Facile microwave assisted synthesis of vastly edge exposed 1T/2H-MoS2 with enhanced activity for hydrogen evolution catalysis

2019 ◽  
Vol 7 (8) ◽  
pp. 3563-3569 ◽  
Author(s):  
Young Bum Lee ◽  
Seong K. Kim ◽  
Seulgi Ji ◽  
Wooseok Song ◽  
Hee-Suk Chung ◽  
...  

One-step microwave-assisted solvothermal synthesis of a 1T–2H MoS2 heterostructure with excellent stability and electrocatalytic performance of 1T-MoS2 as a hydrogen evolution catalyst.

2015 ◽  
Vol 51 (20) ◽  
pp. 4252-4255 ◽  
Author(s):  
Bo You ◽  
Nan Jiang ◽  
Meili Sheng ◽  
Yujie Sun

Hollow cobalt sulfide nanoprisms obtained by a two-step, microwave-assisted synthesis within 15 min exhibit higher hydrogen evolution catalytic activity and better specific capacitance than its counterpart prepared by a traditional solvothermal method.


2021 ◽  
Vol 46 (69) ◽  
pp. 34264-34275
Author(s):  
Guilherme B. Strapasson ◽  
Marcelo Assis ◽  
Cláudio W. Backes ◽  
Silma A. Corrêa ◽  
Elson Longo ◽  
...  

2015 ◽  
Vol 670 ◽  
pp. 177-182
Author(s):  
Alexey A. Sadovnikov ◽  
Alexander E. Baranchikov ◽  
Vladimir Kozik ◽  
Lyudmila P. Borilo ◽  
Sergey A. Kozyukhin ◽  
...  

Microwave-assisted high temperature hydrolysis of titanium oxysulfate, in the presence of ammonium fluoride, allows synthesizing nanocrystalline titanium dioxide photocatalysts possessing photocatalytic activity as high as the commercial photocatalyst Evonik Aeroxide® TiO2 P 25. Dye-sensitized reactions play an important role in organic dye discoloration in the presence of fluorinated titania.


2020 ◽  
Vol 115 ◽  
pp. 272-278
Author(s):  
Xiaobo Hu ◽  
Pingping Song ◽  
Xiaolong Yang ◽  
Cheng Wang ◽  
Jianlong Wang ◽  
...  

2019 ◽  
Vol 6 (6) ◽  
pp. 190196 ◽  
Author(s):  
Kai Cheng ◽  
Jie-pin Hu ◽  
Yan-cheng Wu ◽  
Chu-qi Shi ◽  
Zhi-geng Chen ◽  
...  

A novel aromatic diamine containing pyridyl side group, 4-pyridine-4,4-bis(3,5-dimethyl-5-aminophenyl)methane (PyDPM), was successfully synthesized via electrophilic substitution reaction. The polyimides (PIs) containing pyridine were obtained via the microwave-assisted one-step polycondensation of the PyDPM with pyromellitic dianhydride (PMDA), 3,3′,4,4′-biphenyltetracarboxylic dianhydride (BPDA), 3,3′,4,4′-diphenylether tetracarboxylic dianhydride (ODPA) and 4,4′-(hexafluoroisopropylidene)diphthalic anhydride (6FDA). Contrarily to the reported similar PIs, these PIs exhibit much higher thermal stability or heat resistance, i.e. high glass transition temperatures ( T g s) in the range of 358–473°C, and the decomposition temperatures at 5% weight loss over 476°C under nitrogen. They can afford flexible and strong films with tensile strength of 82.1–93.3 MPa, elongation at break of 3.7%–15.2%, and Young's modulus of 3.3–3.8 GPa. Furthermore, The PI films exhibit good optical transparency with the cut-off wavelength at 313–366 nm and transmittance higher than 73% at 450 nm. The excellent thermal and optical transmittance can be attributed to synthesis method and the introduction of pyridine rings and ortho-methyl groups. The inherent viscosities of PIs via one-step method were found to be 0.58–1.12 dl g −1 in DMAc, much higher than those via two-step method. These results indicate these PIs could be potential candidates for optical substrates of organic light emitting diodes (OLEDs).


2016 ◽  
Vol 6 (23) ◽  
pp. 8257-8267 ◽  
Author(s):  
Francisco Gonell ◽  
David Portehault ◽  
Beatriz Julián-López ◽  
Karine Vallé ◽  
Clément Sanchez ◽  
...  

One-step microwave synthesis allows one to tune WOx species and ZrO2 polymorphs showing different activities in acid reactions.


2019 ◽  
Vol 54 (9) ◽  
pp. 6930-6942 ◽  
Author(s):  
Yanqi Xu ◽  
Cui Du ◽  
Jay D. Steinkruger ◽  
Chen Zhou ◽  
Shengyang Yang

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