scholarly journals Effect of MDP-Based Primers on the Luting Agent Bond to Y-TZP Ceramic and to Dentin

2018 ◽  
Vol 2018 ◽  
pp. 1-6
Author(s):  
Sheila Butler ◽  
Bernie Linke ◽  
Ysidora Torrealba
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Tetragonal Zirconia ◽  
Silica Particles ◽  
Resin Cement ◽  
Ceramic Surface ◽  
Universal Adhesive ◽  
Luting Agent ◽  
Post Hoc ◽  
Application Protocols

Purpose. The aim of this study was to evaluate the influence of multimode MDP-based primers and different application protocols on the bond strength of a representative resin cement to an yttrium stabilized tetragonal zirconia (Y-TZP) ceramic.Materials and Methods. The occlusal dentin from 60 human molars was exposed. The teeth and zirconia cylinders (N = 60) (3 mm of diameter; 4 mm of height) were divided into six groups (n = 10) according to the ceramic surface conditioning: (1) air abraded with SiO2particles; (2) Z-Prime Plus; (3) air abraded with SiO2particles + Z-Prime Plus; (4) air abraded with SiO2particles + All-Bond Universal; (5) air abraded with SiO2particles + ScotchBond Universal Adhesive; and (6) untreated zirconia. The luting agent (Duo-Link cement) was applied on the treated dentin surface. Specimens were stored in water (37°C, 24 h) and tested in shear bond strength. Data were statistically analyzed using 2-way ANOVA and Post hoc Tukey tests (α= 0.05).Results. Significant effects of ceramic conditioning were found (p<0.0001). The specimens sandblasted with silica particles followed by the application of Z-Prime Plus or All-Bond Universal presented greater bond strength values. For the untreated zirconia, several specimens failed prematurely prior to testing.Conclusions. Sandblasting with silica particles combined with Z-Prime Plus increased the bond strength.

scholarly journals Influence of Etching Protocol and Silane Treatment with a Universal Adhesive on Lithium Disilicate Bond Strength

2015 ◽  
Vol 40 (4) ◽  
pp. 372-378 ◽  
Author(s):  
VK Kalavacharla ◽  
NC Lawson ◽  
LC Ramp ◽  
JO Burgess
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Lithium Disilicate ◽  
Ceramic Surface ◽  
Silane Treatment ◽  
Universal Adhesive ◽  
Plastic Tube ◽  
C 50 ◽  
Post Hoc

SUMMARY Objectives To measure the effects of hydrofluoric acid (HF) etching and silane prior to the application of a universal adhesive on the bond strength between lithium disilicate and a resin. Methods and Materials Sixty blocks of lithium disilicate (e.max CAD, Ivoclar Vivadent) were sectioned into coupons and polished. Specimens were divided into six groups (n=10) based on surface pretreatments, as follows: 1) no treatment (control); 2) 5% HF etch for 20 seconds (5HF); 3) 9.5% HF etch for 60 seconds (9.5HF); 4) silane with no HF (S); 5) 5% HF for 20 seconds + silane (5HFS); and 6) 9.5% HF for 60 seconds + silane (9.5HFS). All etching was followed by rinsing, and all silane was applied in one coat for 20 seconds and then dried. The universal adhesive (Scotchbond Universal, 3M ESPE) was applied onto the pretreated ceramic surface, air thinned, and light cured for 10 seconds. A 1.5-mm-diameter plastic tube filled with Z100 composite (3M ESPE) was applied over the bonded ceramic surface and light cured for 20 seconds on all four sides. The specimens were thermocycled for 10,000 cycles (5°C-50°C/15 s dwell time). Specimens were loaded until failure using a universal testing machine at a crosshead speed of 1 mm/min. The peak failure load was used to calculate the shear bond strength. Scanning electron microscopy images were taken of representative e.max specimens from each group. Results A two-way analysis of variance (ANOVA) determined that there were significant differences between HF etching, silane treatment, and the interaction between HF and silane treatment (p&lt;0.01). Silane treatment provided higher shear bond strength regardless of the use or concentration of the HF etchant. Individual one-way ANOVA and Tukey post hoc analyses were performed for each silane group. Shear bond strength values for each etch time were significantly different (p&lt;0.01) and could be divided into significantly different groups based on silane treatment: no silane treatment: 0 HF &lt; 5% HF &lt; 9.5% HF; and RelyX silane treatment: 0 HF &lt; 5% HF and 9.5% HF. Conclusions Both HF and silane treatment significantly improved the bond strength between resin and lithium disilicate when used with a universal adhesive.

