Characterization of crystalline quality of diamond films by Raman spectroscopy

1989 ◽  
Vol 55 (25) ◽  
pp. 2608-2610 ◽  
Author(s):  
M. Yoshikawa ◽  
G. Katagiri ◽  
H. Ishida ◽  
A. Ishitani ◽  
M. Ono ◽  
...  
1994 ◽  
Vol 9 (11) ◽  
pp. 2839-2844 ◽  
Author(s):  
G. Popovici ◽  
S. Khasawinah ◽  
T. Sung ◽  
M.A. Prelas ◽  
B.V. Spitsyn ◽  
...  

The crystalline quality of a diamond film with two different preferential orientations (100) and (111), obtained in the same run by hot filament chemical deposition, has been studied. The quality of the film determined by Raman spectroscopy measurements was found to be nearly the same for both orientations. The second order Raman spectrum for diamond film was observed by using an infrared excitation.


1989 ◽  
Vol 162 ◽  
Author(s):  
Y. M. LeGrice ◽  
E. C. Buehler ◽  
R. J. Nemanich ◽  
J. T. Glass ◽  
K. Kobashi ◽  
...  

ABSTRACTCVD diamond films prepared under varying conditions have been investigated with IR and Raman spectroscopy. Raman spectroscopy was used to characterize the crystal structure, and ir absorption was used to determine the H bonding environments. The growth temperatures were varied in one series, while the CH4/H2 ratio was varied in another. The IR absorption of all the samples showed a weak broad band extending from approximately 2800 to 2970 cm−1 which was attributed to H bonded to sp3 C sites. There was no evidence of ir absorption at 3000 to 3200 cm−1 which would indicate H bonded to sp2 or sp1 C sites. For both series, the Raman measurements showed progression from diamond-like films to diamond films. The ir absorption showed a general trend of less H with more well ordered diamond structures. No sharp transition of the H incorporation vs the growth parameters was observed.


Author(s):  
S. Intarasiri ◽  
A. Hallén ◽  
T. Kamwanna ◽  
L.D. Yu ◽  
G. Possnert ◽  
...  

2004 ◽  
Vol 851 ◽  
Author(s):  
Eduardo B. Barros ◽  
Nasser S. Demir ◽  
Antonio G. Souza Filho ◽  
Josué Medes Filho ◽  
Ado Jorio ◽  
...  

ABSTRACTTo better understand the very high thermal conductivity to weight ratio of the graphitic foams recently developed at the Oak Ridge National Laboratory, a Raman spectroscopy study was performed. It was also shown that the Raman scattering can be useful for the characterization of the graphitic foam, being able to evaluate the quality of the samples with respect to the density and location of lattice defects.


2001 ◽  
Vol 674 ◽  
Author(s):  
R. A. Lukaszew ◽  
V. Stoica ◽  
R. Clarke

ABSTRACTOne interesting application of epitaxial magnetic thin films is to use them as one of the electrodes in a spin-dependent tunneling junction, in order to use the magnetocrystalline anisotropy to define the required two states of the magnetization. [1] In our preliminary work, we prepared epitaxial magnetic films on copper buffer layers grown on silicon substrates. [2] The single crystalline quality of the films was particularly evident in the magnetization hysteresis loops, showing a sharp reversal at fairly high fields (120 Oe), when the samples were magnetized along the crystallographic easy axis. One technological disadvantage in this type of samples is the chemical interaction between the metallic layers and the silicon substrate.In order to explore the possibility of epitaxial magnetic films on less reactive substrates, we studied the growth on MgO substrates. We have shown that it is possible to obtain epitaxial (001) and (111) Ni films grown on MgO substrates. [3] In particular we observed that the crystalline quality of the films improved considerably after 10 nm of film growth. We will now present our studies on the magnetic properties of these films, particularly the azimuthal dependence of the magnetization reversal using MOKRE, correlating our finding with the structural characterization obtained with RHEED, STM and XRD.


2019 ◽  
Vol 34 (01n03) ◽  
pp. 2040024
Author(s):  
Lin Yu ◽  
Yuan-Yuan Xu ◽  
Jing Zhao ◽  
Jin Xiao ◽  
Wei-Long Xu

Titanium dioxide ([Formula: see text]) is a kind of wide bandgap transparent metal oxide semiconductor and has shown great potential applications in photocatalysis, gas sensors and biomedical fields due to its superior properties, such as nontoxic, high photocatalytic efficiency and physicochemical stability. In this work, one-dimensional [Formula: see text] nanostructure was successfully synthesized by hydrothermal method. The morphology and crystalline quality of [Formula: see text] were characterized by scanning electron microscope (SEM) and X-ray diffraction (XRD), respectively. The results demonstrate that the structure of [Formula: see text] evolved from “flower-like” structure to nanowire with the acid concentration increment. The sintering temperature has an important effect on the structure and crystalline quality of [Formula: see text]. The crystalline quality of [Formula: see text] nanobelt was improved with the annealing temperature increment. When the sintering temperature increased to 1000[Formula: see text]C, the phase of [Formula: see text] would transfer from anatase to rutile.


Sign in / Sign up

Export Citation Format

Share Document