Characterization of crystal system of BaPb1−xBixO3 with X-ray diffraction for synchrotron radiation

This article presents the progress on characterization of the interfacial interaction between sulfur oxidizing microbes and sulfide minerals by using of synchrotron radiation-based techniques including S/Fe/Cu X-ray absorption near-edge structure spectroscopy (XANES), X-ray Diffraction (XRD), micro-X-ray fluorescence (μ-XRF) mapping and micro-scanning transmission X-ray microscopy (μ-STXM) imaging, together with other accessory approaches such as SEM/EDS, Raman spectroscopy, FT-IR spectroscopy, and electrochemical methods as well as comparative proteomics methodology.

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Synthesis and Structural Characterization of N,N´- Dipropyl-N,N,N´,N´-tetramethyl-1,2- ethylenediammonium Dichloride and Dibromide

Zeitschrift für Naturforschung B ◽

10.1515/znb-2011-0720 ◽

2011 ◽

Vol 66 (7) ◽

pp. 755-758

Author(s):

Sari M. Närhi ◽

Janne Asikkala ◽

Jatta Kostamo ◽

Marja K. Lajunen ◽

Raija Oilunkaniemi ◽

...

Keyword(s):

Hydrogen Bonding ◽

Water Molecules ◽

Monoclinic Crystal System ◽

X Ray Diffraction ◽

Monoclinic Crystal ◽

Triclinic Crystal System ◽

Space Group ◽

X Ray ◽

Crystal System

N,N´-Dipropyl-N,N,N´ ,N´-tetramethyl-1,2-ethylenediammonium dichloride (1) and dibromide (2) were prepared by the reaction of N,N,N´,N´-tetramethyl-1,2-ethylenediamine and the corresponding 1-halopropane. The structures of the compounds were characterized by single-crystal X-ray diffraction. 1 · 2H2O crystallizes in the triclinic crystal system, space group P1, with Z = 1, and 2 in the monoclinic crystal system, space group P21/c, with Z = 2. The crystal structures of the salts consist of discrete dications and halide anions. The packing in 1 · 2H2O consists of layers of cations with the chloride anions and water molecules forming hydrogen-bonded chains between the cation layers. In 2, the strongest H· · ·Br hydrogen bonds of 2.8138(6) and 2.8187(7) °A link the cations and anions into doublestranded chains. In both salts, cations and anions are also linked together by a further weak C-H· · ·Cl/Br hydrogen bonding network.

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Structural Characterization of Nickel(II) Tetraphenylporphyrin

Australian Journal of Chemistry ◽

10.1071/ch9961273 ◽

1996 ◽

Vol 49 (12) ◽

pp. 1273 ◽

Cited By ~ 32

Author(s):

AL Maclean ◽

GJ Foran ◽

BJ Kennedy ◽

P Turner ◽

TW Hambley

Keyword(s):

Synchrotron Radiation ◽

Single Crystal ◽

Bond Length ◽

Diffraction Pattern ◽

Structural Characterization ◽

X Ray Diffraction ◽

X Ray ◽

Bond Lengths ◽

Single Crystal Analysis

The structure of 5,10,15,20-tetraphenylporphinatonickel(II) ([Ni( tpp )]) has been studied by both X-ray diffraction (powder and single-crystal methods) and EXAFS. The bond lengths obtained from analysis of the EXAFS agree, within standard deviations, with those obtained from the X-ray diffraction studies. The Ni-N bond length of 1.93(1) Ǻ agrees especially well with the value of 1.931(2) Ǻ obtained from the single-crystal analysis. The powder X-ray diffraction pattern, collected by using synchrotron radiation, is presented.

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In situ synchrotron radiation grazing incidence X-ray diffraction—A powerful technique for the characterization of solid-state ion-selective electrode surfaces

Electrochimica Acta ◽

10.1016/j.electacta.2006.01.034 ◽

2006 ◽

Vol 51 (23) ◽

pp. 4886-4891 ◽

Cited By ~ 11

Author(s):

Roland De Marco ◽

Zhong-Tao Jiang ◽

Bobby Pejcic ◽

Arie van Riessen

Keyword(s):

Solid State ◽

Synchrotron Radiation ◽

Grazing Incidence ◽

X Ray Diffraction ◽

Selective Electrode ◽

X Ray ◽

Powerful Technique ◽

Electrode Surfaces

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Synthesis and Characterization of La2Ca2Cu2O7 Compound

Modern Physics Letters B ◽

10.1142/s0217984998001153 ◽

1998 ◽

Vol 12 (23) ◽

pp. 991-993

Author(s):

L. K. Kaliyaperumal ◽

J. Srinivas ◽

K. Jeyabalan

Keyword(s):

Diffraction Analysis ◽

Ambient Pressure ◽

Lattice Parameters ◽

Synthesis And Characterization ◽

Orthorhombic Crystal System ◽

X Ray Diffraction ◽

Orthorhombic Crystal ◽

X Ray ◽

Crystal System

Synthesis and characterization of La 2 Ca 2 Cu 2 O 7 compound at ambient pressure is reported here. The powder X-ray diffraction analysis shows that the compound crystallizes in an orthorhombic crystal system with lattice parameters a = 5.770(4) Å, b = 5.887(7) Å and c = 27.37(2) Å.

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