Determination of Ivermectin in Medicated Swine Feeds at the 2 ppm Concentration Level

1990 ◽  
Vol 73 (6) ◽  
pp. 931-934
Author(s):  
Stephen J Doherty ◽  
Allen Fox ◽  
David W Fink
Keyword(s):  
Chromatographic Analysis ◽  
Concentration Level ◽  
Reverse Phase ◽  
Ultraviolet Detection ◽  
Mean Relative Error ◽  
Relative Standard ◽  
Liquid Chromatographic Analysis ◽  
Liquid Chromatographic ◽  
Medicated Feeds

Abstract An analytical method has been developed that Is applicable to the determination of Ivermectin in medicated feeds at the 2 ppm concentration level. It Is based upon liquid chromatographic analysis with a reverse-phase column and ultraviolet detection. After the drug Is extracted from the feed Into methanol, an analytical sample Is prepared by the consecutive use of column chromatography on alumina and solidphase extraction on Sep-Pak C18 and silica cartridges. This procedure has been applied to the concentration range 0.50- 3.0 ppm of Ivermectin In feed with an accuracy of ±2% mean relative error and a precision of ± 2% relative standard deviation at the 2 ppm concentration level.

scholarly journals Determination of 4-Hexylresorcinol in Shrimp by Liquid Chromatography with Fluorescence Detection

2000 ◽  
Vol 83 (1) ◽  
pp. 241-244 ◽  
Author(s):  
Klaas M Jonker ◽  
Colinda P Dekker
Keyword(s):  
Liquid Chromatography ◽  
Chromatographic Analysis ◽  
Reversed Phase ◽  
Fluorimetric Detection ◽  
Relative Standard ◽  
Liquid Chromatographic Analysis ◽  
Liquid Chromatographic ◽  
Phase Column ◽  
Reversed Phase Column

Abstract A method was developed to determine 4-hexylresorcinol in shrimp meat. The procedure is based on extraction of test portions with methanol followed by liquid chromatographic analysis of the extracts, using a reversed-phase column and fluorimetric detection (excitation: 280 nm, and emission: 310 nm). The confidence interval of the recovery in working range of 1.5–2.5 mg/kg was 81.6 ± 0.8%. The relative standard deviation in the working range was 2.1%. Limits of quantitation and detection were 6.59 and 1.98 ng/mL extract, respectively, corresponding to 0.26 and 0.08 mg/kg in shrimp.

Liquid Chromatographic Determination of Zoalene in Medicated Feeds

1984 ◽  
Vol 67 (5) ◽  
pp. 861-862 ◽  
Author(s):  
John Morawski ◽  
Glenn Kyle
Keyword(s):  
Colorimetric Method ◽  
Chromatographic Determination ◽  
Activated Alumina ◽  
Reverse Phase ◽  
Liquid Chromatographic Determination ◽  
Phase Liquid ◽  
Aoac Official ◽  
Liquid Chromatographic ◽  
Medicated Feeds

Abstract A rapid, reliable separation and quantitation of zoalene (3,5-dinitroo-toluamide) from feeds is accomplished by using reverse phase liquid chromatography (LC) and ultraviolet detection. An extraction technique which is similar to the present AOAC official colorimetric method is used before chromatographic analysis. This extraction is followed by an activated alumina cleanup and LC to separate zoalene from feed matrix. The methodology was applied to a variety of spiked feed matrices, and yielded good recoveries. Liquid chromatographic results were shown to correlate with colorimetric determinations.

Liquid Chromatographic Determination of Sulfentrazone in Soil

1999 ◽  
Vol 82 (5) ◽  
pp. 1214-1216 ◽  
Author(s):  
G Anthony Ohmes ◽  
Thomas C Mueller
Keyword(s):  
Chromatographic Determination ◽  
Soil Samples ◽  
Ultraviolet Detection ◽  
Liquid Chromatographic Separation ◽  
Relative Standard ◽  
Limit Of Quantitation ◽  
Liquid Chromatographic Determination ◽  
Liquid Chromatographic ◽  
Soluble Components

Abstract A rapid method for the determination of sulfentrazone in soils is described. The method consists of extraction of soil samples with methanol, filtration, liquid chromatographic separation of methanol-soluble components through a C18 column, and ultraviolet detection at 220 nm. Recoveries from fortified surface soils were >85% for sulfentrazone. Average relative standard deviations over the soils examined was 7.7%. A conservative lower limit of quantitation for sulfentrazone was 40 ng/g soil.

Liquid Chromatographic Determination of Carminic Acid in Yogurt

1989 ◽  
Vol 72 (2) ◽  
pp. 231-234 ◽  
Author(s):  
Mercedes Jalón ◽  
Majesús Peńa ◽  
Julián C Rivas
Keyword(s):  
Chromatographic Determination ◽  
Carminic Acid ◽  
Reverse Phase ◽  
Liquid Chromatographic Method ◽  
Relative Standard ◽  
Array Detection ◽  
Liquid Chromatographic Determination ◽  
Phase Liquid ◽  
Liquid Chromatographic

Abstract A reverse-phase liquid chromatographic method is described for the determination of carminic acid in yogurt. A C18 column is used with acetonitrile-1.19M formic acid (19 + 81) as mobile phase and diode array detection. Sample preparation includes deproteinization with papain and purification in a polyamide column. The relative standard deviation for repeated determinations of carminic acid in a commercial strawberry-flavored yogurt was 3.0%. Recoveries of carminic acid added to a natural-flavored yogurt ranged from 87.2 to 95.3% with a mean of 90.2%. The method permits measurement of amounts as low as 0.10 mg/kg.

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