STUDY OF THE PUREPECHA METALS BY PIXE AND METALLOGRAPHY TECHNIQUES

2006 ◽  
Vol 16 (01n02) ◽  
pp. 137-143 ◽  
Author(s):  
U. MÉNDEZ ◽  
D. TENORIO ◽  
G. MURILLO ◽  
B. MÉNDEZ-GARRIDO ◽  
LUIS C. LONGORIA ◽  
...  
Keyword(s):  
Elemental Analysis ◽  
X Ray ◽  
Suitable Technique ◽  
Metallic Artifacts

Proton-Induced-X-Ray-Emission (PIXE) is a suitable technique for the elemental analysis of ancient metallic artifacts, without any deterioration of the samples. Metallography was used to determine the manufacture technique of ancient metallic artifacts. These techniques were applied to study 12 copper artifacts collected, from burial offerings of a "Señor Tarasco", discovered by Eduardo Pareyon, in "El Portal de Matamoros", Uruapan, Michoacán, in 1957.

Signal/Noise Ratio and Elemental Detectivity by Eels

1982 ◽  
Vol 40 ◽  
pp. 488-489
Author(s):  
R. F. Egerton
Keyword(s):  
Energy Loss ◽  
Electron Energy ◽  
Elemental Analysis ◽  
Electron Energy Loss Spectroscopy ◽  
Emission Spectroscopy ◽  
X Ray ◽  
Signal Noise ◽  
Characteristic Signal ◽  
Noise Ratio ◽  
Electron Energy Loss

An important parameter governing the sensitivity and accuracy of elemental analysis by electron energy-loss spectroscopy (EELS) or by X-ray emission spectroscopy is the signal/noise ratio of the characteristic signal.

scholarly journals 4-vinylpyridine derivatives: Protonation, methylation and silver(I) coordination chemistry

2021 ◽  
pp. 174751982198965
Author(s):  
Guoqi Zhang
Keyword(s):  
Mass Spectrometry ◽  
Schiff Base ◽  
Coordination Chemistry ◽  
Elemental Analysis ◽  
Silver Complex ◽  
Spectroscopic Techniques ◽  
X Ray ◽  
X Ray Crystallography ◽  
Pyridine Moiety ◽  
New Compounds

( E)-4-[2-(Pyridin-4-yl)vinyl]benzaldehyde, containing both a 4-vinylpyridine and an aldehyde functionality, is utilized to develop new, highly conjugated chalcone compounds and a bis-Schiff base azine compound. The chalcone-containing compounds are further explored for their protonation, methylation and silver(I) coordination chemistry using the pyridine moiety. In parallel, a cyano-containing analogue, ( E)-4-[2-(pyridin-4-yl)vinyl]benzonitrile is also synthesized and studied for its silver(I) coordination chemistry. These new compounds are fully characterized by mass spectrometry, elemental analysis and spectroscopic techniques. The methylated product of ( E)-1-(9-anthryl)-3-{4-[2-(pyridin-4-yl)vinyl]phenyl}prop-2-en-1-one and a silver complex of ( E)-4-[2-(pyridin-4-yl)vinyl]benzonitrile are structurally determined by X-ray crystallography.

scholarly journals Modular MA-XRF Scanner Development in the Multi-Analytical Characterisation of a 17th Century Azulejo from Portugal

Sensors ◽  
2021 ◽  
Vol 21 (5) ◽  
pp. 1913
Author(s):  
Sergio Augusto Barcellos Lins ◽  
Marta Manso ◽  
Pedro Augusto Barcellos Lins ◽  
Antonio Brunetti ◽  
Armida Sodo ◽  
...  
Keyword(s):  
Monte Carlo ◽  
Monte Carlo Simulations ◽  
17Th Century ◽  
Scanning System ◽  
X Ray ◽  
Portable Instruments ◽  
Complementary Techniques ◽  
Non Destructive ◽  
Suitable Technique ◽  
Cobalt Blue

A modular X-ray scanning system was developed, to fill in the gap between portable instruments (with a limited analytical area) and mobile instruments (with large analytical areas, and sometimes bulky and difficult to transport). The scanner has been compared to a commercial tabletop instrument, by analysing a Portuguese tile (azulejo) from the 17th century. Complementary techniques were used to achieve a throughout characterisation of the sample in a complete non-destructive approach. The complexity of the acquired X-ray fluorescence (XRF) spectra, due to inherent sample stratigraphy, has been resolved using Monte Carlo simulations, and Raman spectroscopy, as the most suitable technique to complement the analysis of azulejos colours, yielding satisfactory results. The colouring agents were identified as cobalt blue and a Zn-modified Naples-yellow. The stratigraphy of the area under study was partially modelled with Monte Carlo simulations. The scanners performance has been compared by evaluating the images outputs and the global spectrum.

