A Selective Determination of the Proton Nuclear Relaxation Times of the Alkaloid Vindoline
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An audiofrequency-pulse n.m.r. spectrometer has been used to measure the nuclear relaxation times of individual protons of the alkaloid, vindoline. For this substance in deuterochloroform solution the spin–lattice relaxation times (T1) vary between 1.15 and 1.50 s and the spin–spin relaxation times (T2) are between 0.90 and 1.40 s. The N-methyl group has the shortest relaxation time of those resonances which were measured. A discussion of the apparatus and methodology is given.
1970 ◽
Vol 2
(2)
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pp. 174-180
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2009 ◽
Vol 149
(39-40)
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pp. 1702-1705
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1989 ◽
Vol 12
(2)
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pp. 209-218
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1971 ◽
Vol 32
(C1)
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pp. C1-513-C1-515
1966 ◽
Vol 21
(3)
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pp. 296-300
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2007 ◽
Vol 46
(15)
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pp. 5122-5130
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