Determination of Active Ingredients and Total Fatty Matter in Sulfonated and Sulfated Oils

1935 ◽  
Vol 7 (3) ◽  
pp. 137-140 ◽  
Author(s):  
Ralph Hart
Keyword(s):  
Fatty Matter ◽  
Active Ingredients ◽  
Total Fatty Matter

A Simple Rapid Method for Direct Determination of Total Fatty Matter in Soaps

1977 ◽  
Vol 79 (7) ◽  
pp. 285-288 ◽  
Author(s):  
M. K. Kundu ◽  
A. T. Deb ◽  
S. P. Gupta
Keyword(s):  
Rapid Method ◽  
Direct Determination ◽  
Fatty Matter ◽  
Total Fatty Matter

RP-HPLC in determination of seven active ingredients in blood-invigorating and stasis-removing prescription

2013 ◽  
Vol 33 (10) ◽  
pp. 1125-1129 ◽  
Author(s):  
Lin CHEN ◽  
Xin-xin ZHANG ◽  
Xuan DANG ◽  
Tian-long ZHANG ◽  
Zhen-zhi LI ◽  
...  
Keyword(s):  
Active Ingredients ◽  
Rp Hplc

scholarly journals Characterization and stability study of some pharmaceutical ointments

2012 ◽  
Vol 23 (1) ◽  
pp. 87-91
Author(s):  
Viorica Popescu ◽  
Alina Soceanu ◽  
Simona Dobrinas ◽  
Gabriela Stanciu
Keyword(s):  
Stability Study ◽  
Fatty Matter ◽  
Volatile Substances ◽  
Ph Values ◽  
Acidity Index ◽  
Anti Inflammatory ◽  
Type Water ◽  
Total Fatty Matter ◽  
Antibiotic Ointment

Abstract In the present study we have determined some characteristics (aspect, odor, solubility, emulsion type, water and volatile substances content, total fatty matter, saponification index, ester index) for three pharmaceutical ointments belonging to the group of non-steroidal anti-inflammatory: Diclac, Ketonal, Indometacin and one antibiotic ointment for ophthalmic use: Ophtagram. In order to achieve stability study of studied ointments, the pH, the acidity index, the peroxide index and the iodine index were determined over a year every three months. After 9 months from the opening of the tubes, analytical determinations have shown that pH values, acidity, peroxide and iodine indexes no longer fit to the values recommended for medical use, which confirms the directions available on the package.

Simultaneous determination of the active ingredients in composite pseudoephedrine hydrochloride tablets by capillary electrophoresis

2000 ◽  
Vol 424 (2) ◽  
pp. 257-262 ◽  
Author(s):  
Lan Zhang ◽  
Qin Hu ◽  
Guonan Chen ◽  
Yuzhi Fang
Keyword(s):  
Capillary Electrophoresis ◽  
Simultaneous Determination ◽  
Active Ingredients

scholarly journals Simultaneous Determination of Three Active Ingredients in Schisandra chinensis (Turcz.) Baill by HPLC

2014 ◽  
Vol 26 (8) ◽  
pp. 2434-2436
Author(s):  
Weiming Cheng ◽  
Jie Gao ◽  
Shan Zhong
Keyword(s):  
Simultaneous Determination ◽  
Schisandra Chinensis ◽  
Active Ingredients

scholarly journals Laundry Soap Production from the Respective Tallows of Goat, Sheep and Cow: Evaluation of Physicochemical Properties for the Best

2021 ◽  
pp. 22-33
Author(s):  
Abdullahi Nwaha Isah ◽  
Umi Aisah Asli ◽  
Nasiru Audu ◽  
Sadiku Itopa Bello ◽  
Jibrin Waziri ◽  
...  
Keyword(s):  
Moisture Content ◽  
Physicochemical Properties ◽  
Foam Height ◽  
Acid Value ◽  
Deep Penetration ◽  
Free Acidity ◽  
Fatty Matter ◽  
National Agency ◽  
Laundry Soap ◽  
Total Fatty Matter