Cobalt(II) Mercury Tetrathiocyanate Complexes with Lewis Bases

1973 ◽  
Vol 51 (3) ◽  
pp. 438-447 ◽  
Author(s):  
R. Makhija ◽  
L. Pazdernik ◽  
R. Rivest
Keyword(s):  
Magnetic Susceptibility ◽  
Powder Diffraction ◽  
Elemental Analysis ◽  
Far Infrared ◽  
Crystalline Solid ◽  
Ultraviolet Spectroscopy ◽  
X Ray ◽  
Lewis Bases ◽  
Polydentate Ligands

A new series of octahedral cobalt(II) complexes are formed when CoX2(X = Cl, Br, I, SCN) reacts with Hg(SCN)2 in the presence of Lewis bases. These complexes of stoichiometry CoHg(SCN)4•2L (L = THF, dioxane, pyridine, aniline) are pink to violet solids which slowly decompose to the blue crystalline solid, CoHg(SCN)4, the stable magnetic susceptibility standard. On further reaction of CoHg(SCN)4•2THF with mono-, bi-, and polydentate ligands in dry ethanol, complexes of the following types are obtained: CoHg(SCN)4•2L (L = PΦ3), CoHg(SCN)4•2LL (LL = trien), CoHg(SCN)4•3LL (LL = en, bipy), and CoHg(SCN)4•4LL (LL = phen). The stoichiometry of these were determined by elemental analysis. Possible structures of these are discussed with the help of mid and far infrared, visible, and ultraviolet spectroscopy, magnetic susceptibility, and X-ray powder diffraction. Some new i.r. bands like Co—P, Co—N, and Hg—S are assigned in the low region.

A new cockroach (Blattaria: Caloblattinidae) from the Upper Triassic Xujiahe Formation of Sichuan Province, southwestern China

2013 ◽  
Vol 44 (2) ◽  
pp. 167-174
Author(s):  
Yan Fang ◽  
Haichun Zhang ◽  
Bo Wang ◽  
Daran Zheng
Keyword(s):  
Elemental Analysis ◽  
Anterior Margin ◽  
New Genus ◽  
Sichuan Province ◽  
Upper Triassic ◽  
Southwestern China ◽  
New Taxon ◽  
New Genus And Species ◽  
X Ray ◽  
Xujiahe Formation

A new genus and species of the cockroach family Caloblattinidae, Dazhublattella lini gen. et sp.n., is described from the Upper Triassic Xujiahe Formation of Sichuan Province, in southwestern China. The new taxon is similar to the Triassic Caloblattina mathildae (Geinitz, 1883) (Vršanský & Ansorge 2007) in the venation and pattern, but differs in the less elongated forewing with arched anterior margin. An elemental analysis of the wing is undertaken using Energy Dispersive X-ray analysis.

Elemental analysis of soluble and insoluble fractions of rain and surface waters by particle-induced x-ray emission

1981 ◽  
Vol 15 (3) ◽  
pp. 354-357 ◽  
Author(s):  
Shigeru. Tanaka ◽  
Michael. Darzi ◽  
John W. Winchester
Keyword(s):  
Elemental Analysis ◽  
Surface Waters ◽  
X Ray

Evaluation of X-ray microfluorescence spectrometry for the elemental analysis of firearm discharge residues

1998 ◽  
Vol 97 (1) ◽  
pp. 21-36 ◽  
Author(s):  
Joanne Flynn ◽  
Milutin Stoilovic ◽  
Chris Lennard ◽  
Ian Prior ◽  
Hilton Kobus
Keyword(s):  
Elemental Analysis ◽  
X Ray

An Intramolecular Boron Nitrogen Lewis Acid Base Pair on a Rigid Naphthyl Backbone

2012 ◽  
Vol 67 (6) ◽  
pp. 589-593 ◽  
Author(s):  
Daniel Winkelhaus ◽  
Beate Neumann ◽  
Norbert W. Mitzel
Keyword(s):  
Nmr Spectroscopy ◽  
Single Crystal ◽  
Lewis Acid ◽  
Elemental Analysis ◽  
Base Pair ◽  
Ring System ◽  
X Ray Diffraction ◽  
Acid Base ◽  
X Ray ◽  
Boron Nitrogen

The reaction of (C6F5)2BCl with 8-lithio-N,N-dimethyl-1-naphthylamine (1) afforded the fivemembered ring system 8-bis(pentafluorophenyl)boryl-N,N-dimethyl-1-naphthylamine (2) with an intramolecular dative B-N bond. The compound was characterised by elemental analysis, NMR spectroscopy and single-crystal X-ray diffraction.

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