An improved noninvasive resonance method for water content characterization of Cultural Heritage stone materials

Measurement ◽  
2018 ◽  
Vol 125 ◽  
pp. 257-261 ◽  
Author(s):  
Emanuele Piuzzi ◽  
Erika Pittella ◽  
Stefano Pisa ◽  
Andrea Cataldo ◽  
Egidio De Benedetto ◽  
...  
Keyword(s):  
Cultural Heritage ◽  
Water Content ◽  
Resonance Method ◽  
Stone Materials

Characterization of frozen hydrated biological specimens by low-loss EELS

1992 ◽  
Vol 50 (2) ◽  
pp. 1572-1573
Author(s):  
Songquan Sun ◽  
Richard D. Leapman
Keyword(s):  
Water Content ◽  
Direct Method ◽  
Internal Standard ◽  
Dry Weight ◽  
Dark Field ◽  
Protein Solutions ◽  
Subcellular Compartment ◽  
Differential Shrinkage ◽  
Electron Energy Loss

Analyses of ultrathin cryosections are generally performed after freeze-drying because the presence of water renders the specimens highly susceptible to radiation damage. The water content of a subcellular compartment is an important quantity that must be known, for example, to convert the dry weight concentrations of ions to the physiologically more relevant molar concentrations. Water content can be determined indirectly from dark-field mass measurements provided that there is no differential shrinkage between compartments and that there exists a suitable internal standard. The potential advantage of a more direct method for measuring water has led us to explore the use of electron energy loss spectroscopy (EELS) for characterizing biological specimens in their frozen hydrated state.We have obtained preliminary EELS measurements from pure amorphous ice and from cryosectioned frozen protein solutions. The specimens were cryotransfered into a VG-HB501 field-emission STEM equipped with a 666 Gatan parallel-detection spectrometer and analyzed at approximately −160 C.

KARAKTERISTIK ABON IKAN GABUS (Channa striata) DENGAN SUBTITUSI KLUWIH (Artocarpus camansi)

2018 ◽  
Vol 16 (2) ◽  
pp. 219-226
Author(s):  
Sri Rizqi Annisa ◽  
Dewi Larasati ◽  
Endang Bekti K
Keyword(s):  
Protein Content ◽  
Water Content ◽  
Analysis Of Variance ◽  
Fiber Content ◽  
Substitution Treatment ◽  
Fish Fillet ◽  
Organoleptic Test ◽  
Average Water ◽  
Channa Striata

The aim of this study was to determine the characterization of shredded mureel fish with kluwih substitution on water content, protein content, fiber content and organoleptic (preference for crispness and taste). This study uses a simple Randomized Complete Design (RCD) with the substitution treatment of kluwih and mureel fish, with the following ratio: S1 (240g: 60g), S2 (210g: 90g), S3 (180g: 120g), S4 (150g: 150g), S5 (120g: 180g). Data were analyzed statistically by analysis of variance and if there was a significant effect, further testing was done with BNJ at the level of 5%. The results showed that kluwih substitution in the manufacture of mureel fish shredded had an average: water content of 8.33-10.62%, protein :16.83-22.00%, fiber : 6.79-6.99%, score crispness 2-6.12, taste score 2.6-6.6. Based on the results of the analysis of the variety of kluwih substitutes and mureel fish have a significant effect on water content, protein content and crisp organoleptic test, taste on mureel fish fillet, and no significant effect on fiber content. The best kluwih substitution in S3 treatment with 120 grams of substitute kluwih and 180 grams of mureel fish.

scholarly journals Detection of the TiO2 Concentration in the Protective Coatings for the Cultural Heritage by Means of Hyperspectral Data

2020 ◽  
Vol 13 (1) ◽  
pp. 92
Author(s):  
Antonio Costanzo ◽  
Donatella Ebolese ◽  
Silvestro Antonio Ruffolo ◽  
Sergio Falcone ◽  
Carmelo la Piana ◽  
...  
Keyword(s):  
Titanium Dioxide ◽  
Cultural Heritage ◽  
Urban Areas ◽  
Protective Coatings ◽  
Colloidal Suspensions ◽  
Hyperspectral Data ◽  
Weight Percentage ◽  
Stone Materials ◽  
Test Application ◽  
Nanoparticle Coatings