Influence of Glazed Zirconia on Dual-Cure Luting Agent Bond Strength

2012 ◽  
Vol 37 (2) ◽  
pp. 181-187 ◽  
Author(s):  
TA Valentino ◽  
GA Borges ◽  
LH Borges ◽  
JA Platt ◽  
L Correr-Sobrinho
Keyword(s):  
Bond Strength ◽  
Clinical Relevance ◽  
Tetragonal Zirconia ◽  
Resin Cement ◽  
Zirconia Ceramic ◽  
Ceramic Surface ◽  
Luting Agent ◽  
Ceramic Surfaces

Clinical Relevance Treatment of yttrium-stabilized tetragonal zirconia ceramic surfaces with a low-fusing porcelain layer as a glaze significantly increased the bond strength of dual-cure resin cement to the ceramic surface.

Ceramic Primer Heat-Treatment Effect on Resin Cement/Y-TZP Bond Strength

2012 ◽  
Vol 37 (6) ◽  
pp. 634-640 ◽  
Author(s):  
LH Silva ◽  
AKF Costa ◽  
JRC Queiroz ◽  
MA Bottino ◽  
LF Valandro
Keyword(s):  
Heat Treatment ◽  
Bond Strength ◽  
Shear Bond Strength ◽  
Tetragonal Zirconia ◽  
Resin Cement ◽  
Dihydrogen Phosphate ◽  
Gravimetric Analysis ◽  
Ceramic Surface ◽  
Aging Condition ◽  
Experimental Group

SUMMARY The purpose of this study was to evaluate the effect of different heat-treatment strategies for a ceramic primer on the shear bond strength of a 10-methacryloyloxydecyl-dihydrogen-phosphate (MDP)-based resin cement to a yttrium-stabilized tetragonal zirconia polycrystal (Y-TZP) ceramic. Specimens measuring 4.5 × 3.5 × 4.5 mm3 were produced from Y-TZP presintered cubes and embedded in polymethyl methacrylate (PMMA). Following finishing, the specimens were cleaned using an ultrasound device and distilled water and randomly divided into 10 experimental groups (n=14) according to the heat treatment of the ceramic primer and aging condition. The strategies used for the experimental groups were: GC (control), without primer; G20, primer application at ambient temperature (20°C); G45, primer application + heat treatment at 45°C; G79, primer application + heat treatment at 79°C; and G100, primer application + heat treatment at 100°C. The specimens from the aging groups were submitted to thermal cycling (6000 cycles, 5°C/55°C, 30 seconds per bath) after 24 hours. A cylinder of MDP-based resin cement (2.4 mm in diameter) was constructed on the ceramic surface of the specimens of each experimental group and stored for 24 hours at 37°C. The specimens were submitted to a shear bond strength test (n=14). Thermal gravimetric analysis was performed on the ceramic primer. The data obtained were statistically analyzed by two-way analysis of variance and the Tukey test (α=0.05). The experimental group G79 without aging (7.23 ± 2.87 MPa) presented a significantly higher mean than the other experimental groups without aging (GC: 2.81 ± 1.5 MPa; G20: 3.38 ± 2.21 MPa; G100: 3.96 ± 1.57 MPa), showing no difference from G45 only (G45: 6 ± 3.63 MPa). All specimens of the aging groups debonded during thermocycling and were considered to present zero bond strength for the statistical analyses. In conclusion, heat treatment of the metal/zirconia primer improved bond strength under the initial condition but did not promote stable bonding under the aging condition.

