scholarly journals Extension of the probe-tip error evaluation for areal surface roughness measurements using metrological AFM

2021 ◽  
Vol 18 ◽  
pp. 100092
Author(s):  
Ichiko Misumi ◽  
Ryosuke Kizu ◽  
Kentaro Sugawara ◽  
Akiko Hirai ◽  
Satoshi Gonda
Keyword(s):  
Surface Roughness ◽  
Error Evaluation ◽  
Areal Surface ◽  
Roughness Measurements

Surface roughness measurements of vanadium-contaminated fluidized cracking catalysts by atomic force microscopy

1996 ◽  
Vol 54 ◽  
pp. 866-867
Author(s):  
H. Kinney ◽  
M.L. Occelli ◽  
S.A.C. Gould
Keyword(s):  
Surface Roughness ◽  
Zeolite Y ◽  
Atomic Level ◽  
Microporous Structure ◽  
Contact Mode ◽  
Force Microscopy ◽  
Atomic Force ◽  
Before And After ◽  
Roughness Measurements ◽  
Cracking Catalysts

For this study we have used a contact mode atomic force microscope (AFM) to study to topography of fluidized cracking catalysts (FCC), before and after contamination with 5% vanadium. We selected the AFM because of its ability to well characterize the surface roughness of materials down to the atomic level. It is believed that the cracking in the FCCs occurs mainly on the catalysts top 10-15 μm suggesting that the surface corrugation could play a key role in the FCCs microactivity properties. To test this hypothesis, we chose vanadium as a contaminate because this metal is capable of irreversibly destroying the FCC crystallinity as well as it microporous structure. In addition, we wanted to examine the extent to which steaming affects the vanadium contaminated FCC. Using the AFM, we measured the surface roughness of FCCs, before and after contamination and after steaming.We obtained our FCC (GRZ-1) from Davison. The FCC is generated so that it contains and estimated 35% rare earth exchaged zeolite Y, 50% kaolin and 15% binder.

scholarly journals Atomic force microscopy comparative analysis of the surface roughness of two posterior chamber phakic intraocular lens models: ICL versus IPCL

2021 ◽  
Vol 21 (1) ◽  
Author(s):  
Juan Gros-Otero ◽  
Samira Ketabi ◽  
Rafael Cañones-Zafra ◽  
Montserrat Garcia-Gonzalez ◽  
Cesar Villa-Collar ◽  
...  
Keyword(s):  
Surface Roughness ◽  
Atomic Force Microscopy ◽  
Intraocular Lenses ◽  
Posterior Chamber ◽  
Anterior Surface ◽  
Contact Mode ◽  
Force Microscopy ◽  
Atomic Force ◽  
Phakic Intraocular Lenses ◽  
Roughness Measurements

Abstract Background To compare the anterior surface roughness of two commercially available posterior chamber phakic intraocular lenses (IOLs) using atomic force microscopy (AFM). Methods Four phakic IOLs were used for this prospective, experimental study: two Visian ICL EVO+ V5 lenses and two iPCL 2.0 lenses. All of them were brand new, were not previously implanted in humans, were monofocal and had a dioptric power of − 12 diopters (D). The anterior surface roughness was assessed using a JPK NanoWizard II® atomic force microscope in contact mode immersed in liquid. Olympus OMCL-RC800PSA commercial silicon nitride cantilever tips were used. Anterior surface roughness measurements were made in 7 areas of 10 × 10 μm at 512 × 512 point resolution. The roughness was measured using the root-mean-square (RMS) value within the given regions. Results The mean of all anterior surface roughness measurements was 6.09 ± 1.33 nm (nm) in the Visian ICL EVO+ V5 and 3.49 ± 0.41 nm in the iPCL 2.0 (p = 0.001). Conclusion In the current study, we found a statistically significant smoother anterior surface in the iPCL 2.0 phakic intraocular lenses compared with the VISIAN ICL EVO+ V5 lenses when studied with atomic force microscopy.

Testing the Accuracy of Surface Roughness Measurements Carried out with a Portable Profilometer

2015 ◽  
Vol 637 ◽  
pp. 69-73 ◽  
Author(s):  
Krzysztof Stępień
Keyword(s):  
Surface Roughness ◽  
Measurement Accuracy ◽  
Environmental Changes ◽  
Experimental Tests ◽  
Evaluation Procedure ◽  
Human Errors ◽  
Modern Manufacturing ◽  
Machine Parts ◽  
Roughness Measurements

Surface roughness is a factor that has a vital influence on overall quality of machine parts. This is the reason why proper measurements of surface roughness are a matter of great importance in modern manufacturing technology. Nowadays portable profilometers are common instruments to be used under industrial conditions. Measurements with such instruments can be affected by numerous factors, for example environmental changes, human errors of an operator, etc. This paper discusses problem of an evaluation of measurement accuracy of portable profilometers. It also describes the evaluation procedure and presents results experimental tests.