Nanotechnology-based materials are currently being tested in the protection of cultural heritage: ethyl silicate or silica nanoparticles dispersed in aqueous colloidal suspensions mixed with titanium dioxide are used as a coating for stone materials. These coatings can play a key role against the degradation of stone materials, due to the deposit of organic matter and other contaminants on the substrate, a phenomenon that produces a greater risk for the monuments in urban areas because of the increasing atmospheric pollution. However, during the application phase, it is important to evaluate the amount of titanium dioxide in the coatings on the substrate, as it can produce a coverage effect on the asset. In this work, we present the hyperspectral data obtained through a field spectroradiometer on samples of different stone materials, which have been prepared in laboratory with an increasing weight percentage of titanium dioxide from 0 to 8 wt%. The data showed spectral signatures dependent on the content of titanium dioxide in the wavelength range 350–400 nm. Afterwards, blind tests were performed on other samples in order to evaluate the reliability of these measurements in detecting the unknown weight percentage of titanium dioxide. Moreover, an investigation was also performed on a test application of nanoparticle coatings on a stone statue located in a coastal town in Calabria (southern Italy). The results showed that the surveys can be useful for verifying the phase of application of the coating on cultural heritage structures; however, they could also be used to check the state of the coated stone directly exposed over time to atmospheric, biological and chemical agents.

Laboratory Characterization of a Commercial Capacitance Sensor for Estimating Permittivity and Inferring Soil Water Content

2006 ◽  
Vol 5 (3) ◽  
pp. 1048-1064 ◽  
Author(s):  
Mike Schwank ◽  
Timothy R. Green ◽  
Christian Mätzler ◽  
Hansruedi Benedickter ◽  
Hannes Flühler
Keyword(s):  
Water Content ◽  
Soil Water ◽  
Soil Water Content ◽  
Capacitance Sensor ◽  
Laboratory Characterization

scholarly journals Analysis of urban vulnerability as a tool for cultural heritage preservation. The cases of the medium-sized historical ensembles in Andalusia

2020 ◽  
Vol 17 ◽  
pp. 171-185
Author(s):  
Daniel Navas Carrillo ◽  
Blanca Del Espino Hidalgo ◽  
Juan-Andrés Rodríguez-Lora ◽  
Teresa Pérez-Cano
Keyword(s):  
Cultural Heritage ◽  
Conceptual Framework ◽  
Vulnerability Assessment ◽  
Heritage Preservation ◽  
Sequential Approach ◽  
Intermediate Scale ◽  
Urban Vulnerability ◽  
Complementary Resource ◽  
Cultural Heritage Preservation

This paper presents the urban vulnerability assessment as a complementary resource in heritage preservation policies, through the analysis of the thirty-nine medium-sized cities that have been listed as Historical Ensemble in Andalusia (Spain). The research seeks to make a sequential approach that addresses, from the general –the conceptual framework on urban vulnerability and the characterization of the analysis sample– to the particular  –the analysis of the socio-economic, socio-demographic or residential vulnerability applied to the intermediate scale which has not been in-deep studied yet–. For this, it proposes to adopt the methodology implemented by the Spanish Ministry of Development in the Atlas of Urban Vulnerability, providing a territorial lecture of the results. The study concludes that medium-sized cities do not present a level of vulnerability lower to the largest ones but detecting specific urban weaknesses that should be addressed to improve the response of these cities to heritage preservation.

scholarly journals CARACTERIZAÇÃO FÍSICA DAS SEMENTES DE URUCUM (Bixa orellana L.), VISANDO PROCESSOS DE PÓS-COLHEITA

2019 ◽  
Vol 34 (4) ◽  
pp. 592-600
Author(s):  
Myrella Katlhen Da Cunha de Araujo ◽  
Claudomiro Roberto De Araújo Júnior ◽  
Arlindo Modesto Antunes ◽  
Rodrigo de Jesus Silva ◽  
Magnun Antonio Penariol da Silva
Keyword(s):  
Water Content ◽  
Unit Volume ◽  
Economic Importance ◽  
Angle Of Repose ◽  
Bixa Orellana ◽  
Post Harvest ◽  
Volume Porosity ◽  
Construction Operation ◽  
And Storage

