scholarly journals Structure of tantalum coatings on NiTi substrate deposited by magnetron sputtering

2022 ◽  
Vol 2155 (1) ◽  
pp. 012013
Author(s):  
A S Dikov ◽  
A S Larionov ◽  
E A Zhakanbayev ◽  
L A Dikova ◽  
A Zh Sanssyzbayeva ◽  
...  

Abstract The paper provides the results of studies of the structural-phase state of tantalum coatings prepared by magnetron deposition. The coatings were deposited on substrates made of titanium nickelide with a shape memory. The NiTi temperature during coating deposition did not exceed 100 °C. The structural-phase state of Ta was determined by X-ray diffraction at different stages of coating formation. It has been shown that at the initial stage of deposition, two-phase coatings (α- and β-Ta) are formed. The synthesis of the coating from Ta leads to the growth of interplanar distance of the B2 austenite phase in the crystallographic direction (100). The growth of interplanar spacing is caused by formation of microstresses during interaction with incident tantalum ions. The lattice parameters of the B19 ‘phase, responsible for appearance of the shape memory effect, do not change during deposition of the tantalum coating.

2022 ◽  
Vol 1213 (1) ◽  
pp. 012004
Author(s):  
D Yu Zhapova ◽  
A I Lotkov ◽  
V N Grishkov ◽  
A A Gusarenko ◽  
I S Rodionov

Abstract The paper presents the experimental results of studies of the temperature dependence of inelastic and plastic strains during torsion of coarse-grained samples of the Ti49.3Ni50.7 (at.%) alloy. Investigations of the deformation behavior of the test alloy samples in the martensitic, two-phase and high-temperature states have been carried out. It is shown that the value of the summary inelastic strain reaches a maximum value of ∼ 18% under deformation of the samples in the martensitic and two-phase state, as well as in the temperature range of pre-transition phenomena.


2017 ◽  
Vol 906 ◽  
pp. 32-37 ◽  
Author(s):  
Vasilii A. Klimenov ◽  
Anatolii A. Klopotov ◽  
Yu.A. Abzaev ◽  
K.A. Kurgan ◽  
Yu.A. Vlasov

The paper presents the results of the X-ray diffraction analysis of structural-phase states in the weld zone of a titanium alloy Grade2 in micro-and submicrocrystalline states. It is established that the structural-phase state in the weld zone and in the heat-affected zone depends on the state of samples of the alloy Grade2 before welding. It is shown that formation process of metastable phases ω-Ti and α′′-Ti occurs in the submicrocrystalline state in the alloy Grade2 in the weld zone and in the heat-affected zone. Investigations of the features of the microhardness distribution in the weld zone in alloys Grade2 in micro-and submicrocrystalline states are carried out. Different character of microhardness distributions in the weld zone in the samples depending on the structural-phase state of welded plates made of alloy Grade2 is determined.


Vacuum ◽  
2021 ◽  
Vol 187 ◽  
pp. 110141
Author(s):  
I.O. Shpetnyi ◽  
I.Yu Protsenko ◽  
S.I. Vorobiov ◽  
V.I. Grebinaha ◽  
L. Satrapinskyy ◽  
...  

Author(s):  
Ivan A. Ditenberg ◽  
Denis A. Osipov ◽  
Michail A. Korchagin ◽  
Ivan V. Smirnov ◽  
Konstantin V. Grinyaev ◽  
...  

1995 ◽  
Vol 398 ◽  
Author(s):  
F.F. Gong ◽  
H.M. Shen ◽  
Y.N. Wang

ABSTRACTThe crystallization of amorphous sputtered NiTi films was investigated for selected heat treatments. From x-ray diffraction patterns, when the films were annealed below the crystallization temperature, the intensity of the broad maximum centered at 2θ = 43.5° increased with increasing the annealing temperature and time. When the films were annealed at 550°C for 0.5hr, parent B2 phase and Ni4Ti3 precipitates appeared. For annealing temperature above 700°C, the films showed embrittlement and volatilization. Therefore the optimum heat treatment for the optimum shape memory effect is found. The average grain size increased slowly in the initial stage of annealing but remained almost unchanged when the films were annealed for more than 1hr. This is because the grain boundary grooving caused by the titanium at a certain temperature volatilization seriously hinder the grain growth.


2021 ◽  
Vol 33 (11) ◽  
pp. 04021324
Author(s):  
Almira Zhilkashinova ◽  
Mazhyn Skakov ◽  
Madi Abilev ◽  
Dossym Yerbolatuly

2018 ◽  
Vol 143 ◽  
pp. 03004
Author(s):  
Natalya Popova ◽  
Lyudmila Erygina ◽  
Elena Nikonenko ◽  
Mazhin Skakov

The paper describes results of studies of phase transitions in structural phase state occurring in the type 0.34C-1Cr-1Ni-1Mo-Fe steel under electrolytic plasma nitriding in nitrogen-containing water solution. The nitriding voltages considered in the given study were 550 and 600 V. The research was conducted by means of X-ray diffraction electron microscopy. The specimens were studied in two states : 1) before modification (original state) and 2) after nitriding in the surface layer of the specimen. The study was conducted on thin foils. It was found that nitriding lead to significant changes in the structure of steel, namely in its phase composition and in the number of existing phases. In the original state the structure of steel was given as lamellar pearlite, ferritic carbide mix and fragmented ferrite. After 550 V nitriding it was lath martensite, plates of α-phase, with colonies of thin parallel plates of γ-phase and coarse grains of α-phase, containing γ-phase grains which were different in size and shape and were various-directional. Increase in nitriding voltage up to 600 V lead to change in the structure given as a lamellar non-fragmented pearlite and fragmented ferrite. The original state was marked by presence of particles of M3C cementite, after nitriding irrespective of the voltage it had the particles of M3C alloyed cementite, Fe3Mo3N nitride and Cr2C0.61N0.39 carbonitride. The sizes, volume fractions and locations of particles were dependent on nitriding voltage.


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