scholarly journals Effect of Molar Ratio on Crystal Structure and Surface Morphology of Nd1(Fe)xBa2-xCu3O7 Oxide Alloy by Solid-State Reaction Method

Author(s):  
N. A. Humairah ◽  
D. Sartika ◽  
Muris ◽  
E. H. Sujiono
Author(s):  
Hongqiang Cui ◽  
Yongze Cao ◽  
Lei Zhang ◽  
Yuhang Zhang ◽  
Siying Ran ◽  
...  

Er3+ with different concentrations doped K2Yb(PO4)(MoO4) phosphors were prepared by a solid-state reaction method, and the layered orthorhombic crystal structure of the samples was confirmed by X-ray diffraction (XRD). Under...


RSC Advances ◽  
2018 ◽  
Vol 8 (28) ◽  
pp. 15613-15620 ◽  
Author(s):  
Xiaochun He ◽  
Ruiqing Chu ◽  
Zhijun Xu ◽  
Zhongran Yao ◽  
Jigong Hao

Lead-free ceramics, SrBi2Nb2O9–xBi2O3 (SBN–xBi), with different Bi contents of which the molar ratio, n(Sr) : n(Bi) : n(Nb), is 1 : 2(1 + x/2) : 2 (x = −0.05, 0.0, 0.05, 0.10), were prepared by conventional solid-state reaction method.


RSC Advances ◽  
2017 ◽  
Vol 7 (56) ◽  
pp. 35305-35310 ◽  
Author(s):  
Chao Xing ◽  
Jianzhu Li ◽  
Huiling Chen ◽  
Hengyang Qiao ◽  
Jun Yang ◽  
...  

Herein, a Y(Mg1/2Sn1/2)O3 (YMS) ceramic was synthesized using a conventional solid-state reaction method.


2012 ◽  
Vol 512-515 ◽  
pp. 1488-1493 ◽  
Author(s):  
Li Hong Liu ◽  
Rong Jun Xie ◽  
Xu Dong Sun ◽  
Qing Huang ◽  
Naoto Hirosaki

This paper reports the photoluminescence properties of Ca9Eu1-xSmx(VO4)7 (x=0.2-0.4) synthesized at 1250 oC in air for 12 h using traditional solid-state reaction method. With the increase of Sm3+ substitution amount, purity Ca9Eu1-xSmx(VO4)7 phase was obtained even when the Eu3+ ions were totally substituted by Sm3+. The experimental results showed that when Sm3+ was codoped with Eu3+ into Ca9Eu1-xSmx(VO4)7 crystal structure, Sm3+ would act as a sensitizer and transfer the excitation energy to Eu3+ ions and finally enhance the emission intensity of Ca9Eu1-xSmx(VO4)7 under 405 nm excitation, which leads to more favorite of this kind of phosphor used in UV LED based white LEDs.


2016 ◽  
Vol 852 ◽  
pp. 454-460 ◽  
Author(s):  
Qiu Hong Zhang ◽  
Hai Yong Ni ◽  
Ling Li Wang ◽  
Fang Ming Xiao

Deep red emitting CaAl12-xO19:xMn4+ phosphors were synthesized by solid state reaction method. Various fluxes (BaF2, H3BO3, Na2CO3 and NH4Cl) were added in preparation of the phosphors. The influences of the various fluxes on the crystal structure, morphology and luminescent properties of CaAl12O19:Mn4+ phosphors were studied. The results show that the obtained phosphors with fluxes possessed better luminescent intensity than that of the phosphors without fluxes. The maximum luminescent intensities were found with the following order: H3BO3 (2.0 wt%) > Na2CO3 (0.5 wt%) > NH4Cl (0.3 wt%) > BaF2 (0.1 wt%) > no flux. The H3BO3 flux can decrease the single phase forming temperature of CaAl12O19:Mn4+ phosphors by about 150°C.


2013 ◽  
Vol 745-746 ◽  
pp. 113-118
Author(s):  
Lei Wang ◽  
Xue Ying Chen ◽  
Jin Bao Xu ◽  
Liang Bian ◽  
Bo Gao

BiFeO3nanoparticles were synthesized by a NaNO3-assisted low-heating temperature solid state reaction method. The effects of the molar ratio of added NaNO3and the calcination temperature on the characteristics of the products were discussed. The structure, morphology, magnetic, optical and electrical properties of BiFeO3were characterized by XRD, SEM, VSM and UV-VIS. The experimental results showed that the introduction of leachable inert inorganic salt as a hard agglomeration inhibitor in the mixture precursor led to the formation of BiFeO3nanoparticles with uniform size. With the addition of NaNO3in the process, the particle morphology decreased from a diameter of 300-500 nm to 80-100 nm. The BiFeO3attained at 600 °C showed a smaller band gap (2.12 eV) and weak ferromagnetism at room temperature with a remnant magnetization value (Mr) of approximately 3.1×10-5emu/g and a coercive filed value (Hc) of nearly 20 Oe.


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