CARACTERIZAÇÃO FÍSICA DAS SEMENTES DE URUCUM (Bixa orellana L.), VISANDO PROCESSOS DE PÓS-COLHEITA   MYRELLA KATLHEN DA CUNHA DE ARAUJO1; CLAUDOMIRO ROBERTO DE ARAUJO JÚNIOR2; ARLINDO MODESTO ANTUNES3; RODRIGO DE JESUS SILVA4 E MAGNUN ANTONIO PENARIOL DA SILVA5   1Acadêmica do curso de Engenharia Agrícola, Universidade Federal Rural da Amazônia – UFRA, (PA 451, Km 03, Bairro Açaizal, 68680-000, Tomé-Açu, Pará, Brasil) e [email protected]. 2 Acadêmico do curso de Engenharia Agrícola, Universidade Federal Rural da Amazônia – UFRA, (PA 451, Km 03, Bairro Açaizal, 68680-000, Tomé-Açu, Pará, Brasil) e [email protected]. 3 Professor Assistente do curso de Engenharia Agrícola, Universidade Federal Rural da Amazônia – UFRA, (PA 451, Km 03, Bairro Açaizal, 68680-000, Tomé-Açu, Pará, Brasil) e [email protected]. 4 Professor Adjunto do curso de Engenharia Agrícola, Universidade Federal Rural da Amazônia – UFRA, (PA 451, Km 03, Bairro Açaizal, 68680-000, Tomé-Açu, Pará, Brasil) e [email protected]. 5 Professor Adjunto do Campus de Engenharia Agrícola, Universidade Federal Rural da Amazônia – UFRA, (PA 451, Km 03, Bairro Açaizal, 68680-000, Tomé-Açu, Pará, Brasil) e [email protected].   RESUMO: O urucum demonstra importância econômica na comercialização dos grãos moídos para produção colorífica e de corantes, no entanto, há poucos estudos sobre suas características físicas em processos pós-colheita. Além disso, o intuito deste trabalho foi comparar o ângulo de repouso das sementes em diferentes protótipos. O estudo foi realizado no laboratório da Universidade Federal Rural da Amazônia, Tomé-Açu (PA), para verificar: teor de água, biometria, esfericidade, volume unitário, porosidade e ângulo de repouso. O teor de água utilizou cinco amostras (50 sementes), biometria obteve eixos ortogonais de 100 sementes, e utilizadas 20 sementes para esfericidade e volume unitário. Ainda, obtidas médias em 3 equipamentos de ângulo de repouso, (5 repetições). Como resultado, o teor de água (b.u.) foi baixo, (0 a 10%); a esfericidade variou de 61,45 a 90,66%; volume unitário foi de 0,03 a 0,13 cm3 e as porosidades foram (0,69, 0,77 e 0,78). Os ângulos de repouso nos equipamentos (A- adaptado em relação a B; B- equipamento estabelecido e C- protótipo alternativo) foram, respectivamente: 38,85; 31,92 e 32,14°, não diferindo estatisticamente. Ademais, o estudo buscou trazer informações sobre a espécie e colaborar com trabalhos de construção, operação e adaptação de equipamentos de secagem e armazenamento.   Palavras-chave: esfericidade, porosidade, volume unitário.   PHYSICAL CHARACTERIZATION OF ANNATTO (Bixa orellana L.) SEEDS, AIMED POST-HARVEST PROCESSES   ABSTRACT: Annatto demonstrates economic importance in the commercialization of ground grains for color and dye production; however, there are few studies on their physical characteristics in post-harvest processes. In addition, the aim of this work was to compare the rest angle of seeds in different prototypes. The study was carried out in the laboratory of Federal Rural University of the Amazon, Tomé-Açu (PA), to verify: water content, biometrics, sphericity, unit volume, porosity and angle of repose. The water content used five samples (50 seeds), biometrics obtained orthogonal axes of 100 seeds, and 20 seeds were used for sphericity and unit volume. Still, averages were obtained in 3 equipment of angle of rest (5 repetitions). As result, the water content (b.u.) was low (0 to 10%); sphericity ranged from 61.45 to 90.66%; unit volume was 0.03 to 0.13 cm3 and porosities were 0.69, 0.77 and 0.78. The rest angles in the equipment (A- adapted in relation to B; B- established equipment and C- alternative prototype) were, respectively: 38.85; 31.92 and 32.14°, not differing statistically. In addition, the study sought to bring information about the species and collaborate with construction, operation and adaptation of drying and storage equipment.   Keywords: sphericity, porosity, unit volume.

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