scholarly journals Measurement of average particle size in metal powders by microwave cavity perturbation in the magnetic field

2017 ◽  
Vol 259 ◽  
pp. 137-143 ◽  
Author(s):  
N. Clark ◽  
N. Jones ◽  
A. Porch
2019 ◽  
Vol 135 ◽  
pp. 02019
Author(s):  
Yuriy Vernigorov ◽  
Valeriy Lebedev ◽  
Natalya Frolova ◽  
Kirill Leletko

The design features of the grinding devices that implement the impact destruction of the ferromagnetic materials particles in a magneto vibrating layer formed in a non-uniform magnetic field are considered. It is shown that when a magnetizable powder is affected by an alternating magnetic field with certain parameters, a magneto vibrating layer is formed, under the conditions of which, a random perturbing factor occurs. It is caused by the dipole particles clusters interactions and provides highefficient finish powder grinding. Methods for producing metal powders, which are distinguished according to the operating principle and to the requirements for the technological properties of the powders obtained, are analyzed. For coarse grinding, jaw, roller and cone crushers and mullers are used; at this, particles of 1-10 mm in size, which are the source material for fine grinding, are obtained. The finish grinding of the material obtained is carried out on the ball rotating, vibrating or planar centrifugal, vortex and hammer mills. The main drawback of these techniques of metal powder grinding is sticking of grinding body residue on the powder particles, which reduces the quality and operational properties of the powder. A relation to calculate the dependence of the fineness number of ferromagnetic materials on the induction gradient of an external variable magnetic field is proposed. The design features of an electromagnetic mill based on a screw drum that, due to the spatial orientation of its walls, ensures an effective movement of powder flows inside it, such as mixing, rotation, oncoming movement, translational motion and simultaneous advancement through the drum are presented. The concept and technological options of grinding powders in an electromagnetic mobile hammer mill are revealed, which enables to obtain a powder of a given particle size distribution with high uniformity. It is established that mills in which a magneto vibrating layer is implemented are more effective than mechanical ones: grinding of ferromagnetic powders in a magneto vibrating layer increases drastically the performance of the grinding process. Changing the parameters of the electromagnetic field, you can set an average particle size and the degree of homogeneity of the powder.


Author(s):  
Hakan Gokmese

Abstract: A large area cross section of the production of spherical metal powders by gas atomization in the manufacturing method. Powder metal characteristic improves with small powder size. This aim was realized by vertical gas atomization unit, a new a closely-matched nozzle system and manufacture. In the experimental studies, pure aluminium powders which has an important place in the automotive, air and defence industries were produced. In the studies carried out with the Vertical Gas Atomization unit, aluminium was superheated up to 900°C and atomized at different gas pressures (20-30 bar). Scanning electron microscope (SEM) and particle size measuring device were used for the characterization and size measurements of the produced powders, respectively. The average particle size of the finest powder produced with increasing atomization pressure was determined as d50=19.50µm. Aluminium powder shape and morphology was used as spherical and very little satellization was seen. Keywords: Powder Metallurgy, Atomisation, Nozzle, Al powder, Characterisation


2005 ◽  
Vol 277-279 ◽  
pp. 1044-1048 ◽  
Author(s):  
Eun Hee Kim ◽  
Hyo Sook Lee ◽  
Hui Ping Shao

Nanostructured iron and cobalt ferrite particles were prepared from iron chloride and cobalt chloride, respectively, using the sonochemical method. The particles were compared with those synthesized using the co-precipitation method. The properties of the particles were characterized using various techniques, such as XRD, TEM, VSM and a SQUID magnetometer. The iron ferrite particles had an average particle size of about 15 nm and a magnetization value of 83 emu/g at a magnetic field of 50 kOe, while the particle size of cobalt ferrite was about 5 nm and its magnetization value was 33 emu/g at the same magnetic field.


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