Sodium Lauryl Sulfate in Egg Whites

1967 ◽  
Vol 50 (4) ◽  
pp. 847-849
Author(s):  
John Wiskerchen
Keyword(s):  
Chloride Solution ◽  
Sodium Lauryl Sulfate ◽  
Collaborative Study ◽  
Egg White ◽  
Chloride Complex ◽  
Bromphenol Blue ◽  
Lauryl Sulfate ◽  
Benzethonium Chloride ◽  
Alkyl Sulfates

Abstract A method is given for the quantitative determination of sodium lauryl sulfate in liquid, frozen, powdered, or flake-dried egg white. The egg white is dissolved in water and the protein is precipitated with ethanol and filtered off. The filtrate is evaporated, the residue is dissolved in water, and the pH is adjusted to 5.0. Total alkyl sulfates are titrated with standard benzethonium chloride solution in the presence of chloroform with bromphenol blue indicator. Results are calculated as sodium lauryl sulfate. The formation of the bromphenol bluebenzethonium chloride complex, when excess benzethonium chloride is present, is taken as the end point. The blue-green complex is soluble in the chloroform. Overall recoveries of sodium lauryl sulfate from egg whites ranged from 94 to 100%. Collaborative study of the method is recommended.

Collaborative Study of a Method for Sodium Lauryl Sulfate in Egg Whites

1968 ◽  
Vol 51 (3) ◽  
pp. 540-543
Author(s):  
John Wiskerchen
Keyword(s):  
Sulfuric Acid ◽  
Quantitative Determination ◽  
Sodium Lauryl Sulfate ◽  
Collaborative Study ◽  
Colorimetric Method ◽  
Egg White ◽  
Mean Deviation ◽  
Lauryl Sulfate ◽  
Benzethonium Chloride

Abstract A colorimetric method for the quantitative determination of sodium lauryl sulfate in liquid, frozen, and powdered egg white was studied by eight collaborators. Determinations were made on flake and powdered egg white at levels of 0.05, 0.1, and 0.2% (w/w) and on liquid egg white at levels of 0.006, 0.0125, and 0.0250% (w/w) sodium lauryl sulfate. The egg white is dissolved in water, and the protein is precipitated with ethanol and removed by filtration. An aliquot of the filtrate is evaporated to dryness, and the residue is dissolved in water and acidified with sulfuric acid. The sodium lauryl sulfate is complexed with Azure A, extracted into chloroform, and determined spectrophotometrically at 637 mμ. A blank determination is made on another aliquot of the filtrate by complexing the sodium lauryl sulfate with benzethonium chloride. This is a stable colorless complex. Average recoveries in the collaborative study were 98—102% with a mean deviation of 2.8—5.4%. It is recommended that the method be adopted as official, first action.

Thin Layer Chromatographic Method for Determination of Deoxynivalenol in Wheat: Collaborative Study

1986 ◽  
Vol 69 (1) ◽  
pp. 37-40 ◽  
Author(s):  
Robert M Eppley ◽  
Mary W Trucksess ◽  
Stanley Nesheim ◽  
Charles W Thorpe ◽  
Albert E Pohland ◽  
...  
Keyword(s):  
Winter Wheat ◽  
Thin Layer ◽  
Thin Layer Chromatography ◽  
Aluminum Chloride ◽  
Chloride Solution ◽  
Chromatographic Method ◽  
Collaborative Study ◽  
Sample Extraction ◽  
Layer Chromatography

Abstract A collaborative study of a rapid method for the determination of deoxynivalenol (DON) in winter wheat was successfully completed. The method involves sample extraction with acetonitrile-water (84 + 16), cleanup using a disposable column of charcoal, Celite, and alumina, and detection by thin layer chromatography after spraying with an aluminum chloride solution. Each of the 15 collaborators analyzed 12 samples, 2 of which were naturally contaminated, and 10 to which DON was added, in duplicate, at levels of 0,50,100,300, and 1000 ng/ g. Average recoveries of DON ranged from 78 to 96% with repeatabilities of 30-64% and reproducibilities of 33-87%. The results of the study show that false positives were not a problem and that all of the analysts could detect DON at the 300 ng/g level or higher. The method has been adopted official first action.

