Study impact of sample treatment and insitu fluids on shale wettability measurement using NMR

2019 ◽  
Vol 176 ◽  
pp. 352-361 ◽  
Author(s):  
Ishank Gupta ◽  
Chandra Rai ◽  
Carl Sondergeld
Keyword(s):  
Sample Treatment ◽  
Wettability Measurement

INFLUENCE OF RAPID QUENCHING AND SAMPLE TREATMENT ON THE STRUCTURE OF MELT SPUN Al-Si ALLOYS

1985 ◽  
Vol 46 (C8) ◽  
pp. C8-533-C8-537
Author(s):  
J. Chevrier ◽  
P. Sainfort ◽  
P. Germi ◽  
D. Pavuna
Keyword(s):  
Rapid Quenching ◽  
Sample Treatment ◽  
Melt Spun

Improving Mycobacterium spp. detection in water: a new methodological proposal

2004 ◽  
Vol 4 (2) ◽  
pp. 103-106
Author(s):  
R. Santos ◽  
S. Gonçalves ◽  
F. Macieira ◽  
F. Oliveira ◽  
R. Rodrigues ◽  
...  
Keyword(s):  
Water Samples ◽  
Recovery Rate ◽  
Opportunistic Infections ◽  
Environmental Water ◽  
Environmental Water Samples ◽  
Sample Treatment ◽  
Detection Time ◽  
Fast Detection ◽  
Enrichment Step ◽  
Mycobacterium Spp

In recent years, non-tuberculous mycobacteria (NTM), once considered merely environmental saprophytes, have emerged as a major cause of opportunistic infections. There is no evidence of human-to-human transmission but they have been found in several environmental water samples. It is, therefore, of the utmost importance to develop methods of rapidly and accurately detecting non-tuberculous mycobacteria in water samples. To obtain a maximum recovery rate and a reduction of Mycobacterium spp. detection time in water samples, different decontamination, enrichment procedures and antibiotics supplements were tested before the inoculation into the Bactec® system. The proposed method of sample treatment (decrease in the decontamination time, followed for a peptone pre-enrichment step and an aztreonam and cefepime supplement) before the inoculation into the Bactec® system proved to be a good option for reliable and fast detection of Mycobacterium spp. in water samples.

scholarly journals Fast and Sensitive Determination of the Fungicide Carbendazim in Fruit Juices with an Immunosensor Based on White Light Reflectance Spectroscopy

Biosensors ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 153
Author(s):  
Georgios Koukouvinos ◽  
Chrysoula-Evangelia Karachaliou ◽  
Ioannis Raptis ◽  
Panagiota Petrou ◽  
Evangelia Livaniou ◽  
...  
Keyword(s):  
White Light ◽  
Optical Biosensor ◽  
Reflectance Spectroscopy ◽  
Fruit Juices ◽  
Sample Treatment ◽  
Assay Sensitivity ◽  
Reliable Determination ◽  
Light Reflectance ◽  
Sensitive Determination

Carbendazim is a systemic benzimidazole-type fungicide with broad-spectrum activity against fungi that undermine food products safety and quality. Despite its effectiveness, carbendazim constitutes a major environmental pollutant, being hazardous to both humans and animals. Therefore, fast and reliable determination of carbendazim levels in water, soil, and food samples is of high importance for both food industry and public health. Herein, an optical biosensor based on white light reflectance spectroscopy (WLRS) for fast and sensitive determination of carbendazim in fruit juices is presented. The transducer is a Si/SiO2 chip functionalized with a benzimidazole conjugate, and determination is based on a competitive immunoassay format. Thus, for the assay, a mixture of an in-house developed rabbit polyclonal anti-carbendazim antibody with the standards or samples is pumped over the chip, followed by biotinylated secondary antibody and streptavidin. The WLRS platform allows for real-time monitoring of biomolecular interactions carried out onto the Si/SiO2 chip by transforming the shift in the reflected interference spectrum caused by the immunoreaction to effective biomolecular adlayer thickness. The sensor is able to detect 20 ng/mL of carbendazim in fruit juices with high accuracy and precision (intra- and inter-assay CVs ≤ 6.9% and ≤9.4%, respectively) in less than 30 min, applying a simple sample treatment that alleviates any “matrix-effect” on the assay results and a 60 min preincubation step for improving assay sensitivity. Excellent analytical characteristics and short analysis time along with its small size render the proposed WLRS immunosensor ideal for future on-the-spot determination of carbendazim in food and environmental samples.

Fully automated sample treatment method for high throughput proteome analysis

2020 ◽  
Author(s):  
Huiming Yuan ◽  
Zhongpeng Dai ◽  
Xiaodan Zhang ◽  
Baofeng Zhao ◽  
Hongwei Chu ◽  
...  
Keyword(s):  
High Throughput ◽  
Proteome Analysis ◽  
Treatment Method ◽  
Sample Treatment

scholarly journals Synthesis of Polymer-Based Magnetic Nanocomposite for Multi-Pollutants Removal from Water

Polymers ◽  
2021 ◽  
Vol 13 (11) ◽  
pp. 1742
Author(s):  
Fatimah Mohammed Alzahrani ◽  
Norah Salem Alsaiari ◽  
Khadijah Mohammedsaleh Katubi ◽  
Abdelfattah Amari ◽  
Faouzi Ben Rebah ◽  
...  
Keyword(s):  
Adsorption Process ◽  
Magnetic Composite ◽  
Sample Treatment ◽  
Water Type ◽  
X Ray Diffraction ◽  
Solution Ph ◽  
Vibration Sample Magnetometer ◽  
Pollutants Removal ◽  
Co Precipitation ◽  
Red Dye

