Bias in the Weibull Strength Estimation of a SiC Fiber for the Small Gauge Length Case

Axial tensile modulus, compressive modulus and compressive strength of poly(p-phenylene benzobisoxazole) fiber were measured with a Tecam Micro-tensile Testing Machine. This machine was configured to allow direct tension and compression testing of a single fiber at extremely small gauge length. The measured tensile and compressive moduli were analyzed for machine compliance corrections and possible gauge length error. Results were discussed for the effects of non-uniform stress distribution and fiber misalignment. By comparing the axial compressive strengths measured from various single fiber characterization techniques, direct compression furnished data closer to that measured from composite compressive tests.

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OPTIMIZED MEASUREMENT METHOD OF SMALL GAUGE LENGTH USING STEGER ALGORITHM

The 8th International Symposium on Test Automation & Instrumentation (ISTAI 2020) ◽

10.1049/icp.2021.1301 ◽

2021 ◽

Author(s):

Y. Liu ◽

H. Gao ◽

Y. Cheng ◽

Z. Wang ◽

S. Sun

Keyword(s):

Measurement Method ◽

Gauge Length ◽

Small Gauge

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TEM characterization of reaction zone in a SiC fiber-reinforced titanium alloy

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100105758 ◽

1988 ◽

Vol 46 ◽

pp. 738-739

Author(s):

G. Das ◽

R. E. Omlor

Keyword(s):

Titanium Alloys ◽

Reaction Zone ◽

Carbon Layer ◽

Fiber Reinforced ◽

Reaction Products ◽

Sic Fibers ◽

Sic Fiber ◽

The Matrix ◽

Immense Potential

Fiber reinforced titanium alloys hold immense potential for applications in the aerospace industry. However, chemical reaction between the fibers and the titanium alloys at fabrication temperatures leads to the formation of brittle reaction products which limits their development. In the present study, coated SiC fibers have been used to evaluate the effects of surface coating on the reaction zone in the SiC/IMI829 system.IMI829 (Ti-5.5A1-3.5Sn-3.0Zr-0.3Mo-1Nb-0.3Si), a near alpha alloy, in the form of PREP powder (-35 mesh), was used a茸 the matrix. CVD grown AVCO SCS-6 SiC fibers were used as discontinuous reinforcements. These fibers of 142μm diameter contained an overlayer with high Si/C ratio on top of an amorphous carbon layer, the thickness of the coating being ∽ 1μm. SCS-6 fibers, broken into ∽ 2mm lengths, were mixed with IMI829 powder (representing < 0.1vol%) and the mixture was consolidated by HIP'ing at 871°C/0. 28GPa/4h.

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Deformation at interfaces of Ti-6Al-4V/SiC fiber composites

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100121193 ◽

1992 ◽

Vol 50 (1) ◽

pp. 158-159

Author(s):

Warren J. Moberly ◽

Daniel B. Miracle ◽

S. Krishnamurthy

Keyword(s):

Thermal Stresses ◽

Load Transfer ◽

Coefficient Of Thermal Expansion ◽

Hot Isostatic Pressing ◽

Matrix Composites ◽

Ongoing Research ◽

Aerospace Applications ◽

Sic Fiber ◽

The Matrix ◽

Intermetallic Matrix Composites

Titanium-aluminum alloy metal matrix composites (MMC) and Ti-Al intermetallic matrix composites (IMC), reinforced with continuous SCS6 SiC fibers are leading candidates for high temperature aerospace applications such as the National Aerospace Plane (NASP). The nature of deformation at fiber / matrix interfaces is characterized in this ongoing research. One major concern is the mismatch in coefficient of thermal expansion (CTE) between the Ti-based matrix and the SiC fiber. This can lead to thermal stresses upon cooling down from the temperature incurred during hot isostatic pressing (HIP), which are sufficient to cause yielding in the matrix, and/or lead to fatigue from the thermal cycling that will be incurred during application, A second concern is the load transfer, from fiber to matrix, that is required if/when fiber fracture occurs. In both cases the stresses in the matrix are most severe at the interlace.

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TEM of grain growth and phase transformations during creep of SCS-6 silicon carbide fibers

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100138129 ◽

1995 ◽

Vol 53 ◽

pp. 350-351

Author(s):

L. A. Giannuzzi ◽

C. A. Lewinsohn ◽

C. E. Bakis ◽

R. E. Tressler

Keyword(s):

Silicon Carbide ◽

Creep Rate ◽

Vapor Deposition ◽

Chemical Vapor ◽

Primary Creep ◽

Excess Carbon ◽

Silicon Carbide Fibers ◽

Sic Fiber ◽

Carbon Core ◽

Grain Width

The SCS-6 SiC fiber is a 142 μm diameter fiber consisting of four distinct regions of βSiC. These SiC regions vary in excess carbon content ranging from 10 a/o down to 5 a/o in the SiC1 through SiC3 region. The SiC4 region is stoichiometric. The SiC sub-grains in all regions grow radially outward from the carbon core of the fiber during the chemical vapor deposition processing of these fibers. In general, the sub-grain width changes from 50nm to 250nm while maintaining an aspect ratio of ~10:1 from the SiC1 through the SiC4 regions. In addition, the SiC shows a <110> texture, i.e., the {111} planes lie ±15° along the fiber axes. Previous has shown that the SCS-6 fiber (as well as the SCS-9 and the developmental SCS-50 μm fiber) undergoes primary creep (i.e., the creep rate constantly decreases as a function of time) throughout the lifetime of the creep test.

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