Effect of high current pulsed electron beam surface irradiation on the microstructure and electrochemical behavior of zircaloy-4

Author(s):  
Shen Yang ◽  
Zuoxing Guo ◽  
Min Zhang ◽  
Qingfeng Guan ◽  
Yunxue Jin ◽  
...  
2021 ◽  
Vol 11 (10) ◽  
pp. 4372
Author(s):  
Sergey G. Anikeev ◽  
Anastasiia V. Shabalina ◽  
Sergei A. Kulinich ◽  
Nadezhda V. Artyukhova ◽  
Daria R. Korsakova ◽  
...  

A new approach to fabricate TiNi surfaces combining the advantages of both monolithic and porous materials for implants is used in this work. New materials were obtained by depositing a porous TiNi powder onto monolithic TiNi plates followed by sintering at 1200 °C. Then, further modification of the material surface with a high-current-pulsed electron beam (HCPEB) was carried out. Three materials obtained (one after sintering and two after subsequent beam treatment by 30 pulses with different pulse energy) were studied by XRD, SEM, EDX, surface profilometry, and by means of electrochemical measurements, including OCP and EIS. Structural and compositional changes caused by HCPEB treatment were investigated. Surface properties of the samples during their storage in saline for 10 days were studied and a model experiment with cell growth (MCF-7) was carried out for the unmodified sample with an electron beam to detect cell appearance on different surface locations.


Author(s):  
Sergey G. Anikeev ◽  
Anastasiia V. Shabalina ◽  
Sergei A. Kulinich ◽  
Nadezhda V. Artyukhova ◽  
Darya R. Korsakova ◽  
...  

A new approach to fabricate TiNi surfaces combining the advantages of both monolithic and porous materials for implants is used in this work. New materials were obtained by depositing a porous TiNi powder onto monolithic TiNi plates followed by sintering at 1200°C. Then, further modification of the material surface with a high-current-pulsed electron beam (HCPEB) was carried out. Three materials obtained (one after sintering and two after subsequent beam treatment by 20 and 30 pulses, respectively) were studied by XRD, SEM, EDX, EIS methods, profilometry and OCP measurements. Structural and compositional changes caused by HCPEB treatment were investigated. Surface properties of the samples during their storage in saline for 10 days were studied and a model experiment with cell growth (MCF-7) was carried out for the sample unmodified with electron beam to detect cell appearance on different surface locations.


2016 ◽  
Author(s):  
Yuri Ivanov ◽  
Oleg Tolkachev ◽  
Maria Petyukevich ◽  
Anton Teresov ◽  
Olga Ivanova ◽  
...  

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