-eutectic Pb-Sn alloys are important solders used by the electronics industry. In these solders, the eutectic mixture, which solidifies last, is the important microstructural consituent. The orientation relation (OR) between the eutectic phases has previously been determined for directionally solidified (DS) eutectic alloys using x-ray diffraction or electron chanelling techniques. In the present investigation the microstructure of a conventionally cast, hyper-eutectic Pb-Sn alloy was examined by transmission electron microscopy (TEM) and the OR between the eutectic phases was determined by electron diffraction. Precipitates of Sn in Pb were also observed and the OR determined. The same OR was found in both the eutectic and precipitation reacted materials. While the precipitation of Sn in Pb was previously shown to occur by a discontinuous precipitation reaction,3 the present work confirms a recent finding that volume diffusion controlled precipitation can also occur.Samples that are representative of the solder's cast microstructure are difficult to prepare for TEM because the alloy is multiphase and the phases are soft.


2000 ◽  
Vol 313 (1-2) ◽  
pp. 154-160 ◽  
Author(s):  
Héctor J. Dorantes-Rosales ◽  
Vı́ctor M. López-Hirata ◽  
José L. Méndez-Velázquez ◽  
Maribel L. Saucedo-Muñoz ◽  
David Hernández-Silva

2009 ◽  
Vol 16 (1) ◽  
pp. 1-10 ◽  
Author(s):  
C. Wilhelm ◽  
G. LaCaille ◽  
N. Wright ◽  
N. Ward ◽  
C. Shu ◽  
...  

2013 ◽  
Vol 542 ◽  
pp. 167-173 ◽  
Author(s):  
Jie He ◽  
Minghui Zhang ◽  
Jiechao Jiang ◽  
Jaroslav Vlček ◽  
Petr Zeman ◽  
...  

2014 ◽  
Vol 289 ◽  
pp. 366-369 ◽  
Author(s):  
Qiang Wang ◽  
Dong Qiu ◽  
Yuming Xiong ◽  
Nick Birbilis ◽  
Ming-Xing Zhang

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