Thermal degradation of calcium lactate pentahydrate using TGA/FTIR/MS: thermal kinetic and thermodynamics studies

2021 ◽  
pp. 1-14
Author(s):  
Sevgi Polat
1981 ◽  
Vol 42 (C1) ◽  
pp. C1-301-C1-307
Author(s):  
I. T. Ritchie ◽  
J. Spitz
Keyword(s):  

Author(s):  
Sh.M. Rakhimbayev ◽  
◽  
T.V. Anikanova ◽  
I.M. Kolesnikov ◽  
◽  
...  

2016 ◽  
Vol 38 (4) ◽  
pp. 302-306
Author(s):  
V.V. Boyko ◽  
◽  
O.A. Radchenko ◽  
S.V. Riabov ◽  
S.I. Sinelnikov ◽  
...  

2009 ◽  
Author(s):  
Yuan Kim ◽  
Edward M. Steadham ◽  
Steven M. Lonergan ◽  
Elisabeth J. Huff-Lonergan

2013 ◽  
Vol 56 (4) ◽  
pp. 133-135
Author(s):  
Yuki IKEDA ◽  
Satoru IWAMORI ◽  
Hiroyuki MATSUMOTO ◽  
Kiyoshi YOSHINO ◽  
Itsuo NISHIYAMA ◽  
...  

Author(s):  
P. Singh ◽  
G.T. Galyon ◽  
J. Obrzut ◽  
W.A. Alpaugh

Abstract A time delayed dielectric breakdown in printed circuit boards, operating at temperatures below the epoxy resin insulation thermo-electrical limits, is reported. The safe temperature-voltage operating regime was estimated and related to the glass-rubber transition (To) of printed circuit board dielectric. The TG was measured using DSC and compared with that determined from electrical conductivity of the laminate in the glassy and rubbery state. A failure model was developed and fitted to the experimental data matching a localized thermal degradation of the dielectric and time dependency. The model is based on localized heating of an insulation resistance defect that under certain voltage bias can exceed the TG, thus, initiating thermal degradation of the resin. The model agrees well with the experimental data and indicates that the failure rate and truncation time beyond which the probability of failure becomes insignificant, decreases with increasing glass-rubber transition temperature.


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