Modified Method for Extracting Light Filth from Chocolate Liquor by Using 2% Igepal CO 630 as Detergent Solution: Collaborative Study

1978 ◽  
Vol 61 (5) ◽  
pp. 1041-1042
Author(s):  
Donald A Mastrorocco ◽  
Geraldine H Wagner
Keyword(s):  
Sodium Lauryl Sulfate ◽  
Collaborative Study ◽  
Detergent Solution ◽  
Lauryl Sulfate ◽  
Chocolate Liquor ◽  
Modified Method ◽  
Filter Papers ◽  
Detergent Solutions

Abstract A collaborative study was conducted among 3 laboratories comparing 2 detergent solutions, 2% Igepal CO 630 and the AOAC-approved 2% sodium lauryl sulfate, in the analysis of extraneous materials in chocolate liquor. Each laboratory tested a minimum of 8 samples per detergent solution. No significant differences were found between the numbers of rodent hairs and insect fragments recovered with the 2 detergent solutions and, in addition, igepal produced cleaner filter papers. The 2% Igepal CO 630 detergent solution has been adopted as a substitute for 2% sodium lauryl sulfate in 44.006(b) for chocolate liquor.

Colorimetric Determination of Sodium Lauryl Sulfate

1959 ◽  
Vol 31 (10) ◽  
pp. 1673-1676 ◽  
Author(s):  
H. D. Graham ◽  
R. McL. Whitney
Keyword(s):  
Sodium Lauryl Sulfate ◽  
Colorimetric Determination ◽  
Lauryl Sulfate

Alternative Sieving Method for Extraction of Light Filth from Cheeses: Collaborative Study

1994 ◽  
Vol 77 (5) ◽  
pp. 1153-1156
Author(s):  
Marvin J Nakashima
Keyword(s):  
Sodium Lauryl Sulfate ◽  
Collaborative Study ◽  
Sulfate Solution ◽  
Lauryl Sulfate ◽  
Test Portion ◽  
Alternative Method ◽  
Broad Variety ◽  
Filter Papers

Abstract A collaborative study was conducted on an alternative sieving method for the extraction of light filth from cheeses. The alternative method was developed that is applicable to broad variety of cheeses. A 225 g test portion is dispersed in a solution of 5.7% HCI, Igepal CO-730, and Igepal DM-710. Digested cheese is wet-sieved on a No. 230 sieve. The residue is treated with Tergitol Anionic 4, transferred to 1% sodium lauryl sulfate solution, heated, and maintained at 65°-75°C for 10 min. The residue is washed with these 2 surfactants a maximum of 4 times until it is reduced to an amount that is filterable. The residue is filtered and the filter papers are examined microscopically at a magnification of ca 30×. Average recoveries by 9 collaborators for 3 spike levels of rat hairs (5,10, and 15) were 80, 68, and 81%, respectively; for insect fragments (5,15, and 30) recoveries were 97, 90, and 92%, respectively. The alternative sieving method for extraction of light filth from cheeses has been adopted first action by AOAC INTERNATIONAL.

scholarly journals Final Report on the Safety Assessment of Sodium Cetearyl Sulfate and Related Alkyl Sulfates as Used in Cosmetics

2010 ◽  
Vol 29 (3_suppl) ◽  
pp. 115S-132S ◽  
Author(s):  
Monice Fiume ◽  
Wilma F. Bergfeld ◽  
Donald V. Belsito ◽  
Curtis D. Klaassen ◽  
James G. Marks ◽  
...  
Keyword(s):  
Sodium Salt ◽  
Safety Assessment ◽  
Sodium Lauryl Sulfate ◽  
Expert Panel ◽  
The Other ◽  
Final Report ◽  
Lauryl Sulfate ◽  
Alkyl Sulfates ◽  
Sodium Decyl Sulfate

Sodium cetearyl sulfate is the sodium salt of a mixture of cetyl and stearyl sulfate. The other ingredients in this safety assessment are also alkyl salts, including ammonium coco-sulfate, ammonium myristyl sulfate, magnesium coco-sulfate, sodium cetyl sulfate, sodium coco/hydrogenated tallow sulfate, sodium coco-sulfate, sodium decyl sulfate, sodium ethylhexyl sulfate, sodium myristyl sulfate, sodium oleyl sulfate, sodium stearyl sulfate, sodium tallow sulfate, sodium tridecyl sulfate, and zinc coco-sulfate. These ingredients are surfactants used at concentrations from 0.1% to 29%, primarily in soaps and shampoos. Many of these ingredients are not in current use. The Cosmetic Ingredient Review (CIR) Expert Panel previously completed a safety assessment of sodium and ammonium lauryl sulfate. The data available for sodium lauryl sulfate and ammonium lauryl sulfate provide sufficient basis for concluding that sodium cetearyl sulfate and related alkyl sulfates are safe in the practices of use and concentration described in the safety assessment.

Sign in / Sign up

Export Citation Format

Share Document