Tallow mainly consists of triglycerides, whose major constituents are derived from stearic, palmitic and oleic acids, and its usage reduces production cost of soap, adds lather stability and hardness to soap. Laundry soaps were produced with variation on amount of tallow (sourced from cow, sheep and goat) and labelled as A, B, C, D and E formulations. The respective tallows were characterized in terms of saponification value and acid value and determined to be 192.14 and 2.24mg KOH/g (cow tallow); 200.56 and 2.38mgKOH/g (sheep tallow) and 197.75 and 1.96 mgKOH/g (goat tallow). The physicochemical properties of soap which determine its area of usage and cleansing properties were determined. The properties considered in this work were hardness, moisture content, foam capacity, pH, free acidity content, and total fatty matter. The hardness, moisture content, foam capacity, pH, free acidity content and total fatty matter of the produced soaps were determined and ranged between mild-deep penetration level; 11-21%; 1-9cm; 8-10.5; 0.16-0.82% and 40-86% respectively. From the comparative analysis, soap made from sheep tallow has the lowest penetration level (with formulations B and E), lowest free acidity content of 0.16% (with formulation A), highest total fatty matter of 86% (using formulation E), highest foam height of 9cm (with formulation A), lowest moisture content of 11% (with formulation A) and mild alkalinity of 8 (with formulations A, B and E). These results showed that the soaps produced from sheep tallow are the best in terms of hardness, lather and skin friendliness, due to its high degree of longer carbon chain lengths of fatty acids. These values satisfy the standard limit set for good quality laundry soap by National Agency for Food and Drug Administration and Control and Encyclopaedia of Industrial Chemical Analysis, respectively.

scholarly journals Development and Validation of Chemometrics-Assisted Spectrophotometry and Liquid Chromatography Methods for the Simultaneous Determination of the Active Ingredients in Two Multicomponent Mixtures Containing Chlorpheniramine Maleate and Phenylpropanolamine Hydrochloride

2007 ◽  
Vol 90 (4) ◽  
pp. 957-970 ◽  
Author(s):  
Ghada M Hadad ◽  
Alaa El-Gindy ◽  
Waleed M M Mahmoud
Keyword(s):  
Liquid Chromatography ◽  
Simultaneous Determination ◽  
Analytical Sensitivity ◽  
Multicomponent Mixtures ◽  
Active Ingredients ◽  
Chlorpheniramine Maleate ◽  
Calibration Methods ◽  
Limit Of Quantitation ◽  
Phenylpropanolamine Hydrochloride

Abstract Multivariate spectrophotometric calibration and liquid chromatography (LC) methods were used for the simultaneous determination of the active ingredients in 2 multicomponent mixtures containing chlorpheniramine maleate and phenylpropanolamine hydrochloride with ibuprofen and caffeine (mixture 1) or with propyphenazone (mixture 2). For the multivariate spectrophotometric calibration methods, principal component regression (PCR) and partial least squares (PLS-1), a calibration set of the mixtures consisting of the components of each mixture was prepared in distilled water. A leave-1-out cross-validation procedure was used to find the optimum numbers of latent variables. Analytical parameters such as sensitivity, selectivity, analytical sensitivity, limit of quantitation, and limit of detection were determined for both PLS-1 and PCR. The LC method depends on the use of a cyanopropyl column with the mobile phase acetonitrile-12 mM ammonium acetate, pH 5.0 (25 + 75, v/v), for mixture 1 or acetonitrile10 mM potassium dihydrogen phosphate, pH 4.7 (45 + 55, v/v), for mixture 2; the UV detector was set at 212 nm. In spite of the presence of a high degree of spectral overlap of these components, they were rapidly and simultaneously determined with high accuracy and precision, with no interference from the matrix excipients. The proposed methods were successfully applied to the analysis of pharmaceutical formulations and laboratory-prepared mixtures containing the 2 multicomponent combinations.

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