scholarly journals In situ synchrotron pair distribution function analysis to monitor synthetic pathways under electromagnetic excitation

2020 ◽  
Vol 8 (31) ◽  
pp. 15909-15918 ◽  
Author(s):  
Nathan Nakamura ◽  
Laisuo Su ◽  
Jianming Bai ◽  
Sanjit Ghose ◽  
B. Reeja-Jayan

In situ pair distribution function analysis reveals that electromagnetic radiation exposure during SnO2 nanoparticle growth alters local atomic structure and the synthetic pathway compared to conventional hydrothermal synthesis routes.

2018 ◽  
Vol 20 (13) ◽  
pp. 8593-8606 ◽  
Author(s):  
Kengran Yang ◽  
V. Ongun Özçelik ◽  
Nishant Garg ◽  
Kai Gong ◽  
Claire E. White

Drying-induced nanoscopic alterations to the local atomic structure of silicate-activated slag and the mitigated effects of nano-ZrO2 are elucidated using in situ X-ray pair distribution function analysis.


2021 ◽  
Vol 56 (9) ◽  
pp. 5637-5657
Author(s):  
Emily T. Nienhuis ◽  
Manzila Tuheen ◽  
Jincheng Du ◽  
John S. McCloy

2020 ◽  
Vol 2 (6) ◽  
pp. 2234-2254 ◽  
Author(s):  
Troels Lindahl Christiansen ◽  
Susan R. Cooper ◽  
Kirsten M. Ø. Jensen

We review the use of pair distribution function analysis for characterization of atomic structure in nanomaterials.


2020 ◽  
Vol 22 (34) ◽  
pp. 18860-18867 ◽  
Author(s):  
Matthew E. Potter ◽  
Mark E. Light ◽  
Daniel J. M. Irving ◽  
Alice E. Oakley ◽  
Stephanie Chapman ◽  
...  

Novel in situ synchrotron total scattering measurements probe the assembly of primary building units into templated hierarchically porous aluminophosphate catalysts, providing unique insights to understanding crystallisation kinetics.


2017 ◽  
Vol 5 (35) ◽  
pp. 18434-18441 ◽  
Author(s):  
Nathan Nakamura ◽  
Maxwell W. Terban ◽  
Simon J. L. Billinge ◽  
B. Reeja-Jayan

The effect of electromagnetic fields on nanoscale atomic structure was determined using synchrotron X-ray pair distribution function (PDF) analysis.


2015 ◽  
Vol 3 (16) ◽  
pp. 8597-8605 ◽  
Author(s):  
Antoine E. Morandeau ◽  
Claire E. White

The kinetics of reaction and the local atomic structure of carbonating C–S–H gel are characterised using high-energy synchrotron radiation.


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