Characterization of Vinyl Polymer/Silica Colloidal Nanocomposites Using Solid State NMR Spectroscopy:  Probing the Interaction between the Inorganic and Organic Phases on the Molecular Level

2003 ◽  
Vol 107 (45) ◽  
pp. 12497-12502 ◽  
Author(s):  
Gyan K. Agarwal ◽  
Jeremy J. Titman ◽  
Matthew J. Percy ◽  
Steven P. Armes
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Molecular Level ◽  
Solid State Nmr Spectroscopy ◽  
Vinyl Polymer ◽  
Inorganic And Organic

Molecular-level characterization of probucol nanocrystal in water by in situ solid-state NMR spectroscopy

2012 ◽  
Vol 423 (2) ◽  
pp. 571-576 ◽  
Author(s):  
Junying Zhang ◽  
Kenjirou Higashi ◽  
Waree Limwikrant ◽  
Kunikazu Moribe ◽  
Keiji Yamamoto
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Molecular Level ◽  
Solid State Nmr Spectroscopy

scholarly journals Use of Solid-State NMR Spectroscopy for the Characterization of Molecular Structure and Dynamics in Solid Polymer and Hybrid Electrolytes

Polymers ◽  
2021 ◽  
Vol 13 (8) ◽  
pp. 1207
Author(s):  
Gabrielle Foran ◽  
Nina Verdier ◽  
David Lepage ◽  
Cédric Malveau ◽  
Nicolas Dupré ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Pulse Sequence ◽  
Dynamic Properties ◽  
Double Resonance ◽  
Solid Polymer ◽  
Pulse Field ◽  
Solid State Nmr Spectroscopy

Solid-state NMR spectroscopy is an established experimental technique which is used for the characterization of structural and dynamic properties of materials in their native state. Many types of solid-state NMR experiments have been used to characterize both lithium-based and sodium-based solid polymer and polymer–ceramic hybrid electrolyte materials. This review describes several solid-state NMR experiments that are commonly employed in the analysis of these systems: pulse field gradient NMR, electrophoretic NMR, variable temperature T1 relaxation, T2 relaxation and linewidth analysis, exchange spectroscopy, cross polarization, Rotational Echo Double Resonance, and isotope enrichment. In this review, each technique is introduced with a short description of the pulse sequence, and examples of experiments that have been performed in real solid-state polymer and/or hybrid electrolyte systems are provided. The results and conclusions of these experiments are discussed to inform readers of the strengths and weaknesses of each technique when applied to polymer and hybrid electrolyte systems. It is anticipated that this review may be used to aid in the selection of solid-state NMR experiments for the analysis of these systems.

scholarly journals Synthesis, characterization and modeling of self-assembled porphyrin nanorods

2019 ◽  
Vol 23 (11n12) ◽  
pp. 1346-1354 ◽  
Author(s):  
Danielle Laurencin ◽  
Pascal G. Yot ◽  
Christel Gervais ◽  
Yannick Guari ◽  
Sébastien Clément ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Dft Calculations ◽  
Powder Diffraction ◽  
Solid State Nmr ◽  
Molecular Level ◽  
Ion Association ◽  
Free Base ◽  
X Ray ◽  
Solid State Nmr Spectroscopy

Porphyrin nanorods were prepared by ion-association between free-base meso 5,10,15,20-tetrakis-(4-[Formula: see text]-methylpyridinium)porphyrin cations and tetraphenylborate anions. The nanorods have variable lengths (up to a few micrometers long) and diameters ([Formula: see text]50–500 nm). Their structure at the molecular level was elucidated by combining multinuclear solid state NMR spectroscopy, synchrotron X-ray powder diffraction and DFT calculations.

Rapid Characterization of Formulated Pharmaceuticals Using Fast MAS 1H Solid-State NMR Spectroscopy

2019 ◽  
Vol 16 (7) ◽  
pp. 3121-3132 ◽  
Author(s):  
David A. Hirsh ◽  
Anuradha V. Wijesekara ◽  
Scott L. Carnahan ◽  
Ivan Hung ◽  
Joseph W. Lubach ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Solid State Nmr Spectroscopy ◽  
Fast Mas ◽  
Rapid Characterization

High-Resolution Solid-State NMR Spectroscopy: Characterization of Polymorphism in Cimetidine, a Pharmaceutical Compound

2014 ◽  
Vol 91 (8) ◽  
pp. 1236-1239 ◽  
Author(s):  
Julia E. Pacilio ◽  
John T. Tokarski ◽  
Rosalynn Quiñones ◽  
Robbie J. Iuliucci
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Solid State Nmr ◽  
Solid State Nmr Spectroscopy ◽  
Pharmaceutical Compound

ChemInform Abstract: Contribution of Solid State NMR Spectroscopy to the Characterization of Materials

ChemInform ◽  
1990 ◽  
Vol 21 (41) ◽  
Author(s):  
A. P. LEGRAND ◽  
H. HOMMEL ◽  
H. TAIBI ◽  
J. L. MIQUEL ◽  
P. TOUGNE
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Solid State Nmr Spectroscopy ◽  
Characterization Of Materials
Sign in / Sign up

Export Citation Format

Share Document