Influence of lamination on the flexural strength of a dental castable glass ceramic

1996 ◽  
Vol 76 (1) ◽  
pp. 23-28 ◽  
Author(s):  
Sharifa A Al-Shehri ◽  
Hamdi Mohammed ◽  
Clive A Wilson
2019 ◽  
Vol 44 (2) ◽  
pp. 200-209 ◽  
Author(s):  
F Murillo-Gómez ◽  
RB Wanderley ◽  
MF De Goes

SUMMARY The aim of this study was to determine whether using a silane-containing universal adhesive as a silane primer in glass-ceramic/resin cement systems affects biaxial flexural strength (BFS) and bonded interface integrity after loading. Glass-ceramic (IPS e.max CAD, Ivoclar/Vivadent, Schaan, Liechtenstein) disc-shaped specimens (6.5±0.1mm in diameter, 0.5±0.1mm thick) were etched with 5% hydrofluoric acid (HF) for 20 seconds and divided into four groups of 30 specimens, to be treated as follows: 1) One bottle silane primer (RCP); 2) Separate application of silane and adhesive (RCP+SB); 3) Silane-containing universal adhesive (SBU); 4) No treatment (C). After silanization, all specimens were resin cement– coated and polymerized for 40 seconds. Each specimen layer was measured, as well as each assembly's thickness, using a digital caliper and scanning electron microscope (SEM). Specimens were stored for 24 hours and submitted to a BFS test (1.27 mm/min). BFS values were calculated using the bilayer disc-specimen solution. Bonded interfaces were analyzed on fractured fragments using SEM. One-way ANOVA and Tukey tests (α=0.05) were applied, as well as the Weibull analysis. Factor “silane treatment” was statistically significant (p<0.0001). RCP+SB (372.2±29.4 MPa) and RCP (364.2±29.5 MPa) produced significantly higher BFS than did the C (320.7±36.3 MPa) or SBU (338.0±27.1 MPa) groups. No differences were found in the Weibull modulus (m: RCP: 10.1-17.3; RCP+SB: 10.1-17.0; SBU: 12.3-22.4; C: 7.4-12.9). Bonded interface analysis exhibited ceramic-cement separation (SBU, C) and voids within the resin cement layer (all groups). Neither the ceramic/cement system's BFS nor its bonded interface stability were improved by SBU after loading.


2016 ◽  
Vol 32 ◽  
pp. e15-e16
Author(s):  
F. Murillo-Gómez ◽  
R.B.W. Lima ◽  
M.F. De Goes

Cerâmica ◽  
2016 ◽  
Vol 62 (362) ◽  
pp. 121-127 ◽  
Author(s):  
P. P. Kist ◽  
I. L. Aurélio ◽  
M. Amaral ◽  
L. G. May

Abstract The purpose of the present study was to determine the biaxial flexural strength (BFS) of a CAD/CAM leucite reinforced glass-ceramic ground by diamond burs of different grit sizes and the influence of surface roughness on the BFS. For this, 104 plates were obtained from CAD/CAM ceramic blocks and divided into 4 groups (n = 26), according to bur grit size: extra-fine, fine, medium and coarse. Roughness parameters (Ra, RyMax) were measured, and plates were kept dry for 7 days. The flexural test was carried out and BFS was calculated. Ra, RyMax and BFS data were subjected to analysis of variance and post-hoc test. Weibull analysis was used to compare characteristic strength and Weibull modulus. Regression analysis was performed for BFS vs. Ra and RyMax. When burs with coarse grit were used, higher surface roughness values were found, causing a negative effect on the ceramic BFS (117 MPa for extra-fine, and 83 MPa for coarse). Correlation (r) between surface roughness and BFS was 0.78 for RyMax and 0.73 for Ra. Increases in diamond grit size have a significant negative effect on the BFS of leucite-reinforced glass-ceramics, suggesting that grinding of sintered glass-ceramic should be performed using burs with the finest grit possible in order to minimize internal surface flaws and maximize flexural strength.


2019 ◽  
Vol 821 ◽  
pp. 435-439
Author(s):  
Bo Li ◽  
Ke Jing ◽  
Hai Bo Bian

Low temperature sintered MgO-Al2O3-SiO2 glass-ceramic with high mechanical and low thermal expansion was prepared for package. The remarkable influence of B2O3 addition on the electrical, mechanical, and thermal properties was fully investigated. A small amount of B2O3 promoted the sintering process and improved the densification of MAS. The kinetics via Kissinger method indicated that an appropriate B2O3 content decreased the activation energy and helped the occurrence of crystallization. Due to the increase of crystallinity and indialite phase, B2O3 addition significantly enhanced flexural strength and Young’s modulus. MAS doped with 3wt% B2O3 can be sintered at 900 °C and obtained good properties: σ = 229 MPa, φ = 86 GPa, α = 1.66×10-6 /°C, εr = 5.29, and tanδ = 5.9×10-4.


2011 ◽  
Vol 20 (7) ◽  
pp. 553-560 ◽  
Author(s):  
Luis Gustavo Oliveira de Vasconcellos ◽  
Lucas H. Silva ◽  
Luana Marotta Reis de Vasconcellos ◽  
Ivan Balducci ◽  
Fernando E. Takahashi ◽  
...  

Author(s):  
J.Y. Hsu ◽  
Y. Berta ◽  
R.F. Speyer

SiC fiber reinforced lithia-alumina-silica glass-ceramic composites have exhibited superior mechanical properties at room and elevated temperatures. The flexural strength of these composites is 3 to 4 times larger than that of monolithic glass-ceramics. The high flexural strength of these composites is due to the transfer of the applied load from the matrix to the stronger and stiffer SiC fiber reinforcement. These composites also have demonstrated very high fracture toughness, KIC (critical stress intersity factor) values of ∼ 17 MPa m1/2, which is attributed to an amorphous carbon-rich interfacial layer between the fiber and matrix. Nb2O2 has been added to the matrix composition in order to develop a NbC layer outside the amorphous C-rich layer after thermal processing, thereby buffering the fiber/matrix reactivity (avoid carbon forming CO gas which would deteriorate the matrix).


2001 ◽  
Vol 17 (1) ◽  
pp. 21-33 ◽  
Author(s):  
M.J. Cattell ◽  
T.C. Chadwick ◽  
J.C. Knowles ◽  
R.L. Clarke ◽  
E. Lynch

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