Microwave-assisted synthesis of nanocrystalline binary and ternary metal oxides

2017 ◽  
Vol 63 (6) ◽  
pp. 341-374 ◽  
Author(s):  
Markus B. Schütz ◽  
Lisong Xiao ◽  
Thomas Lehnen ◽  
Thomas Fischer ◽  
Sanjay Mathur
2012 ◽  
Vol 2012 ◽  
pp. 1-15 ◽  
Author(s):  
Sarah C. Motshekga ◽  
Sreejarani K. Pillai ◽  
Suprakas Sinha Ray ◽  
Kalala Jalama ◽  
Rui. W. M. Krause

The study of coating carbon nanotubes with metal/oxides nanoparticles is now becoming a promising and challenging area of research. To optimize the use of carbon nanotubes in various applications, it is necessary to attach functional groups or other nanostructures to their surface. The combination of the distinctive properties of carbon nanotubes and metal/oxides is expected to be applied in field emission displays, nanoelectronic devices, novel catalysts, and polymer or ceramic reinforcement. The synthesis of these composites is still largely based on conventional techniques, such as wet impregnation followed by chemical reduction of the metal nanoparticle precursors. These techniques based on thermal heating can be time consuming and often lack control of particle size and morphology. Hence, there is interest in microwave technology recently, where using microwaves represents an alternative way of power input into chemical reactions through dielectric heating. This paper covers the synthesis and applications of carbon-nanotube-coated metal/oxides nanoparticles prepared by a microwave-assisted method. The reviewed studies show that the microwave-assisted synthesis of the composites allows processes to be completed within a shorter reaction time with uniform and well-dispersed nanoparticle formation.


Herein, versatile, and reproducible method to prepare binary metal oxides via microwave assisted synthesis. Catalysts are substances that basically speeds up chemical reactions. Ideally, bonds are formed between the catalysts and the reactants. Also, catalysts permits formation of products from the reactants. These formed products, splits off the catalyst without affecting or changing it. Catalytic kinetics studies the correlate chemical reaction rate with some properties of reactants and/or products for instance; temperature, concentration and pressure. The aim of the project is to prepare pure and bi-metal iron based catalyst by co-precipitation method and to characterize the prepared sample using X-ray diffraction .Metal oxides nanoparticles is a field of interest in catalysis, such that these oxides are used to oxidize carbon monoxide. The samples were prepared through co-precipitation method in laboratory scale. The metals used was copper, iron and cobalt. After preparing pure sample of each metal a mix of two metals were introduced in different ratios. The samples were characterized via X-ray diffraction (XRD) and then the results were compared to exist data introduced from others research, the prepared samples XRD was having a great matching with the data retrieved from internet and we found that the metal could exist in two form of oxides and even could exist as pure metal. Each peak in the XRD figure could indicate one or more phase of the metal.


Nanoscale ◽  
2021 ◽  
Author(s):  
Nitika Devi ◽  
Sumanta Sahoo ◽  
Rajesh Kumar ◽  
Rajesh Kumar Singh

Microwave-assisted synthesis of carbon nanomaterials, metal oxides/hydroxides and their composites for energy storage applications.


2020 ◽  
Vol 57 (3) ◽  
pp. 265-272
Author(s):  
Priya S. Singh ◽  
Aizaz Shaikh ◽  
Aditi Deshmukh ◽  
Amit P. Pratap

2013 ◽  
Vol 17 (20) ◽  
pp. 2279-2304 ◽  
Author(s):  
Shrinivas Joshi ◽  
Uttam More ◽  
Venkatrao Kulkarni ◽  
Tejraj Aminabhavi

Author(s):  
Hadis Khodadad ◽  
Farhad Hatamjafari ◽  
Khalil Pourshamsian ◽  
Babak Sadeghi

Aim and Objective: Microwave-assisted condensation of acetophenone 1 and aromatic aldehydes 2 gave chalcone analogs 3, which were cyclized to pyrazole derivatives 6a-f via the reaction with hydrazine hydrate and oxalic acid in the presence of the catalytic amount of acetic acid in ethanol. Materials and Methods: The structural features of the synthesized compounds were characterized by melting point, FT-IR, 1H, 13C NMR and elemental analysis. Results: The antibacterial activities of the synthesized pyrazoles was evaluated against three gram-positive bacteria such as Enterococcus durans, Staphylococcus aureus, Bacillus subtilis and two gram-negative bacteria such as Escherichia coli and Salmonella typhimurium. Conclusion: All the synthesized pyrazoles showed relatively high antibacterial activity against S. aureus strain and none of them demonstrated antibacterial activity against E. coli.


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