scholarly journals Effects of Universal Adhesive on Shear Bond Strength of Resin Cement to Zirconia Ceramic with Different Surface Treatments

2021 ◽  
Vol 2021 ◽  
pp. 1-6
Author(s):  
Zohreh Moradi ◽  
Farnoosh Akbari ◽  
Sara Valizadeh
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
In Vitro Study ◽  
Surface Treatments ◽  
Resin Cement ◽  
Zirconia Ceramic ◽  
Single Bond ◽  
Universal Adhesive

Aim. This study aimed to assess shear bond strength (SBS) of resin cement to zirconia ceramic with different surface treatments by using Single Bond Universal. Methods. In this in vitro study, 50 zirconia discs (2 × 6 mm) were divided into 5 groups of (I) sandblasting with silica-coated alumina (CoJet)  + silane + Single Bond 2, (II) sandblasting with CoJet + Single Bond Universal, (III) sandblasting with alumina + Single Bond Universal, (IV) sandblasting with alumina + Z-Prime Plus, and (V) Single Bond Universal with no surface treatment. Resin cement was applied in plastic tubes (3 × 5 mm2), and after 10,000 thermal cycles, the SBS was measured by a universal testing machine. The mode of failure was determined under a stereomicroscope at × 40 magnification. Data were analyzed using one-way ANOVA. Results. The maximum (6.56 ± 4.29 MPa) and minimum (1.94 ± 1.96 MPa) SBS values were noted in groups III and I, respectively. Group III had the highest frequency of mixed failure (60%). Group V had the maximum frequency of adhesive failure (100%). Conclusion. Single Bond Universal + sandblasting with alumina or silica-coated alumina particles is an acceptable method to provide a strong SBS between resin cement and zirconia.

scholarly journals Effect of Acid Etching, Silane and Thermal Cycling on the Bond Strength of Metallic Brackets to Ceramic

2016 ◽  
Vol 27 (6) ◽  
pp. 734-738 ◽  
Author(s):  
Natália Regina Santos de Matos ◽  
Ana Rosa Costa ◽  
Heloísa Cristina Valdrighi ◽  
Américo Bortolazzo Correr ◽  
Silvia Amélia Vedovello ◽  
...  
Keyword(s):  
Bond Strength ◽  
Thermal Cycling ◽  
Surface Treatment ◽  
Hydrofluoric Acid ◽  
Shear Bond Strength ◽  
Deionized Water ◽  
Acid Etching ◽  
Ceramic Surface ◽  
Adhesive Remnant Index ◽  
Post Hoc

Abstract The aim of this study was to evaluate the effect of silanes, thermal cycling and acid etching on the shear bond strength (SBS) of metallic brackets to feldspathic ceramic. Feldspathic ceramic cylinders (Groups 1, 2, 5 and 6) were etched for 60 s with 10% hydrofluoric acid and Groups 3, 4, 7 and 8, without acid etching. Two layers of silane Clearfil Ceramic Primer (CCP, Groups 1 to 4) and two layers of RelyX Ceramic Primer (RCP, groups 5 to 8) were applied and dried for 60 s. Brackets were bonded to the cylinders with Transbond XT and light-activated for 40 s with Bluephase G2. All specimens were stored in deionized water at 37 °C for 24 h, and the specimens of groups 1, 3, 5 and 7 were submitted to 7,000 thermal cycles (5 °C/55 °C). After storage, the SBS test was performed at a crosshead speed of 1 mm/min. Data were subjected to three-way ANOVA and Tukey's post hoc test (α=0.05). The adhesive remnant index (ARI) was evaluated at 8x magnification. The SBS of CCP was significantly greater than of RCP (p<0.05), with or without thermal cycling. Thermal cycling significantly reduced the SBS (p<0.05). The groups submitted to acid etching showed significantly higher SBS than those without acid etching (p<0.05). In conclusion, thermal cycling reduced SBS for all groups. The best ceramic surface treatment for bracket bonding was achieved by acid etching and CCP silane. The ARI results showed predominance of score 0 for all groups.

