Electron spectroscopy as applied to the layer-by-layer analysis of hydrocarbon coatings produced by ion-plasma deposition

Author(s):  
V. P. Afanas’ev ◽  
A. N. Ermilov ◽  
I. A. Kostanovsky ◽  
P. M. Tyuryukanov ◽  
A. V. Lubenchenko ◽  
...  
2019 ◽  
Vol 946 ◽  
pp. 174-180
Author(s):  
Olga M. Kanunnikova ◽  
O.Yu. Goncharov ◽  
V.I. Ladyanov

The complex approach based on the combination of methods of equilibrium thermodynamics and x-ray electron spectroscopy for layer-by-layer analysis of the composition of surface layers of amorphous alloys is described on the example of Fe-Si-B-Nb-Cu alloy.


1984 ◽  
Vol 140 (1) ◽  
pp. L253-L258
Author(s):  
Kenji Murakami ◽  
Toshiyuki Adachi ◽  
Tsukasa Kuroda ◽  
Shogo Nakamura

2021 ◽  
Vol 56 ◽  
pp. 97-107
Author(s):  
M. S. Zayats ◽  

A low-temperature (substrate heating temperature up to 400 °C) ion-plasma technology for the formation of nanostructured AlN and BN films by the method of high-frequency reactive magnetron sputtering of the corresponding targets has been developed (the modernized installation "Cathode-1M"), which has in its technological cycle the means of physical and chemical modification, which allow to purposefully control the phase composition, surface morphology, size and texture of nanocrystalline films. The possibility of using the method of high-frequency magnetron sputtering for deposition of transparent hexagonal BN films in the nanoscale state on quartz and silicon substrates is shown. Atomic force microscopy (AFM) has shown that AlN films can have an amorphous or polycrystalline surface with grain sizes of approximately 20-100 nm, with the height of the nanoparticles varying from 3 to 10 nm and the degree of surface roughness from 1 to 10 nm. It was found that the dielectric penetration of polycrystalline AlN films decreases from 10 to 3.5 at increased frequencies from 25 Hz to 1 MHz, and the peak tangent of the dielectric loss angle reaches 0.2 at 10 kHz. Such features indicate the existence of spontaneous polarization of dipoles in the obtained AlN films. Interest in dielectric properties in AlN / Si structures it is also due to the fact that there are point defects, such as nitrogen vacancies and silicon atoms, which diffuse from the silicon substrate during synthesis and play an important role in the dielectric properties of AlN during the formation of dipoles. The technology makes it possible, in a single technological cycle, to produce multilayer structures modified for specific functional tasks with specified characteristics necessary for the manufacture of modern electronics, optoelectronics and sensorics devices. It should also be noted that the technology of magnetron sputtering (installation "Cathode-1M") is highly productive, energetically efficient and environmentally friendly in comparison with other known technologies for creating semiconductor structures and allows them to be obtained with minimal changes in the technological cycle.


1994 ◽  
Vol 3 (1-2) ◽  
pp. 61-65 ◽  
Author(s):  
N.V. Novikov ◽  
M.A. Voronkin ◽  
I.V. Bondar
Keyword(s):  

2014 ◽  
Vol 1013 ◽  
pp. 127-132 ◽  
Author(s):  
Victor Gromov ◽  
Alexei Yuriev ◽  
Yurii F. Ivanov ◽  
Konstantin Morozov ◽  
Sergey Konovalov ◽  
...  

Using transmission electron microscopy methods the layer by layer analysis of the bulk hardened superior quality rails is carried out and the quantitative parameters of structure, phase state and defect substructure gradients are established. It is shown that the interface boundaries globular cementite particles-matrix are the possible places of microcracks initiation.


2018 ◽  
Vol 52 (2) ◽  
pp. 184-188 ◽  
Author(s):  
Ya. V. Lubyanskiy ◽  
A. D. Bondarev ◽  
I. P. Soshnikov ◽  
N. A. Bert ◽  
V. V. Zolotarev ◽  
...  

2019 ◽  
Vol 61 (7) ◽  
pp. 1223-1227 ◽  
Author(s):  
V. A. Vol’pyas ◽  
A. B. Kozyrev ◽  
A. V. Tumarkin ◽  
D. M. Dolgintsev ◽  
V. P. Pronin ◽  
...  

2005 ◽  
Vol 495-497 ◽  
pp. 687-692
Author(s):  
Yuriy Perlovich ◽  
M. Grekhov ◽  
Margarita Isaenkova ◽  
Vladimir Fesenko ◽  
B. Kalin ◽  
...  

Irradiation of metal materials with low-energy ions is accompanied by the long-range effect, consisting in distinct texture and structure changes at the depth, exceeding, at least, by 104 times the thickness of the layer of ion retardation. In order to ascertain mechanisms of this effect, a layer-by-layer X-ray study was carried out as applied to ion-plasma treated cladding tubes of Zr- 1%Nb alloy for nuclear reactors. Impacts of pulse treatments with helium plasma by two different regimes and the ion energy of ~ 1 keV were compared. It was found, that only by minimal surface melting the ion-plasma treatment causes unpredictable bulk texture changes, consisting in arising of the axial texture component. The melted surface layer suppresses shock waves, associated with braking of ions and supposedly responsible for stimulation of dislocation processes at long distances from the surface.


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