Influence of surface roughness on the wetting angle

1995 ◽  
Vol 10 (8) ◽  
pp. 1984-1992 ◽  
Author(s):  
X.B. Zhou ◽  
J.Th.M. De Hosson
Keyword(s):  
Surface Roughness ◽  
Gaussian Distribution ◽  
Rough Surfaces ◽  
Contact Angles ◽  
Wetting Angle ◽  
Experimental Results ◽  
Solid Surfaces ◽  
Roughness Measurements

A this paper the influence of surface roughness on contact angles in the system of liquid Al wetting solid surfaces of Al2O3 has been studied. It was observed that contact angles of liquid Al vary significantly on different rough surfaces of Al2O3. A model is proposed to correlate contact angles with conventional roughness measurements and wavelengths by assuming a cosine profile of rough grooves with a Gaussian distribution of amplitudes. In comparison with the experimental results, the model provides a good estimate for describing the influence of surface roughness on contact angles of liquid Al on Al2O3.

Determination of Hurst exponent by optical signal processing applied on surface roughness measurements

2009 ◽  
Author(s):  
José Antonio Marbán Salgado ◽  
Oscar Sarmiento Martínez ◽  
Darwin Mayorga Cruz ◽  
Jorge Uruchurtu Chavarín
Keyword(s):  
Surface Roughness ◽  
Signal Processing ◽  
Hurst Exponent ◽  
Optical Signal Processing ◽  
Optical Signal ◽  
Roughness Measurements

scholarly journals Sensitivity of C-Band SAR Polarimetric Variables to the Directionality of Surface Roughness Parameters

2021 ◽  
Vol 13 (11) ◽  
pp. 2210
Author(s):  
Zohreh Alijani ◽  
John Lindsay ◽  
Melanie Chabot ◽  
Tracy Rowlandson ◽  
Aaron Berg
Keyword(s):  
Surface Roughness ◽  
Soil Moisture ◽  
Laser Scanner ◽  
Careful Attention ◽  
Roughness Parameters ◽  
Retrieval Models ◽  
Surface Roughness Parameters ◽  
The Look ◽  
The Relationship ◽  
Roughness Measurements

Surface roughness is an important factor in many soil moisture retrieval models. Therefore, any mischaracterization of surface roughness parameters (root mean square height, RMSH, and correlation length, ʅ) may result in unreliable predictions and soil moisture estimations. In many environments, but particularly in agricultural settings, surface roughness parameters may show different behaviours with respect to the orientation or azimuth. Consequently, the relationship between SAR polarimetric variables and surface roughness parameters may vary depending on measurement orientation. Generally, roughness obtained for many SAR-based studies is estimated using pin profilers that may, or may not, be collected with careful attention to orientation to the satellite look angle. In this study, we characterized surface roughness parameters in multi-azimuth mode using a terrestrial laser scanner (TLS). We characterized the surface roughness parameters in different orientations and then examined the sensitivity between polarimetric variables and surface roughness parameters; further, we compared these results to roughness profiles obtained using traditional pin profilers. The results showed that the polarimetric variables were more sensitive to the surface roughness parameters at higher incidence angles (θ). Moreover, when surface roughness measurements were conducted at the look angle of RADARSAT-2, more significant correlations were observed between polarimetric variables and surface roughness parameters. Our results also indicated that TLS can represent more reliable results than pin profiler in the measurement of the surface roughness parameters.

scholarly journals Preliminary In Vitro Wear Assessment of Ceramic Cemented Femoral Components Coupled with Polyethylene Menisci

Materials ◽  
2021 ◽  
Vol 14 (9) ◽  
pp. 2112
Author(s):  
Saverio Affatato ◽  
Paolo Erani ◽  
Maurizio Fersini ◽  
Vincenzo Contaldi ◽  
Anna Rita Terrizzi ◽  
...  
Keyword(s):  
Surface Roughness ◽  
Wear Resistance ◽  
Monoclinic Phase ◽  
Calf Serum ◽  
Wear Test ◽  
Clinical Test ◽  
Preliminary Evaluation ◽  
Before And After ◽  
Roughness Measurements

Success of total knee replacement (TKR) depends on the prosthetic design and materials. The use of metal components is well established with the disadvantage of allergic reactions. Ceramics have been recently proposed because of high wear resistance, excellent biocompatibility, wettability, and suitable mechanical properties. This study was aimed at investigating in vitro wear resistance of Zirconia Toughened Alumina (ZTA)/Ultra-high-molecular-weight polyethylene (UHMWPE) of TKR femoral components. An in vitro protocol was designed with the application of relevant load profile, 6-degrees-of-freedom knee simulator, and 8 × 105 cycles on the ZTA/UHMWPE configuration under bovine calf serum. Before and after wear test, the femoral components were investigated by using the Scanning Electron Microscope (SEM) and the X-Ray Diffraction (XRD) analyses, and stylus surface roughness measurements. The proposed pre-clinical test yielded repeatable results. In particular, gravimetric results showed that, after 8 × 105 cycles, the mean weight loss of the polyethylene mobile components is 5.3 ± 1.1 mg. The surface roughness measurements (Ramax) performed after the wear test showed no significant variation on the UHMWPE menisci. A slight increase of roughness has been found on the ZTA (0.02 µm before wear test, 0.28 µm after the test). SEM observations did not show significant modification of the surface morphology. Tetragonal to monoclinic phase ratio was measured by XRD before and after wear test to evaluate stability of tetragonal ZrO2 phase. Minimal conversion of tetragonal to monoclinic phase was found from 5.4 to 8%. Although this study is a preliminary evaluation limited to in vitro tests, it provides novel pre-clinical indications about the potential of ceramic TKR femoral components.

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