scholarly journals Effect of Ceramic Surface Treatment and Adhesive Systems on Bond Strength of Metallic Brackets

2020 ◽  
Vol 2020 ◽  
pp. 1-8
Author(s):  
Patrapan Juntavee ◽  
Hattanas Kumchai ◽  
Niwut Juntavee ◽  
Dan Nathanson
Keyword(s):  
Bond Strength ◽  
Surface Treatment ◽  
Damage Index ◽  
Resin Cement ◽  
Ceramic Surface ◽  
Adhesive Remnant Index ◽  
Chi Squared ◽  
Ceramic Bracket ◽  
Bonding Systems ◽  
Post Hoc

Objective. This study evaluated the effect of ceramic surface treatments on bond strength of metal brackets to machinable ceramics and veneering porcelain using different adhesive resins. Materials and methods. Machined ceramic specimens (10 × 10 × 2 mm) were prepared from Vitablocs mark II (Vita) and IPS e.max® CAD (Ivoclar). Layered porcelain fused to metal (IPS d.Sign®, Ivoclar) was used to fabricate PFM specimens (n = 60/group). Half of specimens were etched (9.6% HF, 15 sec), and the rest were nonetched. Three resin bonding systems were used for attaching metal brackets (Victory series™ APC II, 3M) to each group (n = 10): Transbond™ XT (3M), Light Bond™ (Reliance), or Blugloo™ (Ormco), all cured with LED curing unit (Bluephase G1600, Vivadent) for 50 s each. Specimens were immersed in deionized water at 37°C for 24 hours prior to shear bond testing (Instron) at crosshead speed of 0.5 mm/min. Debond surface of ceramic and bracket base was examined for failure mode (FM), Ceramic Damage Index (CDI), and Adhesive Remnant Index (ARI). ANOVA and post hoc multiple comparisons were used to analyze the differences in bond strength. The chi-squared test was used to determine significance effect of FM, CDI, and ARI. Results. Significant differences in shear bond strength among group were found (p≤0.05) related to ceramic, surface treatment, and resin cement. Conclusion. Bond strength of bracket to ceramic is affected by type of ceramic, resin cement, and ceramic surface conditioning. Etching ceramic surface enhanced ceramic-bracket bond strength. However, bond strengths in nontreated ceramic surface groups were still higher than bond strength required for bonding in orthodontic treatment.

scholarly journals Influence of different treatments of the ceramic surface and thermal cycling on the bond strength of brackets to ceramic

2017 ◽  
Vol 46 (3) ◽  
pp. 179-183
Author(s):  
Fernando Guerra SÁEZ ◽  
Ana Rosa COSTA ◽  
Adriana Simoni LUCATO ◽  
Ana Paula Terossi de GODOI ◽  
Lourenço CORRER-SOBRINHO ◽  
...  
Keyword(s):  
Bond Strength ◽  
Thermal Cycling ◽  
Hydrofluoric Acid ◽  
Shear Bond Strength ◽  
Deionized Water ◽  
Acid Etching ◽  
Ceramic Surface ◽  
Thermal Cycler ◽  
Post Hoc