A magnetic polymer-based nanocomposite was fabricated by the modification of an Fe3O4/SiO2 magnetic composite with polypyrrole (PPy) via co-precipitation polymerization to form PPy/Fe3O4/SiO2 for the removal of Congo red dye (CR) and hexavalent chromium Cr(VI) ions from water. The nanocomposite was characterized using various techniques including X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscope (SEM), vibration sample magnetometer, and thermogravimetric analysis (TGA). The results confirm the successful fabrication of the nanocomposite in the size of nanometers. The effect of different conditions such as the contact time, adsorbent dosage, solution pH, and initial concentration on the adsorption process was investigated. The adsorption isotherm suggested monolayer adsorption of both contaminants over the PPy/Fe3O4/SiO2 nanocomposite following a Langmuir isotherm, with maximum adsorption of 361 and 298 mg.g−1 for CR dye and Cr(VI), respectively. Furthermore, the effect of water type on the adsorption process was examined, indicating the applicability of the PPy/Fe3O4/SiO2 nanocomposite for real sample treatment. Interestingly, the reusability of the nanocomposite for the removal of the studied contaminants was investigated with good results even after six successive cycles. All results make this nanocomposite a promising material for water treatment.

scholarly journals Determination of Oxalate and Some Inorganic Anions in Green and Black Tea

2013 ◽  
Vol 67 (4-5) ◽  
pp. 429-432 ◽  
Author(s):  
Elena Yusenko ◽  
Evgeniya Polyntseva ◽  
Anna Lyzhova ◽  
Olga Kalyakina
Keyword(s):  
Oxalic Acid ◽  
Green Tea ◽  
Ion Chromatography ◽  
Black Tea ◽  
Inorganic Anions ◽  
Sample Treatment ◽  
Oxalate Concentration ◽  
Relative Standard ◽  
Oxalate Ions

Abstract Oxalate concentration differs in various daily consumed food products. The role of oxalic acid in the human body is very significant, as its compounds are responsible for the stability of biological membranes. However, insoluble calcium and magnesium oxalates can be accumulated in the body in the form of kidney stones. Oxalate concentration has been measured by high performance liquid, gas after derivatization and ion chromatography (IC). The most effective method for the simultaneous determination of oxalate and inorganic anions is ion chromatography with conductometric detection. Here, we report the results of the measurement of oxalic acid in bleak and green tea samples. Separation was performed by IC on an anion-exchange column Shodex IC SI-90 with surface-layer sorbent and conductimetric detection. The main analytical features of the method were: limit of detection of oxalic acid 0.03 mg/l, linear range 0.1-20 mg/l, correlation 0.9998, relative standard deviation 1%. The method did not need specific sample treatment and was successfully applied to the analysis of black and green tea samples. Oxalic acid was determined in the ranges 16.7-84 mg/l for green tea and 63-116 mg/l for black tea. Green tea contained lower oxalate ions concentration than black tea. The IC method has a lower detection limit for oxalate ions than HPLS and GC, ten and two times less, respectively

scholarly journals Mycotoxin Analysis: New Proposals for Sample Treatment

2014 ◽  
Vol 2014 ◽  
pp. 1-12 ◽  
Author(s):  
Natalia Arroyo-Manzanares ◽  
José F. Huertas-Pérez ◽  
Ana M. García-Campaña ◽  
Laura Gámiz-Gracia
Keyword(s):  
Raw Materials ◽  
Animal Health ◽  
Analytical Techniques ◽  
Sample Treatment ◽  
Analytical Technique ◽  
Chemical Structures ◽  
Technical Developments ◽  
Food And Feed ◽  
Ultrahigh Performance Liquid Chromatography ◽  
Food Commodities

Mycotoxins are toxic secondary metabolites produced by different fungi, with different chemical structures. Mycotoxins contaminate food, feed, or raw materials used in their production and cause diseases and disorders in humans and livestock. Because of their great variety of toxic effects and their extreme heat resistance, the presence of mycotoxins in food and feed is considered a high risk to human and animal health. In order to ensure food quality and health consumers, European legislation has set maximum contents of some mycotoxins in different matrices. However, there are still some food commodities susceptible to fungal contamination, which were not contemplated in this legislation. In this context, we have developed new analytical techniques for the multiclass determination of mycotoxins in a great variety of food commodities (some of them scarcely studied), such as cereals, pseudocereals, cereal syrups, nuts, edible seeds, and botanicals. Considering the latest technical developments, ultrahigh performance liquid chromatography coupled to tandem mass spectrometry has been chosen as an efficient, fast, and selective powerful analytical technique. In addition, alternative sample treatments based on emerging methodologies, such as dispersive liquid-liquid microextraction and QuEChERS, have been developed, which allow an increased efficiency and sample throughput, as well as reducing contaminant waste.

Integrated set-up of sampling, sample treatment and assay of an intracellular protein during fermentation

2010 ◽  
Vol 150 (3) ◽  
pp. 366-371 ◽  
Author(s):  
Mohammadali Mazlomi ◽  
Martin Hedström ◽  
Bo Mattiasson
Keyword(s):  
Sample Treatment ◽  
Intracellular Protein ◽  
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