Experiment Test Program Planning and Statistical Analysis Fundamentals

1981 ◽  
Vol 103 (2) ◽  
pp. 164-170 ◽  
Author(s):  
F. Matanzo ◽  
J. T. Metcalf

Nine wire rope terminations were evaluated with respect to true efficiency, service life, and sensitivity to poor workmanship in a comprehensive laboratory test program. The portion of the program concerned with true efficiency, as determined by pull tests to destruction, is reported here. Five diameter values of Lang and Regular construction ropes of the 6 × 19 and 6 × 37 class were used on the following wire rope terminations: Flemish Loop with Steel Sleeve and Thimble, Flemish Loop with Steel Sleeve, Wedge Socket, Swaged Socket, Turn Back Loop with Aluminum Sleeve and Thimble, Thimble Splice with Four Tucks, U-Bolt Clips with Thimble, Zinc Poured Socket, and Resin Poured Socket. The true efficiency was shown to be affected by termination type, rope type, and the interaction of these factors. The efficiency values measured in this test program are less than those reported in the literature which are based on the catalog breaking load rather than on the true breaking load. From a graphic and statistical analysis of the data it was possible to present a selection procedure for optimizing the efficiency.


1966 ◽  
Vol 49 (2) ◽  
pp. 251-254
Author(s):  
L E Mitchell ◽  
A C O’dowd ◽  
D R Patterson

Abstract A collaborative study, begun in 1963, to evaluate an infrared method for determining the DDVP content of four commercially available formulations, was continvied in 1964. Formulations assayed in 1964 were as follows: 0.5% sugar bait, 4 lb/gallon emulsible concentrate, 0.5% spray solution, and 1.0% cattle spray. Special emphasis was placed on refining the procedure applicable to the low-concentration hydrocarbon solutions. A statistical analysis of the data indicates that results of the test program were satisfactory, and the method is recommended for adoption as official, first action.


1966 ◽  
Vol 24 ◽  
pp. 188-189
Author(s):  
T. J. Deeming

If we make a set of measurements, such as narrow-band or multicolour photo-electric measurements, which are designed to improve a scheme of classification, and in particular if they are designed to extend the number of dimensions of classification, i.e. the number of classification parameters, then some important problems of analytical procedure arise. First, it is important not to reproduce the errors of the classification scheme which we are trying to improve. Second, when trying to extend the number of dimensions of classification we have little or nothing with which to test the validity of the new parameters.Problems similar to these have occurred in other areas of scientific research (notably psychology and education) and the branch of Statistics called Multivariate Analysis has been developed to deal with them. The techniques of this subject are largely unknown to astronomers, but, if carefully applied, they should at the very least ensure that the astronomer gets the maximum amount of information out of his data and does not waste his time looking for information which is not there. More optimistically, these techniques are potentially capable of indicating the number of classification parameters necessary and giving specific formulas for computing them, as well as pinpointing those particular measurements which are most crucial for determining the classification parameters.


Author(s):  
Gianluigi Botton ◽  
Gilles L'espérance

As interest for parallel EELS spectrum imaging grows in laboratories equipped with commercial spectrometers, different approaches were used in recent years by a few research groups in the development of the technique of spectrum imaging as reported in the literature. Either by controlling, with a personal computer both the microsope and the spectrometer or using more powerful workstations interfaced to conventional multichannel analysers with commercially available programs to control the microscope and the spectrometer, spectrum images can now be obtained. Work on the limits of the technique, in terms of the quantitative performance was reported, however, by the present author where a systematic study of artifacts detection limits, statistical errors as a function of desired spatial resolution and range of chemical elements to be studied in a map was carried out The aim of the present paper is to show an application of quantitative parallel EELS spectrum imaging where statistical analysis is performed at each pixel and interpretation is carried out using criteria established from the statistical analysis and variations in composition are analyzed with the help of information retreived from t/γ maps so that artifacts are avoided.


Author(s):  
John J. Friel

Committee E-04 on Metallography of the American Society for Testing and Materials (ASTM) conducted an interlaboratory round robin test program on quantitative energy dispersive spectroscopy (EDS). The test program was designed to produce data on which to base a precision and bias statement for quantitative analysis by EDS. Nine laboratories were sent specimens of two well characterized materials, a type 308 stainless steel, and a complex mechanical alloy from Inco Alloys International, Inconel® MA 6000. The stainless steel was chosen as an example of a straightforward analysis with no special problems. The mechanical alloy was selected because elements were present in a wide range of concentrations; K, L, and M lines were involved; and Ta was severely overlapped with W. The test aimed to establish limits of precision that could be routinely achieved by capable laboratories operating under real world conditions. The participants were first allowed to use their own best procedures, but later were instructed to repeat the analysis using specified conditions: 20 kV accelerating voltage, 200s live time, ∼25% dead time and ∼40° takeoff angle. They were also asked to run a standardless analysis.


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