Abstract Objective To evaluate in vitro the effect of different treatments of the ceramic surface and thermal cycling on the shear bond strength (SBS) of metallic brackets bonded to feldspathic ceramic. Material and method Ceramic cylinders were divided into four groups (n=4) according to the treatment of ceramic surface: G1-Clearfil Ceramic Primer silane and Transbond XT (CCPT); G2-etched with 10% hydrofluoric acid (HFA) for 60 s, CCP and Transbond XT (ACCPT); G3-etched with 10% HFA for 60 s, Ambar Adhesive and Transbond XT (AAAT); and, G4 - etched with 10% HFA for 60 s, RelyX Ceramic Primer silane -RCP, adhesive primer Transbond and Transbond XT (ACPPT). Brackets were bonded to the cylinders with Transbond XT and light-activated for 40 s with LED Radii Plus. All specimens were stored in deionized water at 37 °C for 24 h, and two cylinders from each group were subject to 7,000 thermal cycles in a thermal cycler (5 °C/55 °C). After storage and thermal cycling, the SBS test was performed at a crosshead speed of 1 mm/min. Data were subjected to two-way ANOVA and Tukey’s post hoc test (α=0.05). Result The SBS of ACCPT was significantly higher than the other groups (p<0.05). The specimens submitted to thermal cycling showed significantly lower SBS than those without thermal cycling (p<0.05), regardless the ceramic surface treatment. The ARI showed predominance of score 0 for all groups. Conclusion Acid etching, CCP silane and Transbond XT method obtained the best results for bracket bonding. Thermal cycling reduced SBS for all groups. Score 0 was predominant for ARI in all groups.

scholarly journals Influence of adhesive and bonding material on the bond strength of bracket to bovine tooth

2017 ◽  
Vol 16 ◽  
pp. 1-7
Author(s):  
Bruna Lorena dos Santos Oliveira ◽  
Ana Rosa Costa ◽  
Américo Bortolazzo Correr ◽  
Marcus Vinicius Crepaldi ◽  
Lourenço Correr-Sobrinho ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Acrylic Resin ◽  
Single Bond ◽  
Universal Adhesive ◽  
Bonding Material ◽  
Significant Difference ◽  
Post Hoc ◽  
Group 1

Aim: To evaluate, in vitro, the effect of adhesive and bonding materials on the shear bond strength (SBS) of metallic brackets bonded to bovine teeth. Methods: Bovine teeth were embedded with acrylic resin, etched with 35% phosphoric acid for 20 s, rinsed, dried for 20 s and divided into 8 groups (n=20), according to the bonding materials and adhesive: Groups 1 and 5 – Transbond XT; Groups 2 and 6 – Fill Magic; Groups 3 and 7 – Biofix; and, Groups 4 and 8 – Orthocem. One layer of adhesive 3 M Unitek (Group 1), and one layer of Single Bond Universal Adhesive (Groups 2, 3 and 4) were applied and light-cured with LED for 10 s. Brackets were bonded to the buccal surface with four bonding materials and light-cured with LED for 40 s. SBS was carried out after 24 h and thermocycling (7,000 cycles - 5°/55 °C). Data were submitted to two way ANOVA and Tukey’s post hoc test (α=0.05). The Adhesive Remaining Index (ARI) was evaluated at 8×. Results: The adhesive was effective in increasing the SBS for all bonding materials (p<0.05). Significant difference (p<0.05) on the SBS was observed between bonding materials with or without adhesive. The ARI showed a predominance of scores 0 for all groups. Conclusions: The adhesive improved significantly the SBS of the brackets to teeth. Different SBS values occurred among the bonding materials. ARI index showed predominance of score 0 for all groups.

Bonding Polycrystalline Zirconia With 10-MDP–containing Adhesives

2017 ◽  
Vol 42 (3) ◽  
pp. 335-341 ◽  
Author(s):  
AE Llerena-Icochea ◽  
RM Costa ◽  
AFS Borges ◽  
JFS Bombonatti ◽  
AY Furuse
Keyword(s):  
Bisphenol A ◽  
Bond Strength ◽  
Shear Bond Strength ◽  
Failure Modes ◽  
Tetragonal Zirconia ◽  
Resin Cement ◽  
Dihydrogen Phosphate ◽  
Single Bond ◽  
Glycol Dimethacrylate ◽  
Significant Difference

