Behaviour of oxide inclusions and sulphur in ‘two-stage basicity control’ refining method of Si-killed spring steel

2020 ◽  
pp. 1-11
Author(s):  
Chen Wang ◽  
Yan-Shen Han ◽  
Jiang-Shan Zhang ◽  
Dong Xiao ◽  
Jun Yang ◽  
...  
China Foundry ◽  
2017 ◽  
Vol 14 (4) ◽  
pp. 233-243 ◽  
Author(s):  
Cong Li ◽  
Jian-guo Li ◽  
Yi-zhe Mao ◽  
Jia-cheng Ji

2011 ◽  
Vol 52-54 ◽  
pp. 1681-1686 ◽  
Author(s):  
Yang Li ◽  
Zhou Hua Jiang ◽  
Shi You Yin ◽  
Ying Zhuang ◽  
Ming Li

The variation of non-metallic inclusions and total oxygen contents in different steel grades were investigated by taking samples in steelmaking process, including gear steel, anchor chain steel, hard wire steel, bearing steel and spring steel. The inclusions mainly were Al2O3, MnS, and their composite inclusions in aluminum killed steel at the beginning of LF refining due to addition of FeAl alloy during the tapping from EAF and feeding of Al wire in LF process, and then Al2O3 inclusion changed to the Al2O3 - CaO composite inclusions after feeding of SiCa wire. The inclusions at the beginning of LF refining mainly were MnS, SiC and their composite inclusions in non-aluminum killed steel due to addition of the composite deoxidation and slagging agents (mainly including CaC2 and SiC) when EAF taping, while the inclusions in tundish mainly were MnS, CaO - SiO2 - Al2O3 composite oxide - sulfide inclusions. It is showed that the inclusions in bearing steel and spring steel samples were mainly globular oxide inclusions and silicate inclusions with higher rated results. Therefore, the refining process should be improved to remove globular oxide inclusions. The inclusions in molten steel were controlled by enhancing the diffusion deoxidation process, adjusting and controlling the basicity and composition of refining slags, respectively, and satisfactory results were obtained. The industrial test shows that the total oxygen content of the aluminum killed steel in the test heat after feeding wire reached the minimum value, which indicates that the optimized slag has a strong ability of absorbing Al2O3 inclusions. For non-aluminum killed steel, the total oxygen content was 0.0027 % to 0.0029 % in rolled products. The inclusions in the end of refining and rolled product were small and dispersed composite inclusions, and the separate Al2O3 inclusions can not be found in the non-aluminum killed steel after optimization of the refining process.


2013 ◽  
Vol 331 ◽  
pp. 508-512 ◽  
Author(s):  
Xiao Dong Wu ◽  
Rui Long Chen ◽  
Bo Xiao ◽  
Zhong Ying Wang

The inclusions in ultra-low oxygen spring steel during process were studied. Sufficient aluminium was used during tapping. The refining slag has high basicity and strong reducibility. The total oxygen is only 10×10-6 in billet and the oxide inclusions in the steel have finished the transformation during refining and some complex oxide inclusions are easy to remove at steelmaking temperature. Residual oxide inclusions in the steel are CaO-MgO-Al2O3 complex inclusions with a relatively lower melting point, which have a little deform-ability during hot-working and can improve the fatigue properties of high speed wheel steel effectively.


2013 ◽  
Vol 744 ◽  
pp. 379-382
Author(s):  
Xiao Dong Wu ◽  
Rui Long Chen ◽  
Bo Xiao ◽  
Zhong Ying Wang

A production process of high tensile strength spring steel is discussed in this paper. Sufficient aluminum was added into ladle during tapping and barium alloy was used in late refining process. It was found that the refining slag with high basicity is strongly deoxidized after refining, with total oxygen content being less than 10×10-6 in billet. Thus, the oxide inclusions in the steel is finished the transformation during refining and some complex oxide inclusions are remarkably removed at steelmaking temperature. The tensile strength over 2.0GPa and the extension rate up to 10% are obtained for the spring steel after quenching temperature at 900oC and tempering at 410 oC. So, the strength and plasticity of the steel are improved obviously.


2019 ◽  
Vol 50 (4) ◽  
pp. 1862-1877
Author(s):  
Sha Lyu ◽  
Xiaodong Ma ◽  
Zongze Huang ◽  
Zan Yao ◽  
Hae-Geon Lee ◽  
...  

Author(s):  
Sengshiu Chung ◽  
Peggy Cebe

We are studying the crystallization and annealing behavior of high performance polymers, like poly(p-pheny1ene sulfide) PPS, and poly-(etheretherketone), PEEK. Our purpose is to determine whether PPS, which is similar in many ways to PEEK, undergoes reorganization during annealing. In an effort to address the issue of reorganization, we are studying solution grown single crystals of PPS as model materials.Observation of solution grown PPS crystals has been reported. Even from dilute solution, embrionic spherulites and aggregates were formed. We observe that these morphologies result when solutions containing uncrystallized polymer are cooled. To obtain samples of uniform single crystals, we have used two-stage self seeding and solution replacement techniques.


2007 ◽  
Vol 177 (4S) ◽  
pp. 121-121
Author(s):  
Antonio Dessanti ◽  
Diego Falchetti ◽  
Marco Iannuccelli ◽  
Susanna Milianti ◽  
Gian P. Strusi ◽  
...  
Keyword(s):  

2007 ◽  
Vol 177 (4S) ◽  
pp. 120-120
Author(s):  
Pamela I. Ellsworth ◽  
Anthony Caldamone
Keyword(s):  

2005 ◽  
Vol 38 (18) ◽  
pp. 68
Author(s):  
SHARON WORCESTER
Keyword(s):  

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