Shear bond strength of one-step self-etch adhesives to enamel: effect of acid pretreatment

ABSTRACTObjectives: The aim of this study was to compare the shear bond strength of several self-etch adhesives to their two-step predecessors to ground and unground enamel.Methods: Seventy-five extracted, non-carious human third molar teeth were selected for this study. The buccal surfaces of each tooth were mechanically ground to obtain flat enamel surfaces (ground enamel), while the lingual surfaces were left intact (unground enamel). The teeth were randomly divided into five groups according to the adhesive systems (n=15): one-step self-etch adhesive - Clearfil S3 Bond, its two-step predecessor - Clearfil SE Bond, one-step self-etch adhesive - AdheSE One, and its two-step predecessor - AdheSE, and a two-step etch-and-rinse adhesive - Adper Single Bond 2(control). After application of the adhesives to the buccal and lingual enamel surfaces of each tooth, a cylindrical capsule filled with a hybrid composite resin (TPH) was seated against the surfaces. The specimens were stored in distilled water at 37°C for 24 hours, followed by thermocycling (5°C-55°C/500 cycles). They were subjected to shear bond strength test in a universal testing machine at a crosshead speed of 1.0 mm/minute. The data were compared using a two-way ANOVA, followed by Bonferroni test at P<.05Results: All adhesives exhibited statistically similar bond strengths to ground and unground enamel except for the etch-and-rinse adhesive that showed significantly higher bond strengths than the self-etch adhesives (P<.05). No significant differences in bond strength values were observed between ground and unground enamel for any of the adhesives tested (P=.17).Conclusions:Similar bond strengths to ground and unground enamel were achieved with one-step self-etch adhesives and their predecessors. Enamel preparation did not influence the bonding performance of the adhesives tested. (Eur J Dent 2012;6:280-286)

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Bonding Effectiveness of Universal Adhesive to Intracoronal Bleached Dentin Treated with Sodium Ascorbate

Brazilian Dental Journal ◽

10.1590/0103-6440201600647 ◽

2016 ◽

Vol 27 (3) ◽

pp. 303-308 ◽

Cited By ~ 7

Author(s):

Thaís Fantinato Trindade ◽

Luana Kelle Batista Moura ◽

Walter Raucci Neto ◽

Danielle Cristine Furtado Messias ◽

Vivian Colucci

Keyword(s):

Bond Strength ◽

Shear Bond Strength ◽

Composite Resin ◽

Sodium Ascorbate ◽

Control Groups ◽

Universal Adhesive ◽

Bleaching Procedure ◽

Etch And Rinse ◽

One Step ◽

Self Etch

Abstract This study evaluated the effect of restorative protocol with sodium ascorbate on the shear bond strength (SBS) of a universal adhesive to intracoronal bleached dentin. One hundred-and-twenty bovine dentin fragments were randomly divided into 12 groups (n=10), according to the bleaching procedure (unbleached and bleached) and restorative protocol (no treatment, 10% sodium ascorbate -10SA, 35% sodium ascorbate -35SA and two-step etch-and-rinse -ER or one-step self-etch -SE Scotchbond universal adhesive approaches). Four whitening sessions were performed using 35% hydrogen peroxide. The samples from control groups were kept in relative humidity at 37 °C. Immediately after bleaching procedures, the assigned antioxidant solution was applied on dentin and restorative procedures were performed following either the ER or the SE approach. After 24 h, the specimens were subjected to SBS test. Data (MPa) were analyzed by ANOVA and Tukey's test (?=0.05). Lower SBS values were found for bleached specimens (8.54 MPa) compared with those unbleached (12.13 MPa) (p<0.05). The bond strength of the sodium ascorbate-treated groups was higher than those untreated, regardless of the strategy employed (p<0.05). Groups restored without sodium ascorbate showed lower bond strength values for both ER (8.32 MPa) and SE (8.28 MPa) adhesive strategies. The group treated with 10SA submitted to ER approach (10.14 MPa) was similar to untreated groups (p>0.05). It may be concluded that bond strength of composite resin to intracoronal dentin was affected by restorative protocol and reduced by bleaching.

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Effect of Decontamination Treatments on Micro-Shear Bond Strength between Blood–Saliva-Contaminated Post-Etched Dentin Substrate and Composite Resin

Healthcare ◽

10.3390/healthcare7040128 ◽

2019 ◽

Vol 7 (4) ◽

pp. 128

Author(s):

Satheesh B. Haralur ◽

Salem Mohammed Alharthi ◽

Saeed Aied Abohasel ◽

Khalid Mohammed alqahtani

Keyword(s):

Bond Strength ◽

Shear Bond Strength ◽

Composite Resin ◽

Testing Machine ◽

One Step ◽

The One ◽

Cleaning Methods ◽

Saliva Contamination ◽

Post Hoc ◽

Self Etch

Blood–saliva contamination negatively affects the bonding potential of adhesive agents. The study aimed to assess the effect of various cleaning protocols on micro-shear bond strength (μSBS) between blood–saliva-contaminated post-etched dentin and composite resin in total-etch and self-etch adhesives. The cleaning methods tested were water rinsing, 37.5% phosphoric acid (H3PO4) re-etching, 6% sodium hypochlorite (NaoCl), 2% chlorhexidine gluconate (CXG), isopropyl alcohol (IPA), and pumice. Nono-hybrid composite cylinders with a 3-mm diameter and 2-mm height were directly cured over the dentin substrate, stored for 24 h, and subjected to 12,000 thermocycles. The shear force was exerted with a 200-μm knife-edged chisel-shaped head from a universal testing machine. The type of failure was assessed with stereomicroscope magnified images. The obtained data were evaluated by Kruskal–Wallis and Mann–Whitney U post-hoc tests. Water-rinsed contaminated dentin surfaces showed substantially reduced μSBS in the total etch from 25.93 to 20.29 Mpa and the corresponding values for the one-step self-etch adhesive were 10.10 to 8.8. Re-etching with 37.5% H3Po4 resulted in a recovery of bonding potential in both total-etch (24.58 Mpa) and self-etch adhesive (9.23 Mpa). Alternately, NaoCl and pumice cleaning showed promising results for the total-etch (23.51 Mpa) and self-etch (7.79 Mpa).

