scholarly journals Designing TiO2 nanostructures through hydrothermal growth: influence of process parameters and substrate position

Nano Express ◽  
2021 ◽  
Author(s):  
Sutapa Dey ◽  
Somnath Chanda Roy
2012 ◽  
Vol 428 ◽  
pp. 147-152
Author(s):  
Wen Chang Lang ◽  
Rong Song ◽  
Bin Gao

This paper systematically studies the distribution of macro-particles on the surface of film influenced by the substrate position under conditions of the same magnetic field, different pulsed bias voltage and reaction gas partial pressure, and analyzes the mechanism of macro-particles influenced by different parameters. This study indicates that the substrate position has a better effect on decreasing macro-particles than that of the pulsed bias voltage and particles in different substrate position are very different in their forms and appearances, which easily leads to uneven deposition; under the same bias, the number of particles firstly increases and then decreases with the increasing the distance from substrate position to the center, and the number of particles with over 2μm diameter largely decreases with the increasing the distance from substrate position to the center, so surface morphologies of films are improving; under the lower intensity of magnetic field, the distribution of macro-particles has a great change with the increasing the distance from substrate position to the center, and under the higher intensity of magnetic field, the substrate position has little influence on the distribution of macro-particles on the surface of film. Under the higher intensity (30G) of magnetic field, the distribution of macro-particles on the surface of film has minor change whatever reaction gas partial pressure and substrate position increase, and most particles are small in sizes and are solid spherical in shape. The higher intensity (30G) of magnetic field enhances the uniformity of film deposition and decreases the dependency of macro-particles distribution on other parameters.


2019 ◽  
Vol 34 (3) ◽  
pp. 367-375
Author(s):  
L.-X. Wang ◽  
D.-F. Wang ◽  
L. Jiang ◽  
N. Bian ◽  
Q. Li ◽  
...  

2021 ◽  
Vol 54 ◽  
pp. 961-971
Author(s):  
Sergey Shantarenko ◽  
Victor Kuznetsov ◽  
Eugene Ponomarev ◽  
Alexander Vaganov ◽  
Alexey Evseev

2018 ◽  
Vol 26 ◽  
pp. 690-699 ◽  
Author(s):  
Guillaume Filliard ◽  
Mohamed El Mansori ◽  
Mathieu De Metz-Noblat ◽  
Christian Bremont ◽  
Anthony Reullier ◽  
...  

2015 ◽  
Vol 1111 ◽  
pp. 211-216
Author(s):  
Bogdan Florin Toma ◽  
Iulian Ionita ◽  
Diana Antonia Gheorghiu ◽  
Lucian Eva ◽  
Costică Bejinariu ◽  
...  

Influence of the process parameters and geometry of the spraying nozzle on the properties of titanium deposits obtained in wire arc spraying. Wire arc spraying is a process in which through minor modifications of the spray parameters, they can have a major impact on the coatings properties. In this paper there is presented a study on the influence of process parameters and fluid dynamics of the atomization gas on the properties of titanium deposits (14T - 99.9% Ti). For this there were used three different frontal spraying nozzles, having different geometries, and were varied the spraying gas pressure and the electrical current on three levels. There were evaluated the particles velocity, coating density, chemical composition and characteristic interface between deposition and substrate. Obviously, the high speed of the atomization gas determinate the improving of all properties, but in the same time increased the oxide content in the layer. However, the oxidation can be drastically reduced if the melting and atomization of the wire droplets is produced at the point of formation of the electric arc, and the spraying jet is designed to constrain the electric arc. The assessment of deposits adherence allowed the observation of process parameters that contribute to its improvement.


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