Deformation cubic anvil press and stress and strain measurements using monochromatic X-rays at high pressure and high temperature

2011 ◽  
Vol 31 (3) ◽  
pp. 399-406 ◽  
Author(s):  
Rei Shiraishi ◽  
Eiji Ohtani ◽  
Tomoaki Kubo ◽  
Naoko Doi ◽  
Akio Suzuki ◽  
...  
2009 ◽  
Vol 16 (6) ◽  
pp. 742-747 ◽  
Author(s):  
Norimasa Nishiyama ◽  
Yanbin Wang ◽  
Tetsuo Irifune ◽  
Takeshi Sanehira ◽  
Mark L. Rivers ◽  
...  

1998 ◽  
Vol 5 (3) ◽  
pp. 1023-1025 ◽  
Author(s):  
Yoshinori Katayama ◽  
Kazuhiko Tsuji ◽  
Osamu Shimomura ◽  
Takumi Kikegawa ◽  
Mohamed Mezouar ◽  
...  

A new method for density measurements by means of X-ray absorption under high pressure and high temperature using synchrotron radiation has been developed. The method has been modified for a large-volume Paris–Edinburgh press and combined with intense high-energy X-rays at the ESRF. In order to overcome effects of deformation of sample shape under pressure, a ruby cylinder was used as a sample container. The density was determined from the intensity profile of transmitted X-rays. The densities of crystalline and liquid Bi were successfully measured up to 750 K at 1 GPa.


Author(s):  
E. F. Koch

Because of the extremely rigid lattice structure of diamond, generating new dislocations or moving existing dislocations in diamond by applying mechanical stress at ambient temperature is very difficult. Analysis of portions of diamonds deformed under bending stress at elevated temperature has shown that diamond deforms plastically under suitable conditions and that its primary slip systems are on the ﹛111﹜ planes. Plastic deformation in diamond is more commonly observed during the high temperature - high pressure sintering process used to make diamond compacts. The pressure and temperature conditions in the sintering presses are sufficiently high that many diamond grains in the sintered compact show deformed microtructures.In this report commercially available polycrystalline diamond discs for rock cutting applications were analyzed to study the deformation substructures in the diamond grains using transmission electron microscopy. An individual diamond particle can be plastically deformed in a high pressure apparatus at high temperature, but it is nearly impossible to prepare such a particle for TEM observation, since any medium in which the diamond is mounted wears away faster than the diamond during ion milling and the diamond is lost.


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