Analyzing the Effect of Capillary Force on Vibrational Performance of the Cantilever of an Atomic Force Microscope in Tapping Mode with Double Piezoelectric Layers in an Air Environment

2015 ◽  
Vol 21 (5) ◽  
pp. 1195-1206 ◽  
Author(s):  
Amir Nahavandi ◽  
Moharam Habibnejad Korayem

AbstractThe aim of this paper is to determine the effects of forces exerted on the cantilever probe tip of an atomic force microscope (AFM). These forces vary according to the separation distance between the probe tip and the surface of the sample being examined. Hence, at a distance away from the surface (farther than don), these forces have an attractive nature and are of Van der Waals type, and when the probe tip is situated in the range of a0≤dts≤don, the capillary force is added to the Van der Waals force. At a distance of dts≤a0, the Van der Waals and capillary forces remain constant at intermolecular distances, and the contact repulsive force repels the probe tip from the surface of sample. The capillary force emerges due to the contact of thin water films with a thickness of hc which have accumulated on the sample and probe. Under environmental conditions a layer of water or hydrocarbon often forms between the probe tip and sample. The capillary meniscus can grow until the rate of evaporation equals the rate of condensation. For each of the above forces, different models are presented. The smoothness or roughness of the surfaces and the geometry of the cantilever tip have a significant effect on the modeling of forces applied on the probe tip. Van der Waals and the repulsive forces are considered to be the same in all the simulations, and only the capillary force is altered in order to evaluate the role of this force in the AFM-based modeling. Therefore, in view of the remarkable advantages of the piezoelectric microcantilever and also the extensive applications of the tapping mode, we investigate vibrational motion of the piezoelectric microcantilever in the tapping mode. The cantilever mentioned is entirely covered by two piezoelectric layers that carry out both the actuation of the probe tip and the measuringof its position.

1997 ◽  
Vol 5 (10) ◽  
pp. 6-6 ◽  
Author(s):  
Stefan Zauscher

Atomic Force Microscopes (AFM) can measure the force between a surface and the tip of a cantilever as a junction of separation with great precision. For example, van der Waals type forces and electrostatic repulsive forces can easily be measured in aqueous solutions using an AFM. The complex, pyramidal shape of the typical AFM cantilever is, however, not well suited for quantitative measurements. It is thus desirable to attach particles of known geometry (usually spheres) to the tip of a cantilever.


2019 ◽  
Vol 86 (s1) ◽  
pp. 12-16
Author(s):  
Janik Schaude ◽  
Julius Albrecht ◽  
Ute Klöpzig ◽  
Andreas C. Gröschl ◽  
Tino Hausotte

AbstractThis article presents a new tilting atomic force microscope (AFM) with an adjustable probe direction and piezoresistive cantilever operated in tapping-mode. The AFM is based on two rotational axes, which enable the adjustment of the probe direction to cover a complete hemisphere. The whole setup is integrated into a nano measuring machine (NMM-1) and the metrological traceability of the piezoresistive cantilever is warranted by in situ calibration on the NMM-1. To demonstrate the capabilities of the tilting AFM, measurements were conducted on a step height standard.


2013 ◽  
Vol 209 ◽  
pp. 137-142
Author(s):  
Abrarkhan M. Pathan ◽  
Dhawal H. Agrawal ◽  
Pina M. Bhatt ◽  
Hitarthi H. Patel ◽  
U.S. Joshi

With the rapid advancements in the field of nanoscience and nanotechnology, scanning probe microscopy has become an integral part of a typical R&D lab. Atomic force microscope (AFM) has become a familiar name in this category. The AFM measures the forces acting between a fine tip and a sample. The tip is attached to the free end of a cantilever and is brought very close to a surface. Attractive or repulsive forces resulting from interactions between the tip and the surface will cause a positive or negative bending of the cantilever. The bending is detected by means of a laser beam, which is reflected from the backside of the cantilever. Atomic force microscopy is currently applied to various environments (air, liquid, vacuum) and types of materials such as metal semiconductors, soft biological samples, conductive and non-conductive materials. With this technique size measurements or even manipulations of nano-objects may be performed. An experimental setup has been designed and built such that a commercially available Atomic Force Microscope (AFM) (Nanosurf AG, Easyscan 2) can be operated at cryogenic temperature under vacuum and in a vibration-free environment. The design also takes care of portability and flexibility of AFM i.e. it is very small, light weight and AFM can be used in both ambient and cryogenic conditions. The whole set up was assembled in-house at a fairly low cost. It is used to study the surface structure of nanomaterials. Important perovskite manganite Pr0.7Ca0.3MnO3thin films were studied and results such as morphology, RMS area and line roughness as well as the particle size have been estimated at cryogenic temperature.


2013 ◽  
Vol 378 ◽  
pp. 466-471
Author(s):  
Po Jen Shih ◽  
Shang Hao Cai

The dynamic behaviors of carbon nanotube probes applied in Atomic Force Microscope measurement are of interest in advanced nanoscalar topography. In this paper, we developed the characteristic equations and applied the model analysis to solve the eigenvalues of the microcantilever and the carbon nanotube. The eigenvalues were then used in the tapping mode system to predict the frequency responses against the tip-sample separations. It was found that the frequency drop steeply if the separation was less than certain distances. This instability of frequency is deduced from the jump of microcantilever or the jump of the carbon nanotube. Various lengths and binding angles of the carbon nanotube were considered, and the results indicated that the binding angle dominated the frequency responses and jumps.


2008 ◽  
Vol 74 (742) ◽  
pp. 1409-1415
Author(s):  
Masatoshi NUMATSU ◽  
Andrew J. DICK ◽  
Hiroshi YABUNO ◽  
Masaharu KURODA ◽  
Balakumar BALACHANDRAN

2014 ◽  
Vol 25 (6) ◽  
pp. 732-740 ◽  
Author(s):  
Kleber dos Santos Rodrigues ◽  
José Manoel Balthazar ◽  
Angelo Marcelo Tusset ◽  
Bento Rodrigues de Pontes ◽  
Átila Madureira Bueno

Author(s):  
Kleber dos Santos Rodrigues ◽  
José Manoel Balthazar ◽  
Angelo Marcelo Tusset ◽  
Bento Rodrigues de Pontes Junior

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