On the use of a 2D-carbon microfiber fractionation system to improve flow-injection QTOF-HRMS analysis in complex matrices: the case of Abelmoschus manihot flower extracts

The Analyst ◽  
2022 ◽  
Author(s):  
Chol-San Jon ◽  
Lei Yang ◽  
Zhao Wang ◽  
Meiyu Cui ◽  
Huaze Sun ◽  
...  

A two-dimensional microscale carbon fiber/active carbon fiber system combined with a quadrupole time of flight high-resolution mass spectrometer (2DCFs-QTOF-HRMS) system is proposed to rapidly putative identify polar, medium polar and...

The Analyst ◽  
2021 ◽  
Author(s):  
Harald Schoeny ◽  
Evelyn Rampler ◽  
Yasin El Abiead ◽  
Felina Hildebrand ◽  
Olivia Zach ◽  
...  

We propose a fully automated novel workflow for lipidomics based on flow injection- followed by liquid chromatography high resolution mass spectrometry (FI/LC-HRMS). The workflow combined in-depth characterization of the lipidome...


2015 ◽  
Vol 10 (11) ◽  
pp. 1934578X1501001 ◽  
Author(s):  
Mousa AlTarabeen ◽  
Georgios Daletos ◽  
Weaam Ebrahim ◽  
Werner E. G. Müller ◽  
Rudolf Hartmann ◽  
...  

Chemical investigation of the MeOH extract of the sponge Acanthostrongylophora ingens afforded the new manzamine derivative ircinal E (1), in addition to six known metabolites (2–7). The structure of the new compound was unequivocally elucidated using one- and two-dimensional NMR spectroscopy, as well as high-resolution mass spectrometry. Compounds 1–6 exhibited strong to moderate cytotoxicity against the murine lymphoma L5178Y cell line with IC50 values ranging from 2.8 to 21.7 μM.


Nature ◽  
1994 ◽  
Vol 370 (6488) ◽  
pp. 393-395 ◽  
Author(s):  
Yunzhi Li ◽  
Richard L. Hunter ◽  
Robert T. Mclver

Talanta ◽  
2018 ◽  
Vol 190 ◽  
pp. 363-374 ◽  
Author(s):  
Samuel Kaiser ◽  
Jailson C. Dias ◽  
Jorge A. Ardila ◽  
Frederico L.F. Soares ◽  
Marcelo C.A. Marcelo ◽  
...  

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