Electrothermal atomic absorption spectrometric determination of cadmium and lead in environmental, botanic and biological samples by different permanent modifiersElectronic supplementary information (ESI) available: Temperature program for modifier coating; optimization of mass and mass ratio of permanent modifiers and cadmium peak profiles; pyrolysis temperatures; characteristic masses and detection limits of cadmium and lead; and contents and recoveries of cadmium and lead in various reference materials. See http://www.rsc.org/suppdata/ja/b3/b315881k/

2004 ◽  
Vol 19 (5) ◽  
pp. 709 ◽  
Author(s):  
Orhan Acar
1982 ◽  
Vol 65 (3) ◽  
pp. 647-650 ◽  
Author(s):  
Gerard K H Tam ◽  
Gladys Lacroix

Abstract A dry ashing, flameless atomic absorption spectrometric method was evaluated to determine arsenic and selenium in foods. Samples were dry-ashed with Mg(N03)2-MgO and dissolved in HC1. Selenate was reduced to selenite by boiling in 4N HC1, and arsenate to arsenite by treatment with KI. Hydrides of arsenic and selenium were generated by the addition of NaBH4 and were swept by nitrogen and hydrogen into a thermally heated silicate tube furnace. The detection limit was about 5 ppb for each element based on a 10 g sample. Analytical results obtained for several samples of NBS reference materials agreed with the certified values. The procedure was evaluated by another laboratory and results were satisfactory.


1999 ◽  
Vol 54 (5) ◽  
pp. 805-818 ◽  
Author(s):  
Marcela Burguera ◽  
José Luis Burguera ◽  
Carlos Rondón ◽  
Marı́a Luisa di Bernardo ◽  
Máximo Gallignani ◽  
...  

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