Analysis of a Bi-Harmonic Tapping Mode for Atomic Force Microscopy

Author(s):  
Muthukumaran Loganathan ◽  
Douglas A. Bristow

The tapping mode (TM) is a popularly used imaging mode in atomic force microscopy (AFM). A feedback loop regulates the amplitude of the tapping cantilever by adjusting the offset between the probe and sample; the image is generated from the control action. This paper explores the role of the trajectory of the tapping cantilever in the accuracy of the acquired image. This paper demonstrates that reshaping the cantilever trajectory alters the amplitude response to changes in surface topography, effectively altering the mechanical sensitivity of the instrument. Trajectory dynamics are analyzed to determine the effect on mechanical sensitivity and analysis of the feedback loop is used to determine the effect on image accuracy. Experimental results validate the analysis, demonstrating better than 30% improvement in mechanical sensitivity using certain trajectories. Images obtained using these trajectories exhibit improved sharpness and surface tracking, especially at high scan speeds.

1998 ◽  
Vol 66 (7) ◽  
pp. S283-S286 ◽  
Author(s):  
D. Sarid ◽  
J.P. Hunt ◽  
R.K. Workman ◽  
X. Yao ◽  
C.A. Peterson

Nanomaterials ◽  
2018 ◽  
Vol 8 (10) ◽  
pp. 807 ◽  
Author(s):  
Ashley Slattery ◽  
Cameron Shearer ◽  
Joseph Shapter ◽  
Adam Blanch ◽  
Jamie Quinton ◽  
...  

In this work PeakForce tapping (PFT) imaging was demonstrated with carbon nanotube atomic force microscopy (CNT-AFM) probes; this imaging mode shows great promise for providing simple, stable imaging with CNT-AFM probes, which can be difficult to apply. The PFT mode is used with CNT-AFM probes to demonstrate high resolution imaging on samples with features in the nanometre range, including a Nioprobe calibration sample and gold nanoparticles on silicon, in order to demonstrate the modes imaging effectiveness, and to also aid in determining the diameter of very thin CNT-AFM probes. In addition to stable operation, the PFT mode is shown to eliminate “ringing” artefacts that often affect CNT-AFM probes in tapping mode near steep vertical step edges. This will allow for the characterization of high aspect ratio structures using CNT-AFM probes, an exercise which has previously been challenging with the standard tapping mode.


Wear ◽  
2019 ◽  
Vol 418-419 ◽  
pp. 151-159 ◽  
Author(s):  
Juan F. Gonzalez-Martinez ◽  
Erum Kakar ◽  
Stefan Erkselius ◽  
Nicola Rehnberg ◽  
Javier Sotres

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