Heater Size Effect on Temperature Sensing With Wollaston Scanning Thermal Microprobes

Author(s):  
Liang Han ◽  
Yanliang Zhang ◽  
Theodorian Borca-Tasciuc

Scanning thermal microscopy (SThM) is an attractive tool for high spatial resolution thermal characterization with minimal sample preparation1. However, complex thermal contact mechanisms often hinder precise quantification of the sample temperature or thermal properties.2

Author(s):  
Yanliang Zhang ◽  
Liang Han ◽  
Theodorian Borca-Tasciuc

Scanning thermal microscopy (SThM) is an attractive tool for high spatial resolution thermal characterization with minimal sample preparation.1 SThM measurements are usually performed in contact-mode, which entails multiple tip-sample heat transfer pathways, i.e. across air gap, liquid meniscus, and the solid contact. These hinder the quantification of the sample temperature or thermal properties or result in large uncertainties.2


Nanomaterials ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 491
Author(s):  
Christoph Metzke ◽  
Fabian Kühnel ◽  
Jonas Weber ◽  
Günther Benstetter

New micro- and nanoscale devices require electrically isolating materials with specific thermal properties. One option to characterize these thermal properties is the atomic force microscopy (AFM)-based scanning thermal microscopy (SThM) technique. It enables qualitative mapping of local thermal conductivities of ultrathin films. To fully understand and correctly interpret the results of practical SThM measurements, it is essential to have detailed knowledge about the heat transfer process between the probe and the sample. However, little can be found in the literature so far. Therefore, this work focuses on theoretical SThM studies of ultrathin films with anisotropic thermal properties such as hexagonal boron nitride (h-BN) and compares the results with a bulk silicon (Si) sample. Energy fluxes from the probe to the sample between 0.6 µW and 126.8 µW are found for different cases with a tip radius of approximately 300 nm. A present thermal interface resistance (TIR) between bulk Si and ultrathin h-BN on top can fully suppress a further heat penetration. The time until heat propagation within the sample is stationary is found to be below 1 µs, which may justify higher tip velocities in practical SThM investigations of up to 20 µms−1. It is also demonstrated that there is almost no influence of convection and radiation, whereas a possible TIR between probe and sample must be considered.


Author(s):  
Anton O. Chernutsky ◽  
Dmitriy A. Dvoretskiy ◽  
Ilya O. Orekhov ◽  
Stanislav G. Sazonkin ◽  
Yan Zh. Ososkov ◽  
...  

1999 ◽  
Author(s):  
Princy L. Julian ◽  
Mahmoud Farhadiroushan ◽  
Vincent A. Handerek ◽  
Alan J. Rogers

2018 ◽  
Vol 3 (5) ◽  
pp. 505-516 ◽  
Author(s):  
Yifan Li ◽  
Nitin Mehra ◽  
Tuo Ji ◽  
Jiahua Zhu

Quantitative assessment of thermal properties by scanning thermal microscopy (SThM) is a demanded technology, but still not yet available due to the presence of unpredictable thermal contact resistance (TCR) at the tip/substrate interface.


Author(s):  
K. Przybylski ◽  
A. J. Garratt-Reed ◽  
G. J. Yurek

The addition of so-called “reactive” elements such as yttrium to alloys is known to enhance the protective nature of Cr2O3 or Al2O3 scales. However, the mechanism by which this enhancement is achieved remains unclear. An A.E.M. study has been performed of scales grown at 1000°C for 25 hr. in pure O2 on Co-45%Cr implanted at 70 keV with 2x1016 atoms/cm2 of yttrium. In the unoxidized alloys it was calculated that the maximum concentration of Y was 13.9 wt% at a depth of about 17 nm. SIMS results showed that in the scale the yttrium remained near the outer surface.


Author(s):  
E. G. Rightor

Core edge spectroscopy methods are versatile tools for investigating a wide variety of materials. They can be used to probe the electronic states of materials in bulk solids, on surfaces, or in the gas phase. This family of methods involves promoting an inner shell (core) electron to an excited state and recording either the primary excitation or secondary decay of the excited state. The techniques are complimentary and have different strengths and limitations for studying challenging aspects of materials. The need to identify components in polymers or polymer blends at high spatial resolution has driven development, application, and integration of results from several of these methods.


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