Gas—liquid chromatography of isobutyl ester, N(O)-heptafluorobutyrate derivatives of amino acids on a glass capillary column for quantitative separation in clinical biology

Author(s):  
Jean Desgres ◽  
Dominique Boisson ◽  
Prudent Padieu
1982 ◽  
Vol 28 (6) ◽  
pp. 1283-1286 ◽  
Author(s):  
S Yoshioka ◽  
S Saitoh ◽  
T Fujisawa ◽  
A Fujimori ◽  
O Takatani ◽  
...  

Abstract 1-Deoxyglucose (1,5-anhydroglucitol), a metabolite related to diabetes mellitus, was identified in human plasma by gas-liquid chromatography and by gas-liquid chromatography/mass spectrometry. Plasma polyols were accurately determined with a gas-liquid chromatograph equipped with an all-glass capillary column. The plasma content of 1-deoxyglucose in healthy persons varies with age. Although the precise physiological role of 1-deoxyglucose remains obscure, the method described here for determining the minor polyol components of plasma, as well as the findings of 1-deoxyglucose in the plasma of healthy subjects, may be useful for investigating the metabolic roles of 1-deoxyglucose.


1967 ◽  
Vol 20 (2) ◽  
pp. 275-281 ◽  
Author(s):  
Martha A. Ward ◽  
Timothy E. McCarthy ◽  
Jonathan S. Nishimura

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