Identification of the sites of 4-hydroxy-2-nonenal and neprilysin adduction using a linear trap quadrapole Velos Pro-Orbitrap Elite mass spectrometer

Two methods — ICP-MS and ICP-AES are used for certification of the new reference material — needles of Siberian pine (NSP-1). Techniques of the analysis include decomposition of plant samples in two different ways: acid digestion in a microwave system MARS-5 and lithium metaborate fusion followed by ICP-MS and ICP-AES analysis of the solutions. Simultaneous determinations of all the elements were carried out in low, medium and high resolution using SF-mass-spectrometer ELEMENT and atomic-emission spectrometer IRIS Advantage with external calibrations and internal standards (In — ICP-MS, Sc —ICP-AES). Middle and high resolutions of ICP mass spectrometer were used for interference corrections. Data obtained by ICP-MS and ICP-AES with different decomposition techniques are in good agreement. The ICP-MS and ICP-AES techniques have been validated by the analysis of three plant reference materials: LB-1 (leaf of a birch), Tr-1 (grass mixture) and EK-1 (Canadian pondweed). These techniques were used for the determination of 38 elements in the new reference material NSP-1. Relative standard deviations for most of the determined elements were below 10%. Combination of ICP-MS and ICP-AES techniques for certification of the new reference material makes it possible to expand the set of elements to be determined and to reduce the total analysis time.

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User's manual for ANALYST version 2.00; An IBM-PC computer program for control of a thermal-ionization, single-collector mass-spectrometer

Open-File Report ◽

10.3133/ofr92543 ◽

1992 ◽

Cited By ~ 2

Author(s):

K. R. Ludwig

Keyword(s):

Computer Program ◽

Mass Spectrometer ◽

Thermal Ionization ◽

Ibm Pc

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РАДИОУГЛЕРОДНЫЕ ДАТИРОВКИ ПАЛЕОНТОЛОГИЧЕСКИХ ОБРАЗЦОВ ВЕРХНЕГО ПЛЕЙСТОЦЕНА НИЖНЕЙ ОБИ

Радиоуглерод в археологии и палеоэкологии: прошлое, настоящее, будущее. Материалы международной конференции, посвященной 80-летию старшего научного сотрудника ИИМК РАН, кандидата химических наук Ганны Ивановны Зайцевой ◽

10.31600/978-5-91867-213-6-33-34 ◽

2020 ◽

Author(s):

I. Zolnikov ◽

◽

A. Vybornov ◽

A. Anoikin ◽

A. Postnov ◽

...

Keyword(s):

Mass Spectrometer ◽

Rangifer Tarandus ◽

Western Siberia ◽

Budker Institute ◽

Mammuthus Primigenius ◽

Upper Pleistocene ◽

Ovibos Moschatus ◽

The North

In the course of studies conducted by IAET SB RAS in the Lower Ob in 2016–2019, the understanding of the conditions for settlement of the Paleolithic population in the north of Western Siberia was significantly supplemented. Dating of a series of paleontological finds was carried out at the "Accelerated mass spectrometer of the Budker Institute of Nucle- ar Physics of SB RAS". The dates obtained show the distribution of the main representatives of the Upper Pleistocene fauna of Subarctica: Mammuthus primigenius – 50,000–15,000 BP, Coelodonta antiquitatis – 43,000–38,000 BP and 27,000–25,000 BP, Rangifer tarandus, Equus ferus – 40,000–10,000 BP, Bison sp. – 50,000–40,000 BP, Ovibos moschatus – 41,000–32,000 BP.

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