A closed inline system for sample digestion using 70% hydrogen peroxide and UV radiation. Determination of lead in wine employing ETAAS

Talanta ◽  
2019 ◽  
Vol 191 ◽  
pp. 479-484 ◽  
Author(s):  
Raineldes A. Cruz Junior ◽  
Adriano V.B. Chagas ◽  
Caio S.A. Felix ◽  
Rosemario C. Souza ◽  
Luciana A. Silva ◽  
...  
2019 ◽  
Vol 146 ◽  
pp. 1204-1208 ◽  
Author(s):  
Caio S.A. Felix ◽  
Daniel L.F. da Silva ◽  
Adriano V.B. Chagas ◽  
Matheus B. de Melo ◽  
Raineldes A. Cruz Junior ◽  
...  

2016 ◽  
Vol 12 (2) ◽  
pp. 102-107 ◽  
Author(s):  
Walter N.L. dos Santos ◽  
Dannuza D. Cavalcante ◽  
Paula D.N. Gomes ◽  
Daniele C.M.B. Santos ◽  
Luciana B. Oliveira ◽  
...  

1983 ◽  
Vol 29 (8) ◽  
pp. 1513-1517 ◽  
Author(s):  
M W McGowan ◽  
J D Artiss ◽  
B Zak

Abstract A procedure for the enzymatic determination of lecithin and sphingomyelin in aqueous solution is described. The phospholipids are first dissolved in chloroform:methanol (2:1 by vol), the solvent is evaporated, and the residue is redissolved in an aqueous zwitterionic detergent solution. The enzymatic reaction sequences of both assays involve hydrolysis of the phospholipids to produce choline, which is then oxidized to betaine, thus generating hydrogen peroxide. The hydrogen peroxide is subsequently utilized in the enzymatic coupling of 4-aminoantipyrine and sodium 2-hydroxy-3,5-dichlorobenzenesulfonate, an intensely red color being formed. The presence of a non-reacting phospholipid enhances the hydrolysis of the reacting phospholipid. Thus we added lecithin to the sphingomyelin standards and sphingomyelin to the lecithin standards. This precise procedure may be applicable to determination of lecithin and sphingomyelin in amniotic fluid.


1982 ◽  
Vol 102 (12) ◽  
pp. 1120-1123 ◽  
Author(s):  
HIROYUKI IWAI ◽  
SUMIYUKI AKIHAMA

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