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Evaluation of Effect of Different Cavity Disinfectants on Shear Bond Strength of Composite Resin to Dentin using Two-Step Self-Etch and One-Step Self-Etch Bonding Systems: A Comparative in vitro Study

The Journal of Contemporary Dental Practice ◽

10.5005/jp-journals-10024-1313 ◽

2013 ◽

Vol 14 (2) ◽

pp. 275-280 ◽

Cited By ~ 3

Author(s):

Shreetha Bhandary ◽

M Surya Chaitanya Reddy ◽

MC Mahesh ◽

J Pramod ◽

Ashwija Shetty

Keyword(s):

Hydrogen Peroxide ◽

Bond Strength ◽

Sodium Hypochlorite ◽

Shear Bond Strength ◽

Composite Resin ◽

Posterior Teeth ◽

One Step ◽

Bonding Systems ◽

Self Etch

ABSTRACT Aim and objectives To evaluate the effect of 2% chlorhexidine, 2% sodium hypochlorite, 3% hydrogen peroxide on shear bond strength of composite resin to dentin using two-step and onestep self-etch bonding systems and to study the mode of failure of specimens under stereomicroscope. Materials and methods Eighty extracted sound human posterior teeth were used. The occlusal surfaces were ground to expose the dentin and were then randomly divided into 4 main groups. In group I, no cavity disinfectant was used and served as control. In groups II, III, IV, 2% chlorhexidine, 2% sodium hypochlorite and 3% hydrogen peroxide were used as cavity disinfectants respectively. Each group was then divided into two subgroups of 10 teeth each according to the bonding agent used, two-step self-etch (Adper SE Plus) and one-step self-etch (Adper Easy One) respectively. A transparent cylindrical plastic tube was loaded with microhybrid composite and placed over the dentin and light cured for 40 seconds. The specimens were subjected to shear stress in the universal testing machine. Results Pretreatment with 2% chlorhexidine, 2% sodium hypochlorite and 3% hydrogen peroxide, had a negative effect on the shear bond strength of self-etching bonding systems. Conclusion The highest bond strength was found in 2% chlorhexidine group followed by 2% sodium hypochlorite group and the lowest bond strength was found in 3% hydrogen peroxide group. Clinical significance All three cavity disinfectants used in this study reduced the shear bond strength and hence should be used with caution. How to cite this article Reddy MSC, Mahesh MC, Bhandary S, Pramod J, Shetty A. Evaluation of Effect of Different Cavity Disinfectants on Shear Bond Strength of Composite Resin to Dentin using Two-Step Self-Etch and One-Step Self-Etch Bonding Systems: A Comparative in vitro Study. J Contemp Dent Pract 2013;14(2):275-280.

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The Effects of Prophylactic Ozone Pretreatment of Enamel on Shear Bond Strength of Orthodontic Brackets Bonded with Total or Self-Etch Adhesive Systems

European Journal of Dentistry ◽

10.1055/s-0039-1697855 ◽

2010 ◽

Vol 04 (04) ◽

pp. 367-373 ◽

Cited By ~ 6

Author(s):

Sevi Burcak Cehreli ◽

Asli Guzey ◽

Neslihan Arhun ◽

Alev Cetinsahin ◽

Bahtiyar Unver

Keyword(s):

Bond Strength ◽

Shear Bond Strength ◽

Orthophosphoric Acid ◽

Ozone Treatment ◽

Bond Failure ◽

Group 4 ◽

Group 3 ◽

Group 2 ◽

Self Etch ◽

Group 1

Objectives: The aim of this in vitro study is to determine (1) shear bond strength (SBS) of brackets bonded with self-etch and total-etch adhesive after ozone treatment (2) bond failure interface using a modified Adhesive Remnant Index (ARI).Methods: 52 premolars were randomly assigned into four groups (n=13) and received the following treatments: Group 1: 30 s Ozone (Biozonix, Ozonytron, Vehos Medikal, Ankara, Turkey) application + Transbond Plus Self-Etching Primer (SEP) (3M) + Transbond XT (3M), Group 2: Transbond Plus SEP + Transbond XT, Group 3: 30 s Ozone application + 37% orthophosphoric acid + Transbond XT Primer (3M) + Transbond XT, Group 4: 37% orthophosphoric acid + Transbond XT Primer + Transbond XT. All samples were stored in deionised water at 37oC for 24 hours. Shear debonding test was performed by applying a vertical force to the base of the bracket at a cross-head speed of 1 mm/min.Results: The mean SBS results were Group 1: 10.48 MPa; Group 2: 8.89 MPa; Group 3: 9.41 MPa; Group 4: 9.82 MPa. One-Way Variance Test revealed that the difference between the groups was not statistically significant (P=0.267). Debonded brackets were examined by an optical microscope at X16 magnification to determine the bond failure interface using a modified ARI. The results were (mean) Group 1: 2.38; Group 2: 1.31; Group 3: 3.00; Group 4: 1.92. Multiple comparisons showed that Groups 1 and 2, 2 and 3, 3 and 4 were statistically different (P=0.014, P<.001 and P=0.025).Conclusions: Ozone treatment prior to bracket bonding does not affect the shear bond strength. (Eur J Dent 2010;4:367-373)

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