scholarly journals Dyeing of Polyester with Reactive Dyestuffs Using Nano-Chitosan

2018 ◽  
Vol 13 (2) ◽  
pp. 155892501801300
Author(s):  
Neda Najafzadeh ◽  
Sima Habibi ◽  
Mohammadreza A. Ghasri

The main objective of this work is to investigate the effect of nano-chitosan on the dyeing of polyester fabric with reactive dyes. Polyester fabric was treated with alkali and coated with nano-chitosan. Afterwards all samples were dyed with reactive dyes. The water absorption and bending resistance of pristine polyester, alkaline and chitosan-treated polyester were measured. In order to investigate surface chemical bonding, FTIR/ATR was employed. Surface morphology of fabrics was observed using scanning electron microscopy (SEM). Wettability and bending behavior of the treated polyester increased compared to the untreated one. The color difference between the dyed blank and chitosan-treated samples was estimated using a spectrophotometer. The data obtained shows it is possible to use reactive dyes to dye polyester fabrics finished with nano-chitosan and the resulting fabrics will exhibit acceptable washing and rubbing fastness.

2018 ◽  
Vol 3 (1) ◽  
pp. 12 ◽  
Author(s):  
Zaimahwati Zaimahwati ◽  
Yuniati Yuniati ◽  
Ramzi Jalal ◽  
Syahman Zhafiri ◽  
Yuli Yetri

<p>Pada penelitian ini telah dilakukan isolasi dan karakterisasi bentonit alam menjadi nanopartikel montmorillonit. Bentonit alam yang digunakan diambil dari desa Blangdalam, Kecamatan Nisam Kabupaten Aceh Utara.  Proses isolasi meliputi proses pelarutan dengan aquades, ultrasonic dan proses sedimentasi. Untuk mengetahui karakterisasi montmorillonit dilakukan uji FT-IR, X-RD dan uji morfologi permukaan dengan Scanning Electron Microscopy (SEM). Partikel size analyzer untuk menganalisis dan menentukan ukuran nanopartikel dari isolasi bentonit alam. Dari hasil penelitian didapat ukuran nanopartikel montmorillonit hasil isolasi dari bentonit alam diperoleh berdiameter rata-rata 82,15 nm.</p><p><em>In this research we have isolated and characterized natural bentonite into montmorillonite nanoparticles. Natural bentonite used was taken from Blangdalam village, Nisam sub-district, North Aceh district. The isolation process includes dissolving process with aquades, ultrasonic and sedimentation processes.  The characterization of montmorillonite, FT-IR, X-RD and surface morphology test by Scanning Electron Microscopy (SEM). Particle size analyzer to analyze and determine the size of nanoparticles from natural bentonite insulation. From the research results obtained the size of montmorillonite nanoparticles isolated from natural bentonite obtained an average diameter of 82.15 nm.</em></p>


Author(s):  
Christina V. Haden ◽  
Donald A. Jordan ◽  
Pamela M. Norris

A novel and inexpensive bucky gel electrode has been investigated for use as the electrode substrate for deposition of polypyrrole. The electroactive polymer membrane was successfully deposited and the surface morphology studied using scanning electron microscopy. Given the properties of the bucky gel electrode and its ability to conduct ions, this work establishes the first step towards a semi-solid ion-gating system to be used in further applications.


2011 ◽  
Vol 183-185 ◽  
pp. 1837-1841
Author(s):  
Lei Sha ◽  
Yan Lai Wang ◽  
Shi Liang Ban

CuInSe2 thin films were obtained by selenization of the Cu-In precursors in the atmosphere of Se vapour, which were prepared on stainless steel and titanium substrates by electrodeposition. The films were characterized by XRD, scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). The respective influences of composition, phases and surface morphology of Cu-In precursors on indium loss were investigated. The results indicate that the indium loss occurs in selenization process because of volatile In2Se arising. The indium loss is less in selenization process of Cu-In precursors contained CuIn, Cu2In and In phases.


Author(s):  
B. NARASIMHA RAO ◽  
K. RAVINDRA REDDY ◽  
S. RAHATH FATHIMA ◽  
P. PREETHI

Objective: In the current investigation,nanosponges were set up by emulsion solvent diffusion technique utilizing ethyl cellulose and β-cyclodextrin as polymers. Methods: Diltiazem hydrochloride is taken as model medication for considering different nanosponge formulations. The similarity of different formulation segments was set up by Fourier Transform Infra-Red (FTIR) spectroscopy. Molecular size, surface morphology, entrapment efficiency and drug content of nanosponges were analyzed. Shape and surface morphology of the nanosponges were inspected utilizing scanning electron microscopy. Results: Molecule size of formulated nanosponges was seen in the scope of 186 to 476 nm. Scanning electron microscopy uncovered the permeable, round nature of the nanosponges. The drug content of nanosponges for ethyl cellulose containing formulations was seen as in the scope of 62.25 to 85.11% and for the β-cyclodextrin containing details were seen as in the scope of 65.18-89.67%. The percentage entrapment effectiveness of nanosponges for ethyl cellulose containing formulations were seen as in the scope of 54.18 to 79.49% and for the β-cyclodextrin containing details were seen as in the scope of 58.21-83.45%. In vitro drugreleasefindings demonstrated that at 12 h ethyl cellulose containing formulations discharged the drug in the scope of 57.27-89.09% and for the β-cyclodextrin containing formulations discharged in the scope of 73.94-93.26%. Conclusion: Sustained drugreleasefrom formulations is supported if there is an occurrence of ethyl cellulose in the formulations rather with plans containing β-cyclodextrin.


1987 ◽  
Vol 67 (4) ◽  
pp. 965-971 ◽  
Author(s):  
J. M. W. BLACK ◽  
M. J. DUDAS

This study compared the surface morphology of quartz grains from A and C horizons of a Chernozem, Luvisol and a Solonetz. Observations and chemical determinations were based on scanning electron microscopy and energy dispersive X-ray analysis of fine sand separates. Features indicative of glacial and eolian transport, physical weathering by low energy subaqueous impact, and chemical dissolution and silica precipitation dominated surface characteristics. Most surface morphological features were of an inherited origin since they were common to solum and parent material samples. Quartz dissolution features were not uniquely associated with solum samples and apparently not of pedogenic origin. Key words: Scanning electron microscopy, quartz, pedogenesis, surface morphology, weathering classification


Parasitology ◽  
1980 ◽  
Vol 81 (2) ◽  
pp. 423-431 ◽  
Author(s):  
V. R. Parshad ◽  
D. W. T. Crompton ◽  
Jean Martin

SUMMARYThe surface morphology of fixed ovarian balls from female Moniliformis dubius, aged 12, 18, 26, 28, 42, 77, 105 and 118 days, has been examined by means of scanning electron microscopy. The appearance of the surface has been found to be variable between ovarian balls from worms of the same and different ages. Some parts of the surface are seen to possess micro-projections, cavities and ridges while other parts have the appearance of an irregular meshwork of fibres. Various protruding features have been observed to extend from the surfaces of the ovarian balls taken from the inseminated female worms. In most cases, the surfaces of the protruding features differ in appearance from the surrounding surfaces of the ovarian balls. Some of these features have been assumed to represent growing zygotes and developing eggs covered by the supporting syncytium of the ovarian ball. Single or several thread-like structures have been observed in association with the surfaces of ovarian balls taken from the inseminated female worms. At present, the thread-like structures are believed to be portions of spermatozoa. By means of light microscopy, preliminary observations have been made on what is considered to be the division process of ovarian balls taken from uninseminated and inseminated worms varying in age from 7 to 98 days.


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