Positron Spectroscopy of Hydrogen-Loaded Ti-6Al-4V Alloy with Different Defect Structure

Zirconium alloys, such as Zr-1Nb are widely used as cladding materials for nuclear fuel elements of light water reactors. Hydrogen embrittlement problem causes degradation of these parts of nuclear reactors. It is known, that hydrogen uptake causes changes in microstructure and defect structure of metals. The aim of this work is study of Zr-1Nb alloys’ defect structure after hydrogen saturation up to the concentration of 600 ppm. Saturation of hydrogen was carried out from the gas phase under high temperature and pressure. This study reveals the increase of average positron lifetime with the increase of hydrogen concentration. Value of the average positron lifetime achieves plateau when the concentration of hydrogen is about 600 ppm. Also the following effects were detected in the material after hydrogen uptake up to different concentrations: crystal lattice expansion, dislocations and vacancy-like defects formation, as well as the defect-hydrogen complexes formation.

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Electron Microscope Observations of Mechanical Metamorphism in Iron Meteorites

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100069430 ◽

1970 ◽

Vol 28 ◽

pp. 488-489

Author(s):

D. Faulkner ◽

G.W. Lorimer ◽

H.J. Axon

Keyword(s):

Electron Microscope ◽

Defect Structure ◽

Shock Loading ◽

List Type ◽

Iron Meteorites

It is now generally accepted that meteorites are fragments produced by the collision of parent bodies of asteroidal dimensions. Optical metallographic evidence suggests that there exists a group of iron meteorites which exhibit structures similar to those observed in explosively shock loaded iron. It seems likely that shock loading of meteorites could be produced by preterrestrial impact of their parent bodies as mentioned above.We have therefore looked at the defect structure of one of these meteorites (Trenton) and compared the results with those made on a) an unshocked ‘standard’ meteorite (Canyon Diablo)b) an artificially shocked ‘standard’ meteorite (Canyon Diablo) andc) an artificially shocked specimen of pure α-iron.

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A new type of defect structure in 124-superconducting oxide revealed by HREM

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100089779 ◽

1991 ◽

Vol 49 ◽

pp. 1092-1093

Author(s):

R. Sharma ◽

B.L. Ramakrishna ◽

N.N. Thadhani ◽

D. Hianes ◽

Z. Iqbal

Keyword(s):

Shock Wave ◽

Defect Structure ◽

Neutron Radiation ◽

Weak Links ◽

Defect Structures ◽

New Materials ◽

New Type ◽

Current Densities ◽

Processing Techniques ◽

Microstructural Studies

After materials with superconducting temperatures higher than liquid nitrogen have been prepared, more emphasis has been on increasing the current densities (Jc) of high Tc superconductors than finding new materials with higher transition temperatures. Different processing techniques i.e thin films, shock wave processing, neutron radiation etc. have been applied in order to increase Jc. Microstructural studies of compounds thus prepared have shown either a decrease in gram boundaries that act as weak-links or increase in defect structure that act as flux-pinning centers. We have studied shock wave synthesized Tl-Ba-Cu-O and shock wave processed Y-123 superconductors with somewhat different properties compared to those prepared by solid-state reaction. Here we report the defect structures observed in the shock-processed Y-124 superconductors.

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Defects in ion implanted silicon

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100109070 ◽

1978 ◽

Vol 36 (1) ◽

pp. 386-387

Author(s):

J.A. Lambert ◽

P.S. Dobson

Keyword(s):

Defect Structure ◽

Dislocation Loops ◽

Frank Loop ◽

Burgers Vector ◽

Temperature Range ◽

Perfect Dislocation ◽

Contrast Analysis ◽

Image Position ◽

Ion Implanted

The defect structure of ion-implanted silicon, which has been annealed in the temperature range 800°C-1100°C, consists of extrinsic Frank faulted loops and perfect dislocation loops, together with‘rod like’ defects elongated along <110> directions. Various structures have been suggested for the elongated defects and it was argued that an extrinsically faulted Frank loop could undergo partial shear to yield an intrinsically faulted defect having a Burgers vector of 1/6 <411>.This defect has been observed in boron implanted silicon (1015 B+ cm-2 40KeV) and a detailed contrast analysis has confirmed the proposed structure.

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A crystallographic analysis of the CoSi/Si(111) interface using Transmission Electron Microscopy

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100176009 ◽

1990 ◽

Vol 48 (4) ◽

pp. 574-575

Author(s):

A.C. Daykin ◽

C.J. Kiely ◽

R.C. Pond ◽

J.L. Batstone

Keyword(s):

Electron Microscopy ◽

Transmission Electron Microscopy ◽

Defect Structure ◽

Room Temperature ◽

Theoretical Method ◽

Crystallographic Analysis ◽

Si Substrate ◽

Transmission Electron ◽

Theoretical Predictions

When CoSi2 is grown onto a Si(111) surface it can form in two distinct orientations. A-type CoSi2 has the same orientation as the Si substrate and B-type is rotated by 180° degrees about the [111] surface normal.One method of producing epitaxial CoSi2 is to deposit Co at room temperature and anneal to 650°C.If greater than 10Å of Co is deposited then both A and B-type CoSi2 form via a number of intermediate silicides .The literature suggests that the co-existence of A and B-type CoSi2 is in some way linked to these intermediate silicides analogous to the NiSi2/Si(111) system. The phase which forms prior to complete CoSi2 formation is CoSi. This paper is a crystallographic analysis of the CoSi2/Si(l11) bicrystal using a theoretical method developed by Pond. Transmission electron microscopy (TEM) has been used to verify the theoretical predictions and to characterise the defect structure at the interface.

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