Instrumental Assessment Of The Formation Of The Elemental Composition Of Wines At The Stage Of Their Clarification With Various Bentonite Clays

2022 ◽  
pp. 107145
Author(s):  
Zaual Temerdashev ◽  
Aleksey Abakumov ◽  
Mikhail Bolshov ◽  
Alexan Khalafyan ◽  
Natalia Ageeva ◽  
...  
Author(s):  
А.Г. АБАКУМОВ ◽  
З.А. ТЕМЕРДАШЕВ ◽  
Н.М. АГЕЕВА

Использование суспензий бентонитовых глин при обработке виноматериалов в процессе их осветления и стабилизации оказывает влияние на минеральный состав вин. Виноматериалы могут обогащаться катионами металлов, оказывающими разнонаправленное влияние на качество и розливостойкость вина. Исследованы изменения элементного состава виноматериалов в результате их обработки 32 образцами бентонитовых глин различных торговых марок. Объектами исследования были образцы виноматериалов из винограда сортов Каберне-Совиньон, Мерло и Молдова, собранного на территории Краснодарского края в 2019 г. Методами ИСП-АЭС и ИСП-МС определен элементный состав виноматериалов до обработки суспензиями бентонитовых глин и после нее. Установлено, что обработка бентонитовыми глинами привела к изменению концентраций практически всех определяемых элементов в образцах виноматериалов. Во всех образцах виноматериалов после обработки снизились концентрации B, Cu, Zn и увеличились концентрации Ag, Al, Cd, Ni, Na, Sb, Sn, Pb, Ti, Fe. As и Hg не были обнаружены ни в исходных, ни в обработанных образцах виноматериалов. Концентрации As, Cd, Hg, Pb, которые регламентируются в Российской Федерации, во всех обработанных образцах виноматериалов были существенно ниже установленного максимального уровня. Концентрации других элементов – Ag, B, Cu, Na, Zn, Ni, нормируемых в документах ЕС и МОВВ, в исследованных обработанных образцах виноматериалов оказались также значительно ниже нормативов. Таким образом, все исследованные бентонитовые глины могут быть рекомендованы к использованию при производстве вин. The use of suspensions of bentonite clays in the processing of wines in order to clarify and stabilize them has a significant effect on the mineral composition of wines. In this case, wines can be enriched with metals cations, which have a different effect on the quality and persistence of wine. Changes in the elemental composition of wine materials as a result of their treatment with 32 samples of bentonite clays of various brands were studied. The objects of the study were samples of wine materials from grapes of the varieties Cabernet Sauvignon, Merlot and Moldova, collected on the territory of the Krasnodar region in 2019. The methods of ICP-NPP and ICP-MS were used to determine the elemental composition of wine materials before and after treatment with bentonite clay suspensions. It was found that the treatment with bentonite clays led to a change in the concentrations of almost all detectable elements in the samples of wine materials. In all samples of wine materials after treatment, the concentrations of B, Cu, Zn decreased and the concentrations of Ag, Al, Cd, Ni, Na, Sb, Sn, Pb, Ti, Fe. As and Hg were not detected in either the initial or treated samples of wine materials. The concentrations of As, Cd, Hg, Pb, which are regulated in the Russian Federation, in all processed samples of wine materials were significantly lower than the established maximum level. The concentrations of other elements – Ag, B, Cu, Na, Zn, Ni, normalized in the EU and the International Organization of Vine and Wine documents, in the studied processed samples of wine materials were also significantly lower than the standards. Thus, all the studied bentonite clays can be recommended for use in the production of wines.


Author(s):  
A. R. Crooker ◽  
M. C. Myers ◽  
T. L. Beard ◽  
E. S. Graham

Cell culture systems have become increasingly popular as a means of screening toxic agents and studying toxic mechanisms of drugs and other chemicals at the cellular and subcellular levels. These in vitro tests can be conducted rapidly in a broad range of relevant mammalian culture systems; a variety of biological and biochemical cytotoxicity endpoints can be examined. The following study utilized human keratinocytes to evaluate the relative cytotoxicities of nitrofurazone (NF) and silver sulfadiazine (SS), the active ingredients of FURACIN(R) Topical Cream and SILVADENE(R) Cream, respectively. These compounds are anti-infectives used in the treatment of burn patients. Cell ultrastructure and elemental composition were utilized as cytotoxicity endpoints.Normal Human Epidermal Keratinocytes (HK) were prepared from the EpiPackTM culture system (Clonetics Corporation, Boulder, CO). For scanning electron microscopy (SEM) and transmission electron microscopy (TEM), cells were seeded on sterile 35 mm Falcon plastic dishes; for elemental microanalysis, cells were plated on polished pyrolytic carbon discs (E. Fullam, Latham, NY) placed in the culture dishes.


Author(s):  
A. J. Tousimis

The elemental composition of amino acids is similar to that of the major structural components of the epithelial cells of the small intestine and other tissues. Therefore, their subcellular localization and concentration measurements are not possible by x-ray microanalysis. Radioactive isotope labeling: I131-tyrosine, Se75-methionine and S35-methionine have been successfully employed in numerous absorption and transport studies. The latter two have been utilized both in vitro and vivo, with similar results in the hamster and human small intestine. Non-radioactive Selenomethionine, since its absorption/transport behavior is assumed to be the same as that of Se75- methionine and S75-methionine could serve as a compound tracer for this amino acid.


2013 ◽  
Vol 23 (2) ◽  
pp. 49-61 ◽  
Author(s):  
Jamie Perry ◽  
Graham Schenck

Despite advances in surgical management, it is estimated that 20–30% of children with repaired cleft palate will continue to have hypernasal speech and require a second surgery to create normal velopharyngeal function (Bricknell, McFadden, & Curran, 2002; Härtel, Karsten, & Gundlach, 1994; McWilliams, 1990). A qualitative perceptual assessment by a speech-language pathologist is considered the most important step of the evaluation for children with resonance disorders (Peterson-Falzone, Hardin-Jones, & Karnell, 2010). Direct and indirect instrumental analyses should be used to confirm or validate the perceptual evaluation of an experienced speech-language pathologist (Paal, Reulbach, Strobel-Schwarthoff, Nkenke, & Schuster, 2005). The purpose of this article is to provide an overview of current instrumental assessment methods used in cleft palate care. Both direct and indirect instrumental procedures will be reviewed with descriptions of the advantages and disadvantages of each. Lastly, new developments for evaluating velopharyngeal structures and function will be provided.


2004 ◽  
Author(s):  
J. Schnackenbeck ◽  
S. Erdal ◽  
T. Schoonover ◽  
L. Conroy

2016 ◽  
Author(s):  
Andreas Roschger ◽  
Paul Roschger ◽  
Felix Repp ◽  
Wolfgang Wagermaier ◽  
Richard Weinkamer ◽  
...  

2020 ◽  
Vol 57 (10) ◽  
pp. 714-742
Author(s):  
V. G. Efremenko ◽  
K. M. Wu ◽  
K. Shimizu ◽  
I. Petryshynets ◽  
B. V. Efremenko ◽  
...  

1992 ◽  
Vol 26 (9-11) ◽  
pp. 2575-2578
Author(s):  
V. Gounaris ◽  
P. R. Anderson ◽  
T. M. Holsen

Colloidal material in landfill leachate were separated and fractionated in size fractions. Analyses were performed to obtain the mass, elemental composition, and pollutants associated with the colloids in each fractions. The stabilization mechanism of the colloids is studied to evaluate their mobility potential.


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