scholarly journals Performance of field‐scale lab vs in situ visible/near‐ and mid‐infrared spectroscopy for estimation of soil properties

Author(s):  
Isabel Greenberg ◽  
Michael Seidel ◽  
Michael Vohland ◽  
Bernard Ludwig
2020 ◽  
Vol 5 (9) ◽  
pp. 1642-1646
Author(s):  
Elyse N. T. DiMaso ◽  
Robert W. Bondi ◽  
John Guo ◽  
Alexander G. O'Brien

In-line Fourier transform mid-infrared spectroscopy (FTIR) in combination with a moving window t-test method was used to determine the endpoint of a reaction with a highly inconsistent rate.


2012 ◽  
Vol 66 (5) ◽  
pp. 574-579 ◽  
Author(s):  
Ian M. Clegg ◽  
Adrian M. Daly ◽  
Craig Donnelly ◽  
Ruth Hardy ◽  
Denise Harris ◽  
...  

The use of in situ mid-infrared spectroscopy to support the development of a pharmaceutical manufacturing process is disclosed. Data on this two-stage telescoped reaction from several reaction scales (<50 mL to 1600 liters) and at multiple manufacturing locations is shown. In addition to providing data on both reactions in the telescope, the mid-IR data has been used to monitor an intermediate distillation operation and therefore it has been possible to profile the whole process. Data is also shown on aliquot addition during the first chemical transformation, which is used to check the instrumentation.


2015 ◽  
Vol 33 (1) ◽  
pp. 99-106 ◽  
Author(s):  
Johana P. Bonett ◽  
Jesús H. Camacho-Tamayo ◽  
Leonardo Ramírez-López

Techniques such as mid-infrared (MIR) spectroscopy can be used to identify the classes and properties of soils with high preci-sion. In the present study, 312 soil samples of different orders, representative of Colombian agricultural zones, were studied, among which are found Inceptisols and Verisols of the Sinú valley (Córdoba), Andisols of the Eastern Andes Mountain range (Cundinamarca), and Oxisols of the Eastern plains of Colombian (Meta), with the aim of evaluating the ability of mid-infrared spectroscopy to estimate soil properties such as organic carbon, Ca, Mg, Na, K, P, Al, and pH. The results obtained through the analysis of the curves allowed observing that the greatest number of properties are reflected in the spectral region be-tween 400 and 850 cm<sup>-1</sup>. The Inceptisols and Vertisols gave the best results in the calibration of the models for the majority of the properties, followed by the Andisols and finally the Oxisols, which did not show good results. In the descriptive analysis, the observed values showed a behavior similar to the values predicted from the models, for those properties with representa-tive spectral models. The majority of the properties did not show a normal distribution, and the coefficients of variation were very high.


Author(s):  
David Conlon ◽  
J Christopher McWilliams ◽  
Robert Reamer ◽  
Bill Izzo ◽  
Paul Collins ◽  
...  

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