SUMMARY Objective: The objective of this study was to evaluate the influence of adhesives with different 10-MDP concentrations on the shear bond strength of a resin cement to zirconia. Methods and Materials: Six experimental adhesives were prepared with the following composition: camphorquinone, 1,2-diaminobenzene, butylhydroxytoluene, diphenyliodonium hexafluorophosphate, 2-hydroxyethyl methacrylate triethylene glycol dimethacrylate, ethoxylated bisphenol A glycol dimethacrylate, urethane dimethacrylate, bisphenol A diglycidyl methacrylate, and ethanol. The 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP) monomer was added at 0wt%, 3wt%, 6wt%, 9wt%, 12wt%, or 15wt%. Three commercially available adhesives were evaluated: Single Bond Universal, Single Bond 2, and Signum Zirconia Bond. Resin cement cylinders made with RelyX Ultimate were bonded to yttria-stabilized tetragonal zirconia polycrystal with one of the evaluated adhesives and were subjected to the shear bond strength evaluation. Failure modes were analyzed with a stereoscopic loupe. Statistical analyses were performed with one-way analysis of variance and the Tukey's Honestly Significant Difference test (α=0.05). Pearson's was used to correlate the percentage of 10-MDP in the experimental adhesives and shear bond strength. Results: There were significant differences between adhesives (p&lt;0.00001). The highest shear bond strength values were obtained with the Signum Zirconia Bond and Single Bond Universal. Single Bond 2 showed the lowest values. There were no differences between experimental adhesives. All groups showed adhesives failures. A nonlinear correlation was found between bond strength and percentage of 10-MDP in experimental adhesives (r=0.872). Conclusions: The commercially available adhesives indicated for bonding to zirconia showed the highest bonding values.

The Effect of Sandblasting and Different Primers on Shear Bond Strength Between Yttria-tetragonal Zirconia Polycrystal Ceramic and a Self-adhesive Resin Cement

2015 ◽  
Vol 40 (1) ◽  
pp. 63-71 ◽  
Author(s):  
Y-A Yi ◽  
J-S Ahn ◽  
Y-J Park ◽  
S-H Jun ◽  
I-B Lee ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Tetragonal Zirconia ◽  
Xrd Analysis ◽  
Resin Cement ◽  
Air Abrasion ◽  
Adhesive Resin ◽  
Multiple Comparison Test ◽  
Adhesive Resin Cement ◽  
Tetragonal Zirconia Polycrystal

SUMMARY Purpose To evaluate the effect of zirconia primers, air-abrasion, and tribochemical surface treatment methods on the shear bond strength between yttria-tetragonal zirconia polycrystal (Y-TZP) ceramic and self-adhesive resin cement. Methods and Materials Y-TZP ceramic surfaces were ground flat with 600-grit silicon carbide paper and then divided into seven groups of 10 and treated as follows: untreated (control), Monobond Plus, Z-PRIME Plus, ESPE Sil with CoJet, air-abrasion, Monobond Plus with air-abrasion, and Z-PRIME Plus with air-abrasion. Self-adhesive resin cement was placed onto the treated Y-TZP specimens for each group. All specimens were thermocycled and subjected to a shear bond strength test. Scanning electron microscope images of the fractured areas and x-ray diffraction (XRD) analysis of the surface-treated Y-TZP specimens were performed. Data were statistically analyzed using one-way analysis of variance and the Student-Newman-Keuls multiple comparison test (p&lt;0.05). Results The Z-PRIME Plus treatment in combination with air-abrasion produced the highest bond strength (16.50±2.26 MPa), followed by air-abrasion (10.56±3.32 MPa), and then Monobond Plus combined with air-abrasion (8.93±3.13 MPa), ESPE Sil after CoJet application (8.54±3.98 MPa), and the Z-PRIME Plus group (8.27±2.79 MPa). The control (3.91±0.72 MPa) and Monobond Plus (4.86±1.77 MPa) groups indicated the lowest results (p&lt;0.05). The XRD results showed the peaks of the monoclinic phase for the air-abrasion and CoJet treatment groups compared with the Y-TZP control. Conclusion Z-PRIME Plus primer application after air-abrasion presented the best results for improving the bond strength between Y-TZP ceramic and self-adhesive resin cement.

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